Wanliang Zhang , Jun Wang , Kaiyu Zhang , Ziyan Shen , Wenli Zhang , Ye Zhang , Zhitao Wu , Chengshuang Zhou , Lin Zhang , Jinyang Zheng
{"title":"多晶FeCrAl薄膜用作高压氢环境应变片:低零漂、蠕变、灵敏度高","authors":"Wanliang Zhang , Jun Wang , Kaiyu Zhang , Ziyan Shen , Wenli Zhang , Ye Zhang , Zhitao Wu , Chengshuang Zhou , Lin Zhang , Jinyang Zheng","doi":"10.1016/j.ijhydene.2025.03.402","DOIUrl":null,"url":null,"abstract":"<div><div>High-pressure hydrogen systems' internal load sensors face challenges such as zero drift, creep, and response hysteresis, primarily due to hydrogen infiltration into traditional resistive strain gauges. To address this, we developed a novel polycrystalline FeCrAl film and fabricated an in-situ Cr/AlN/FeCrAl sandwich-structure thin-film strain gauge (TFSG) on a 316 L stainless steel substrate using magnetron sputtering and a template technique. Results indicate that substrate temperature significantly affects the microstructure and resistance of FeCrAl. At 400 °C, the uniform, fine body-centered cubic (bcc) polycrystalline film exhibits higher resistivity and resistance stability, while higher temperatures lead to grain coarsening and defect proliferation. Testing in a 12 MPa hydrogen environment shows that the Cr/AlN/FeCrAl TFSG outperforms traditional Cu–Ni strain gauges in hydrogen resistance, with zero drift and creep below 30με and a strain sensitivity coefficient of approximately 1.62, demonstrating high hydrogen resistance and practicality in high-pressure environments.</div></div>","PeriodicalId":337,"journal":{"name":"International Journal of Hydrogen Energy","volume":"122 ","pages":"Pages 247-257"},"PeriodicalIF":8.3000,"publicationDate":"2025-04-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Polycrystalline FeCrAl thin films used as high-pressure hydrogen environment strain gauges: Low zero-drift, creep, high sensitivity\",\"authors\":\"Wanliang Zhang , Jun Wang , Kaiyu Zhang , Ziyan Shen , Wenli Zhang , Ye Zhang , Zhitao Wu , Chengshuang Zhou , Lin Zhang , Jinyang Zheng\",\"doi\":\"10.1016/j.ijhydene.2025.03.402\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>High-pressure hydrogen systems' internal load sensors face challenges such as zero drift, creep, and response hysteresis, primarily due to hydrogen infiltration into traditional resistive strain gauges. To address this, we developed a novel polycrystalline FeCrAl film and fabricated an in-situ Cr/AlN/FeCrAl sandwich-structure thin-film strain gauge (TFSG) on a 316 L stainless steel substrate using magnetron sputtering and a template technique. Results indicate that substrate temperature significantly affects the microstructure and resistance of FeCrAl. At 400 °C, the uniform, fine body-centered cubic (bcc) polycrystalline film exhibits higher resistivity and resistance stability, while higher temperatures lead to grain coarsening and defect proliferation. Testing in a 12 MPa hydrogen environment shows that the Cr/AlN/FeCrAl TFSG outperforms traditional Cu–Ni strain gauges in hydrogen resistance, with zero drift and creep below 30με and a strain sensitivity coefficient of approximately 1.62, demonstrating high hydrogen resistance and practicality in high-pressure environments.</div></div>\",\"PeriodicalId\":337,\"journal\":{\"name\":\"International Journal of Hydrogen Energy\",\"volume\":\"122 \",\"pages\":\"Pages 247-257\"},\"PeriodicalIF\":8.3000,\"publicationDate\":\"2025-04-03\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Hydrogen Energy\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S036031992501554X\",\"RegionNum\":2,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"CHEMISTRY, PHYSICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Hydrogen Energy","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S036031992501554X","RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}
Polycrystalline FeCrAl thin films used as high-pressure hydrogen environment strain gauges: Low zero-drift, creep, high sensitivity
High-pressure hydrogen systems' internal load sensors face challenges such as zero drift, creep, and response hysteresis, primarily due to hydrogen infiltration into traditional resistive strain gauges. To address this, we developed a novel polycrystalline FeCrAl film and fabricated an in-situ Cr/AlN/FeCrAl sandwich-structure thin-film strain gauge (TFSG) on a 316 L stainless steel substrate using magnetron sputtering and a template technique. Results indicate that substrate temperature significantly affects the microstructure and resistance of FeCrAl. At 400 °C, the uniform, fine body-centered cubic (bcc) polycrystalline film exhibits higher resistivity and resistance stability, while higher temperatures lead to grain coarsening and defect proliferation. Testing in a 12 MPa hydrogen environment shows that the Cr/AlN/FeCrAl TFSG outperforms traditional Cu–Ni strain gauges in hydrogen resistance, with zero drift and creep below 30με and a strain sensitivity coefficient of approximately 1.62, demonstrating high hydrogen resistance and practicality in high-pressure environments.
期刊介绍:
The objective of the International Journal of Hydrogen Energy is to facilitate the exchange of new ideas, technological advancements, and research findings in the field of Hydrogen Energy among scientists and engineers worldwide. This journal showcases original research, both analytical and experimental, covering various aspects of Hydrogen Energy. These include production, storage, transmission, utilization, enabling technologies, environmental impact, economic considerations, and global perspectives on hydrogen and its carriers such as NH3, CH4, alcohols, etc.
The utilization aspect encompasses various methods such as thermochemical (combustion), photochemical, electrochemical (fuel cells), and nuclear conversion of hydrogen, hydrogen isotopes, and hydrogen carriers into thermal, mechanical, and electrical energies. The applications of these energies can be found in transportation (including aerospace), industrial, commercial, and residential sectors.