多晶FeCrAl薄膜用作高压氢环境应变片:低零漂、蠕变、灵敏度高

IF 8.3 2区 工程技术 Q1 CHEMISTRY, PHYSICAL
Wanliang Zhang , Jun Wang , Kaiyu Zhang , Ziyan Shen , Wenli Zhang , Ye Zhang , Zhitao Wu , Chengshuang Zhou , Lin Zhang , Jinyang Zheng
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引用次数: 0

摘要

高压氢气系统的内部负载传感器面临着诸如零漂移、蠕变和响应滞后等挑战,这主要是由于氢气渗入传统的电阻应变片。为了解决这一问题,我们开发了一种新型的多晶FeCrAl薄膜,并利用磁控溅射和模板技术在316 L不锈钢衬底上制备了原位Cr/AlN/FeCrAl三明治结构薄膜应变片(TFSG)。结果表明,衬底温度对FeCrAl的显微组织和电阻有显著影响。在400℃时,均匀、精细的体心立方(bcc)多晶薄膜表现出较高的电阻率和电阻稳定性,而较高的温度导致晶粒粗化和缺陷扩散。在12 MPa氢气环境下的测试表明,Cr/AlN/FeCrAl TFSG的耐氢性能优于传统的Cu-Ni应变片,在30με以下无漂移和蠕变,应变敏感系数约为1.62,具有较高的耐氢性能和高压环境的实用性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Polycrystalline FeCrAl thin films used as high-pressure hydrogen environment strain gauges: Low zero-drift, creep, high sensitivity

Polycrystalline FeCrAl thin films used as high-pressure hydrogen environment strain gauges: Low zero-drift, creep, high sensitivity
High-pressure hydrogen systems' internal load sensors face challenges such as zero drift, creep, and response hysteresis, primarily due to hydrogen infiltration into traditional resistive strain gauges. To address this, we developed a novel polycrystalline FeCrAl film and fabricated an in-situ Cr/AlN/FeCrAl sandwich-structure thin-film strain gauge (TFSG) on a 316 L stainless steel substrate using magnetron sputtering and a template technique. Results indicate that substrate temperature significantly affects the microstructure and resistance of FeCrAl. At 400 °C, the uniform, fine body-centered cubic (bcc) polycrystalline film exhibits higher resistivity and resistance stability, while higher temperatures lead to grain coarsening and defect proliferation. Testing in a 12 MPa hydrogen environment shows that the Cr/AlN/FeCrAl TFSG outperforms traditional Cu–Ni strain gauges in hydrogen resistance, with zero drift and creep below 30με and a strain sensitivity coefficient of approximately 1.62, demonstrating high hydrogen resistance and practicality in high-pressure environments.
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来源期刊
International Journal of Hydrogen Energy
International Journal of Hydrogen Energy 工程技术-环境科学
CiteScore
13.50
自引率
25.00%
发文量
3502
审稿时长
60 days
期刊介绍: The objective of the International Journal of Hydrogen Energy is to facilitate the exchange of new ideas, technological advancements, and research findings in the field of Hydrogen Energy among scientists and engineers worldwide. This journal showcases original research, both analytical and experimental, covering various aspects of Hydrogen Energy. These include production, storage, transmission, utilization, enabling technologies, environmental impact, economic considerations, and global perspectives on hydrogen and its carriers such as NH3, CH4, alcohols, etc. The utilization aspect encompasses various methods such as thermochemical (combustion), photochemical, electrochemical (fuel cells), and nuclear conversion of hydrogen, hydrogen isotopes, and hydrogen carriers into thermal, mechanical, and electrical energies. The applications of these energies can be found in transportation (including aerospace), industrial, commercial, and residential sectors.
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