{"title":"Characterisation of strain localisation and crack evolution of Cf/SiC-SiC composites by SEM-DIC method","authors":"Kunjie Wang, Chenghai Xu, Bo Gao, Songhe Meng","doi":"10.1016/j.compositesa.2025.108936","DOIUrl":null,"url":null,"abstract":"<div><div>In thermo-mechanical-oxidative coupling service environments, stress-induced microscale damage in ceramic matrix composites (CMCs) governs diffusion kinetics of oxidising media, accelerating degradation of mechanical properties. Therefore, the quantification of microscale damage is a core issue in revealing damage mechanisms. In this study, a low-cost, highly uniform submicron speckle pattern was prepared on the surface of silicon carbide-coated carbon fibre-reinforced silicon carbide matrix (C<sub>f</sub>/SiC-SiC) composites and the strain localisation and crack evolution were accurately characterised using scanning electron microscopy combined with digital image correlation. For the first time, this study completely tracked and quantified the dynamic damage evolution process of C<sub>f</sub>/SiC-SiC composites at the microscale, including key mechanisms such as strain localisation, interfacial debonding, matrix cracking, fibre slip, and macroscopic failure, further verifying the key contribution of interfacial slip to composite toughening. The experimental results revealed the interaction dynamics of the multicrack system. Further research found that the initial crack widths of the SiC coating follow a log-normal distribution, while the evolution of crack density under tensile load exhibits a strain threshold effect. The crack opening displacement (COD) of the coating has a ‘stress memory’ effect. These findings contribute to deeper understanding of the synergistic effect of stress and oxidation and provide a new perspective for studying the microscale and mesoscale damage behaviour of CMCs.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"194 ","pages":"Article 108936"},"PeriodicalIF":8.1000,"publicationDate":"2025-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Part A: Applied Science and Manufacturing","FirstCategoryId":"1","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1359835X25002301","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
Characterisation of strain localisation and crack evolution of Cf/SiC-SiC composites by SEM-DIC method
In thermo-mechanical-oxidative coupling service environments, stress-induced microscale damage in ceramic matrix composites (CMCs) governs diffusion kinetics of oxidising media, accelerating degradation of mechanical properties. Therefore, the quantification of microscale damage is a core issue in revealing damage mechanisms. In this study, a low-cost, highly uniform submicron speckle pattern was prepared on the surface of silicon carbide-coated carbon fibre-reinforced silicon carbide matrix (Cf/SiC-SiC) composites and the strain localisation and crack evolution were accurately characterised using scanning electron microscopy combined with digital image correlation. For the first time, this study completely tracked and quantified the dynamic damage evolution process of Cf/SiC-SiC composites at the microscale, including key mechanisms such as strain localisation, interfacial debonding, matrix cracking, fibre slip, and macroscopic failure, further verifying the key contribution of interfacial slip to composite toughening. The experimental results revealed the interaction dynamics of the multicrack system. Further research found that the initial crack widths of the SiC coating follow a log-normal distribution, while the evolution of crack density under tensile load exhibits a strain threshold effect. The crack opening displacement (COD) of the coating has a ‘stress memory’ effect. These findings contribute to deeper understanding of the synergistic effect of stress and oxidation and provide a new perspective for studying the microscale and mesoscale damage behaviour of CMCs.
期刊介绍:
Composites Part A: Applied Science and Manufacturing is a comprehensive journal that publishes original research papers, review articles, case studies, short communications, and letters covering various aspects of composite materials science and technology. This includes fibrous and particulate reinforcements in polymeric, metallic, and ceramic matrices, as well as 'natural' composites like wood and biological materials. The journal addresses topics such as properties, design, and manufacture of reinforcing fibers and particles, novel architectures and concepts, multifunctional composites, advancements in fabrication and processing, manufacturing science, process modeling, experimental mechanics, microstructural characterization, interfaces, prediction and measurement of mechanical, physical, and chemical behavior, and performance in service. Additionally, articles on economic and commercial aspects, design, and case studies are welcomed. All submissions undergo rigorous peer review to ensure they contribute significantly and innovatively, maintaining high standards for content and presentation. The editorial team aims to expedite the review process for prompt publication.