{"title":"通过低温固态反应合成纳米级二氧化硒的新方法","authors":"He Zhao, Bocheng Meng, Yanhong Wang, Shikai Zhao","doi":"10.1007/s10876-025-02813-2","DOIUrl":null,"url":null,"abstract":"<div><p>This study presents a novel method for quickly preparing nanoscale SnO<sub>2</sub> materials through a low-heat solid-state reaction. This method utilizes SnSO<sub>4</sub> and H<sub>2</sub>O<sub>2</sub> disinfectant powder (H<sub>2</sub>O<sub>2</sub> as a reactive substance) as raw materials. When the mixed powders were heated to 90 °C, a rapid reaction occurred, which resulted in the formation of SnO<sub>2</sub>. X-ray diffraction results showed that the prepared SnO<sub>2</sub> material was amorphous, The powder exhibited good dispersion, and SnO<sub>2</sub> nanoparticles were approximately 20 nm in size. X-ray photoelectron spectroscopy results revealed that the sample surface was rich in hydroxyl. Finally, a reaction mechanism for preparing nanoscale SnO<sub>2</sub> materials through a solid-state reaction was proposed.</p></div>","PeriodicalId":618,"journal":{"name":"Journal of Cluster Science","volume":"36 3","pages":""},"PeriodicalIF":3.6000,"publicationDate":"2025-04-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A New Approach to Synthesize Nano-Sized SnO2 Via Low Temperature Solid-State Reaction\",\"authors\":\"He Zhao, Bocheng Meng, Yanhong Wang, Shikai Zhao\",\"doi\":\"10.1007/s10876-025-02813-2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>This study presents a novel method for quickly preparing nanoscale SnO<sub>2</sub> materials through a low-heat solid-state reaction. This method utilizes SnSO<sub>4</sub> and H<sub>2</sub>O<sub>2</sub> disinfectant powder (H<sub>2</sub>O<sub>2</sub> as a reactive substance) as raw materials. When the mixed powders were heated to 90 °C, a rapid reaction occurred, which resulted in the formation of SnO<sub>2</sub>. X-ray diffraction results showed that the prepared SnO<sub>2</sub> material was amorphous, The powder exhibited good dispersion, and SnO<sub>2</sub> nanoparticles were approximately 20 nm in size. X-ray photoelectron spectroscopy results revealed that the sample surface was rich in hydroxyl. Finally, a reaction mechanism for preparing nanoscale SnO<sub>2</sub> materials through a solid-state reaction was proposed.</p></div>\",\"PeriodicalId\":618,\"journal\":{\"name\":\"Journal of Cluster Science\",\"volume\":\"36 3\",\"pages\":\"\"},\"PeriodicalIF\":3.6000,\"publicationDate\":\"2025-04-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Cluster Science\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s10876-025-02813-2\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, INORGANIC & NUCLEAR\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Cluster Science","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1007/s10876-025-02813-2","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, INORGANIC & NUCLEAR","Score":null,"Total":0}
A New Approach to Synthesize Nano-Sized SnO2 Via Low Temperature Solid-State Reaction
This study presents a novel method for quickly preparing nanoscale SnO2 materials through a low-heat solid-state reaction. This method utilizes SnSO4 and H2O2 disinfectant powder (H2O2 as a reactive substance) as raw materials. When the mixed powders were heated to 90 °C, a rapid reaction occurred, which resulted in the formation of SnO2. X-ray diffraction results showed that the prepared SnO2 material was amorphous, The powder exhibited good dispersion, and SnO2 nanoparticles were approximately 20 nm in size. X-ray photoelectron spectroscopy results revealed that the sample surface was rich in hydroxyl. Finally, a reaction mechanism for preparing nanoscale SnO2 materials through a solid-state reaction was proposed.
期刊介绍：
The journal publishes the following types of papers: (a) original and important research;
(b) authoritative comprehensive reviews or short overviews of topics of current
interest; (c) brief but urgent communications on new significant research; and (d)
commentaries intended to foster the exchange of innovative or provocative ideas, and
to encourage dialogue, amongst researchers working in different cluster
disciplines.
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