回收污泥焚烧灰高效制备泡沫混凝土:性能、微观结构和机理

Huang Xuquan , Yuhao , Wang Haojie , Xie Xiuqing , Qi Chunbiao , Xue Fei , Zhao Xiaorong
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引用次数: 0

摘要

研究了污泥焚烧灰(SIA)、高炉矿渣(BS)和硅酸盐水泥(PO)制备泡沫混凝土的性能。采用Minitab软件进行混合设计,对SIA、BS、PO进行三组分实验设计,优化确定最佳组分比。探讨了两种外加剂对不同龄期泡沫混凝土抗压强度和干密度的影响。采用XRD和SEM分析了泡沫混凝土的硬化机理。以反应物掺量为变量,泡沫混凝土抗压强度为预期响应。Minitab软件的结果表明,变量与响应之间的回归系数非常高。7天抗压强度的R-sq值为95.03 %,28天抗压强度的R-sq值为96.34 %(其中R-sq表示模型数据拟合的精度;越接近100 %,拟合精度越高)。实测值与拟合值之间的差异较小,说明拟合模型性能良好。最佳配比为SIA 30.87 %,BS 28.65 %,PO 40.48 %。在此条件下,泡沫混凝土的最大抗压强度分别为3.60 MPa (7d)和9.53 MPa (28d),对应的干密度分别为1235 kg/m³ 和1252 kg/m³ 。污泥焚烧灰表现出火山灰活性。其中所含的活性SiO2和活性Fe2O3在室温下与水泥发生水化反应,生成C-S-H凝胶和不溶性AFt相。这些物质相互联锁,形成致密的微观结构,为泡沫混凝土提供了早期强度。考虑外加剂对泡沫混凝土性能的影响,实验数据表明,多羧酸型高效减水剂和硫酸钠型早强剂的加入显著改善了泡沫混凝土的力学性能。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Recycle sludge incineration ash for efficient preparation of foam concrete: Performance, microstructure, and mechanisms
In this paper, the performance of producing foamed concrete by sludge incineration ash(SIA), blast furnace slag(BS) and Portland cement(PO) was investigated. The mixture design in Minitab software was employed to conduct three-component experimental design for SIA, BS and PO and to optimize and determine the optimal component ratio. The influence of two admixtures on the compressive strength and dry density of foamed concrete at different ages was explored. The hardening mechanism of foamed concrete was analyzed by XRD and SEM. With the amount of reactant as the variable, the compressive strength of foam concrete was the expected response. The results of Minitab software showed that the regression coefficient between the variable and the response was very high. The R-sq value of the 7-day compressive strength was 95.03 %, and the 28-day compressive strength was 96.34 % (where R-sq represents the accuracy of the model data fitting; the closer to 100 %, the higher the fitting accuracy). The difference between the measured values and the fitting value was small, indicating that the fitting model performed well. The optimal mix ratio was 30.87 % SIA, 28.65 % BS and 40.48 % PO. Under this condition, the maximum compressive strength of foam concrete were 3.60 MPa (7d) and 9.53 MPa (28d), with corresponding dry densities of 1235 kg/m³ and 1252 kg/m³ . Sludge incineration ash exhibits pozzolanic activity. The reactive SiO2 and active Fe2O3 contained in it can undergo hydration reactions with cement at room temperature, generating C-S-H gel and insoluble AFt phases. These substances interlocked with each other, forming a dense microstructure that provided early strength to the foam concrete. Considering the effect of admixtures on the performance of foamed concrete, the experimental data demonstrated that the addition of polycarboxylic superplasticizer and sodium sulfate-based early strength agent significantly improved the mechanical properties of foamed concrete.
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