柽柳提取物快速生物合成n掺杂TiO2纳米粒子及其抗菌、抗氧化活性和介电性能

Syed Mohd Adnan Naqvi , Sk Najrul Islam , Azam Raza , Deepa Kshirsagar , Padmaja Chavan , Vishakha Chankeshwara , Shakeel Ahmad Firdousi , Absar Ahmad
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引用次数: 0

摘要

绿色合成是一种制备纳米粒子(NPs)的简单、环保且新兴的技术。由于它无毒、廉价、可靠,而且是在环境条件下进行的,目前正受到全世界科学界的关注。本研究旨在合成绿色n掺杂二氧化钛纳米颗粒(N-TiO2),并分析其抗菌、抗氧化活性和介电性能。以柽柳叶提取物为原料,在室温条件下一步制得平均粒径为26.5 nm的N-TiO2纳米颗粒。随后用紫外可见光谱、透射电子显微镜、场发射扫描电子显微镜、x射线衍射、x射线光电子能谱、傅立叶变换红外光谱等方法对它们进行了表征。此外,还研究了合成的纳米颗粒对枯草芽孢杆菌、大肠杆菌和黑曲霉的抑菌效果。以2,2 -二苯基-1-吡啶酰水合肼(DPPH)为原料,对合成的N-TiO2纳米粒子(NPs)的抗氧化活性进行了评价。紫外可见分光光度法测定了N-TiO2 NPs的自由基清除活性。利用阻抗分析仪对其介电性能进行了测试,发现其介电常数较高,切线损耗极低。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Rapid biosynthesis of N-doped TiO2 nanoparticles using plant extract of Tamarix sp.: Its antimicrobial, anti-oxidant activity and dielectric properties
Green synthesis is a technique for the fabrication of nanoparticles (NPs) that is easy, eco-friendly, and emergent. It is currently garnering the attention of the scientific community worldwide since it is non-toxic, inexpensive, and reliable, and it takes place under ambient conditions. This research aimed to synthesize green N-doped titanium dioxide nanoparticles (N-TiO2) and analyze their antimicrobial, anti-oxidant activity, and dielectric properties. A leaf extract of Tamarix sp. was used in a single step at room temperature to fabricate N-TiO2 nanoparticles with an average particle size of 26.5 nm. They were subsequently characterized by certain methods like Ultra Violet-Visible spectroscopy, Transmission Electron Microscopy, Field Emission Scanning Electron Microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, Fourier Transform Infra-Red Spectroscopy, etc. Moreover, the efficiency of the synthesized nanoparticles as antimicrobial agents was investigated against Bacillus subtilis, Escherichia coli and Aspergillus niger. Using 2, 2-diphenyl-1-picrylhydrazyl hydrate (DPPH), the antioxidant activity of synthesized N-TiO2 nanoparticles (NPs) was evaluated. UV–visible spectrophotometry was used to monitor the radical-scavenging activity of N-TiO2 NPs. The dielectric properties were examined with the help of impedence analyzer and we observed high dielectric constant and very low tangent loss.
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