{"title":"利用大功率平顶激光对涡轮叶片专用镍基高温合金进行激光粉末床熔合:迈向高速制造和定向凝固","authors":"Jia Chen, Mengxiao Jin, Kaiwen Wei, Runsen Zhou, Xiaoze Yue, Yuguang Liu, Gaohang Li, Jingjing Liang, Xiaofeng Sun, Xiaoyan Zeng","doi":"10.1016/j.jallcom.2025.179902","DOIUrl":null,"url":null,"abstract":"In this paper, high-power flat-top laser is used during the laser-based powder bed fusion of metals (PBF-LB/M) additive manufacturing process of the ZGH451 alloy, which is a new-type directionally solidified nickel-based superalloy designed specifically for turbine blades. The phase composition, metallurgical defects, build rate, microstructure, grain morphology, crystal orientation, and microhardness of the as-built ZGH451 alloy are studied and compared with the corresponding results of the conventional PBF-LB/M technology using low-power Gaussian laser. By using appropriate processing parameters, both the specimen built using the high-power flat-top laser (hereafter called as HF-PBF-LB/M specimen) and that built using the low-power Gaussian laser (hereafter called as LG-PBF-LB/M specimen) exhibit acceptable relative density that is higher than 99.5%. However, some hot cracks are observed in the HF-PBF-LB/M specimen. The build rate of the LG-PBF-LB/M specimen is only 5.2 cm<sup>3</sup>/h, while the build rate of the HF-PBF-LB/M specimen is as high as 103.0 cm<sup>3</sup>/h, which is 19.8 times of the former. The phase composition and microstructure of as-built ZGH451 change with the employed laser type. The phase composition of the LG-PBF-LB/M specimen is mainly composed of γ-Ni matrix phase, γ' precipitate, and MC carbide, while the HF-PBF-LB/M specimen also contains some γ/γ' eutectics in addition to γ-Ni matrix phase, γ' precipitate, and MC carbide. In comparison with the LG-PBF-LB/M specimen, the HF-PBF-LB/M specimen exhibits coarser cellular dendrite, γ' precipitate, and MC carbide. The solidification microstructure of both the LG-PBF-LB/M specimen and the HF-PBF-LB/M specimen presents a mixture of columnar grains and equiaxed grains. The proportion of the columnar grains with \"<001>//building direction\" crystal orientation of the LG-PBF-LB/M specimen is about 41.2%. In contrast, the proportion of the columnar grains with \"<001>//building direction\" crystal orientation of the HF-PBF-LB/M specimen increases significantly to about 98.3%, which means the HF-PBF-LB/M specimen exhibits stronger directional solidification trend than the LG-PBF-LB/M specimen. There is microhardness anisotropy in both kinds of specimens and the microhardness value of HF-PBF-LB/M specimen is slightly higher than that of LG-PBF-LB/M specimen. In summary, using high-power flat-top laser is helpful to increase the build rate and also enhance the directional solidification trend of the ZGH451 alloy during PBF-LB/M processes, but it also leads to some new issues such as hot cracks, the coarsening of microstructure, and the formation of harmful γ/γ' eutectics, therefore requiring further research.","PeriodicalId":344,"journal":{"name":"Journal of Alloys and Compounds","volume":"88 1","pages":""},"PeriodicalIF":6.3000,"publicationDate":"2025-03-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Laser-based powder bed fusion of nickel-based superalloy designed specifically for turbine blades using high-power flat-top laser: Towards high-speed manufacturing and directional solidification\",\"authors\":\"Jia Chen, Mengxiao Jin, Kaiwen Wei, Runsen Zhou, Xiaoze Yue, Yuguang Liu, Gaohang Li, Jingjing Liang, Xiaofeng Sun, Xiaoyan Zeng\",\"doi\":\"10.1016/j.jallcom.2025.179902\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this paper, high-power flat-top laser is used during the laser-based powder bed fusion of metals (PBF-LB/M) additive manufacturing process of the ZGH451 alloy, which is a new-type directionally solidified nickel-based superalloy designed specifically for turbine blades. The phase composition, metallurgical defects, build rate, microstructure, grain morphology, crystal orientation, and microhardness of the as-built ZGH451 alloy are studied and compared with the corresponding results of the conventional PBF-LB/M technology using low-power Gaussian laser. By using appropriate processing parameters, both the specimen built using the high-power flat-top laser (hereafter called as HF-PBF-LB/M specimen) and that built using the low-power Gaussian laser (hereafter called as LG-PBF-LB/M specimen) exhibit acceptable relative density that is higher than 99.5%. However, some hot cracks are observed in the HF-PBF-LB/M specimen. The build rate of the LG-PBF-LB/M specimen is only 5.2 cm<sup>3</sup>/h, while the build rate of the HF-PBF-LB/M specimen is as high as 103.0 cm<sup>3</sup>/h, which is 19.8 times of the former. The phase composition and microstructure of as-built ZGH451 change with the employed laser type. The phase composition of the LG-PBF-LB/M specimen is mainly composed of γ-Ni matrix phase, γ' precipitate, and