Syed Mohd Adnan Naqvi , Sk Najrul Islam , Azam Raza , Deepa Kshirsagar , Padmaja Chavan , Vishakha Chankeshwara , Shakeel Ahmad Firdousi , Absar Ahmad
{"title":"柽柳提取物快速生物合成n掺杂TiO2纳米粒子及其抗菌、抗氧化活性和介电性能","authors":"Syed Mohd Adnan Naqvi , Sk Najrul Islam , Azam Raza , Deepa Kshirsagar , Padmaja Chavan , Vishakha Chankeshwara , Shakeel Ahmad Firdousi , Absar Ahmad","doi":"10.1016/j.nxmate.2025.100624","DOIUrl":null,"url":null,"abstract":"<div><div>Green synthesis is a technique for the fabrication of nanoparticles (NPs) that is easy, eco-friendly, and emergent. It is currently garnering the attention of the scientific community worldwide since it is non-toxic, inexpensive, and reliable, and it takes place under ambient conditions. This research aimed to synthesize green N-doped titanium dioxide nanoparticles (N-TiO<sub>2</sub>) and analyze their antimicrobial, anti-oxidant activity, and dielectric properties. A leaf extract of <em>Tamarix</em> sp. was used in a single step at room temperature to fabricate N-TiO<sub>2</sub> nanoparticles with an average particle size of 26.5 nm. They were subsequently characterized by certain methods like Ultra Violet-Visible spectroscopy, Transmission Electron Microscopy, Field Emission Scanning Electron Microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, Fourier Transform Infra-Red Spectroscopy, etc. Moreover, the efficiency of the synthesized nanoparticles as antimicrobial agents was investigated against <em>Bacillus subtilis</em>, <em>Escherichia coli</em> and <em>Aspergillus niger</em>. Using 2, 2-diphenyl-1-picrylhydrazyl hydrate (DPPH), the antioxidant activity of synthesized N-TiO<sub>2</sub> nanoparticles (NPs) was evaluated. UV–visible spectrophotometry was used to monitor the radical-scavenging activity of N-TiO<sub>2</sub> NPs. The dielectric properties were examined with the help of impedence analyzer and we observed high dielectric constant and very low tangent loss.</div></div>","PeriodicalId":100958,"journal":{"name":"Next Materials","volume":"7 ","pages":"Article 100624"},"PeriodicalIF":0.0000,"publicationDate":"2025-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Rapid biosynthesis of N-doped TiO2 nanoparticles using plant extract of Tamarix sp.: Its antimicrobial, anti-oxidant activity and dielectric properties\",\"authors\":\"Syed Mohd Adnan Naqvi , Sk Najrul Islam , Azam Raza , Deepa Kshirsagar , Padmaja Chavan , Vishakha Chankeshwara , Shakeel Ahmad Firdousi , Absar Ahmad\",\"doi\":\"10.1016/j.nxmate.2025.100624\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Green synthesis is a technique for the fabrication of nanoparticles (NPs) that is easy, eco-friendly, and emergent. It is currently garnering the attention of the scientific community worldwide since it is non-toxic, inexpensive, and reliable, and it takes place under ambient conditions. This research aimed to synthesize green N-doped titanium dioxide nanoparticles (N-TiO<sub>2</sub>) and analyze their antimicrobial, anti-oxidant activity, and dielectric properties. A leaf extract of <em>Tamarix</em> sp. was used in a single step at room temperature to fabricate N-TiO<sub>2</sub> nanoparticles with an average particle size of 26.5 nm. They were subsequently characterized by certain methods like Ultra Violet-Visible spectroscopy, Transmission Electron Microscopy, Field Emission Scanning Electron Microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, Fourier Transform Infra-Red Spectroscopy, etc. Moreover, the efficiency of the synthesized nanoparticles as antimicrobial agents was investigated against <em>Bacillus subtilis</em>, <em>Escherichia coli</em> and <em>Aspergillus niger</em>. Using 2, 2-diphenyl-1-picrylhydrazyl hydrate (DPPH), the antioxidant activity of synthesized N-TiO<sub>2</sub> nanoparticles (NPs) was evaluated. UV–visible spectrophotometry was used to monitor the radical-scavenging activity of N-TiO<sub>2</sub> NPs. The dielectric properties were examined with the help of impedence analyzer and we observed high dielectric constant and very low tangent loss.</div></div>\",\"PeriodicalId\":100958,\"journal\":{\"name\":\"Next Materials\",\"volume\":\"7 \",\"pages\":\"Article 100624\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2025-04-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Next Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S294982282500142X\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Next Materials","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S294982282500142X","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Rapid biosynthesis of N-doped TiO2 nanoparticles using plant extract of Tamarix sp.: Its antimicrobial, anti-oxidant activity and dielectric properties
Green synthesis is a technique for the fabrication of nanoparticles (NPs) that is easy, eco-friendly, and emergent. It is currently garnering the attention of the scientific community worldwide since it is non-toxic, inexpensive, and reliable, and it takes place under ambient conditions. This research aimed to synthesize green N-doped titanium dioxide nanoparticles (N-TiO2) and analyze their antimicrobial, anti-oxidant activity, and dielectric properties. A leaf extract of Tamarix sp. was used in a single step at room temperature to fabricate N-TiO2 nanoparticles with an average particle size of 26.5 nm. They were subsequently characterized by certain methods like Ultra Violet-Visible spectroscopy, Transmission Electron Microscopy, Field Emission Scanning Electron Microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, Fourier Transform Infra-Red Spectroscopy, etc. Moreover, the efficiency of the synthesized nanoparticles as antimicrobial agents was investigated against Bacillus subtilis, Escherichia coli and Aspergillus niger. Using 2, 2-diphenyl-1-picrylhydrazyl hydrate (DPPH), the antioxidant activity of synthesized N-TiO2 nanoparticles (NPs) was evaluated. UV–visible spectrophotometry was used to monitor the radical-scavenging activity of N-TiO2 NPs. The dielectric properties were examined with the help of impedence analyzer and we observed high dielectric constant and very low tangent loss.