利用大功率平顶激光对涡轮叶片专用镍基高温合金进行激光粉末床熔合:迈向高速制造和定向凝固

IF 6.3 2区 材料科学 Q2 CHEMISTRY, PHYSICAL
Jia Chen, Mengxiao Jin, Kaiwen Wei, Runsen Zhou, Xiaoze Yue, Yuguang Liu, Gaohang Li, Jingjing Liang, Xiaofeng Sun, Xiaoyan Zeng
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引用次数: 0

摘要

ZGH451合金是一种专为涡轮叶片设计的新型定向凝固镍基高温合金,本文采用高功率平顶激光进行激光粉末床金属熔合(PBF-LB/M)增材制造工艺。研究了ZGH451合金的相组成、金相缺陷、晶型速率、显微组织、晶粒形貌、晶体取向和显微硬度,并与传统PBF-LB/M工艺的结果进行了比较。通过适当的工艺参数,高功率平顶激光(HF-PBF-LB/M)和低功率高斯激光(LG-PBF-LB/M)制备的试样均表现出高于99.5%的相对密度。然而,在HF-PBF-LB/M试样中观察到一些热裂纹。LG-PBF-LB/M试样的构建速率仅为5.2 cm3/h,而HF-PBF-LB/M试样的构建速率高达103.0 cm3/h,是前者的19.8倍。制备后的ZGH451的相组成和显微组织随激光类型的变化而变化。lf - pbf - lb /M试样的相组成主要由γ- ni基体相、γ′相和MC碳化物组成,而HF-PBF-LB/M试样除含有γ- ni基体相、γ′相和MC碳化物外,还含有γ/γ′共晶。与LG-PBF-LB/M试样相比,HF-PBF-LB/M试样表现出更粗的细胞枝晶、γ′沉淀和MC碳化物。LG-PBF-LB/M试样和HF-PBF-LB/M试样的凝固组织均为柱状晶粒和等轴晶粒的混合体。LG-PBF-LB/M试样中晶向为“<001>;//构筑方向”的柱状晶粒比例约为41.2%。相反,HF-PBF-LB/M试样中晶向为“<001>;//构建方向”的柱状晶粒比例显著增加,达到98.3%左右,表明HF-PBF-LB/M试样的定向凝固倾向强于LG-PBF-LB/M试样。两种试样均存在显微硬度的各向异性,HF-PBF-LB/M试样的显微硬度值略高于LG-PBF-LB/M试样。综上所述,在PBF-LB/M过程中,使用大功率平顶激光有助于提高ZGH451合金的构建速度,增强其定向凝固趋势,但也会导致热裂纹、组织粗化以及有害γ/γ′共晶的形成等新问题,因此需要进一步研究。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Laser-based powder bed fusion of nickel-based superalloy designed specifically for turbine blades using high-power flat-top laser: Towards high-speed manufacturing and directional solidification
In this paper, high-power flat-top laser is used during the laser-based powder bed fusion of metals (PBF-LB/M) additive manufacturing process of the ZGH451 alloy, which is a new-type directionally solidified nickel-based superalloy designed specifically for turbine blades. The phase composition, metallurgical defects, build rate, microstructure, grain morphology, crystal orientation, and microhardness of the as-built ZGH451 alloy are studied and compared with the corresponding results of the conventional PBF-LB/M technology using low-power Gaussian laser. By using appropriate processing parameters, both the specimen built using the high-power flat-top laser (hereafter called as HF-PBF-LB/M specimen) and that built using the low-power Gaussian laser (hereafter called as LG-PBF-LB/M specimen) exhibit acceptable relative density that is higher than 99.5%. However, some hot cracks are observed in the HF-PBF-LB/M specimen. The build rate of the LG-PBF-LB/M specimen is only 5.2 cm3/h, while the build rate of the HF-PBF-LB/M specimen is as high as 103.0 cm3/h, which is 19.8 times of the former. The phase composition and microstructure of as-built ZGH451 change with the employed laser type. The phase composition of the LG-PBF-LB/M specimen is mainly composed of γ-Ni matrix phase, γ' precipitate, and MC carbide, while the HF-PBF-LB/M specimen also contains some γ/γ' eutectics in addition to γ-Ni matrix phase, γ' precipitate, and MC carbide. In comparison with the LG-PBF-LB/M specimen, the HF-PBF-LB/M specimen exhibits coarser cellular dendrite, γ' precipitate, and MC carbide. The solidification microstructure of both the LG-PBF-LB/M specimen and the HF-PBF-LB/M specimen presents a mixture of columnar grains and equiaxed grains. The proportion of the columnar grains with "<001>//building direction" crystal orientation of the LG-PBF-LB/M specimen is about 41.2%. In contrast, the proportion of the columnar grains with "<001>//building direction" crystal orientation of the HF-PBF-LB/M specimen increases significantly to about 98.3%, which means the HF-PBF-LB/M specimen exhibits stronger directional solidification trend than the LG-PBF-LB/M specimen. There is microhardness anisotropy in both kinds of specimens and the microhardness value of HF-PBF-LB/M specimen is slightly higher than that of LG-PBF-LB/M specimen. In summary, using high-power flat-top laser is helpful to increase the build rate and also enhance the directional solidification trend of the ZGH451 alloy during PBF-LB/M processes, but it also leads to some new issues such as hot cracks, the coarsening of microstructure, and the formation of harmful γ/γ' eutectics, therefore requiring further research.
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来源期刊
Journal of Alloys and Compounds
Journal of Alloys and Compounds 工程技术-材料科学:综合
CiteScore
11.10
自引率
14.50%
发文量
5146
审稿时长
67 days
期刊介绍: The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.
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