MC carbide, while the HF-PBF-LB/M specimen also contains some γ/γ' eutectics in addition to γ-Ni matrix phase, γ' precipitate, and MC carbide. In comparison with the LG-PBF-LB/M specimen, the HF-PBF-LB/M specimen exhibits coarser cellular dendrite, γ' precipitate, and MC carbide. The solidification microstructure of both the LG-PBF-LB/M specimen and the HF-PBF-LB/M specimen presents a mixture of columnar grains and equiaxed grains. The proportion of the columnar grains with \\\"<001>//building direction\\\" crystal orientation of the LG-PBF-LB/M specimen is about 41.2%. In contrast, the proportion of the columnar grains with \\\"<001>//building direction\\\" crystal orientation of the HF-PBF-LB/M specimen increases significantly to about 98.3%, which means the HF-PBF-LB/M specimen exhibits stronger directional solidification trend than the LG-PBF-LB/M specimen. There is microhardness anisotropy in both kinds of specimens and the microhardness value of HF-PBF-LB/M specimen is slightly higher than that of LG-PBF-LB/M specimen. In summary, using high-power flat-top laser is helpful to increase the build rate and also enhance the directional solidification trend of the ZGH451 alloy during PBF-LB/M processes, but it also leads to some new issues such as hot cracks, the coarsening of microstructure, and the formation of harmful γ/γ' eutectics, therefore requiring further research.\",\"PeriodicalId\":344,\"journal\":{\"name\":\"Journal of Alloys and Compounds\",\"volume\":\"88 1\",\"pages\":\"\"},\"PeriodicalIF\":6.3000,\"publicationDate\":\"2025-03-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Alloys and Compounds\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1016/j.jallcom.2025.179902\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, PHYSICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Alloys and Compounds","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1016/j.jallcom.2025.179902","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}
Laser-based powder bed fusion of nickel-based superalloy designed specifically for turbine blades using high-power flat-top laser: Towards high-speed manufacturing and directional solidification
In this paper, high-power flat-top laser is used during the laser-based powder bed fusion of metals (PBF-LB/M) additive manufacturing process of the ZGH451 alloy, which is a new-type directionally solidified nickel-based superalloy designed specifically for turbine blades. The phase composition, metallurgical defects, build rate, microstructure, grain morphology, crystal orientation, and microhardness of the as-built ZGH451 alloy are studied and compared with the corresponding results of the conventional PBF-LB/M technology using low-power Gaussian laser. By using appropriate processing parameters, both the specimen built using the high-power flat-top laser (hereafter called as HF-PBF-LB/M specimen) and that built using the low-power Gaussian laser (hereafter called as LG-PBF-LB/M specimen) exhibit acceptable relative density that is higher than 99.5%. However, some hot cracks are observed in the HF-PBF-LB/M specimen. The build rate of the LG-PBF-LB/M specimen is only 5.2 cm3/h, while the build rate of the HF-PBF-LB/M specimen is as high as 103.0 cm3/h, which is 19.8 times of the former. The phase composition and microstructure of as-built ZGH451 change with the employed laser type. The phase composition of the LG-PBF-LB/M specimen is mainly composed of γ-Ni matrix phase, γ' precipitate, and MC carbide, while the HF-PBF-LB/M specimen also contains some γ/γ' eutectics in addition to γ-Ni matrix phase, γ' precipitate, and MC carbide. In comparison with the LG-PBF-LB/M specimen, the HF-PBF-LB/M specimen exhibits coarser cellular dendrite, γ' precipitate, and MC carbide. The solidification microstructure of both the LG-PBF-LB/M specimen and the HF-PBF-LB/M specimen presents a mixture of columnar grains and equiaxed grains. The proportion of the columnar grains with "<001>//building direction" crystal orientation of the LG-PBF-LB/M specimen is about 41.2%. In contrast, the proportion of the columnar grains with "<001>//building direction" crystal orientation of the HF-PBF-LB/M specimen increases significantly to about 98.3%, which means the HF-PBF-LB/M specimen exhibits stronger directional solidification trend than the LG-PBF-LB/M specimen. There is microhardness anisotropy in both kinds of specimens and the microhardness value of HF-PBF-LB/M specimen is slightly higher than that of LG-PBF-LB/M specimen. In summary, using high-power flat-top laser is helpful to increase the build rate and also enhance the directional solidification trend of the ZGH451 alloy during PBF-LB/M processes, but it also leads to some new issues such as hot cracks, the coarsening of microstructure, and the formation of harmful γ/γ' eutectics, therefore requiring further research.
期刊介绍:
The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.