Bhumika K. P., Mayookha V. P., Arun Sharma K, Suresh Kumar G.
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To further confirm the reduction in the acid value of the treated oil, multiple methods were used, including FFA measurement by titration, gas chromatography (GC), high-performance liquid chromatography (HPLC), and attenuated total reflectance Fourier-transform infrared spectroscopy (ATR-FTIR). All these methods consistently demonstrated a reduction in FFA levels in the oil collected after treatment with resin. Additionally, to assess the effect of the resin on the oil, various physicochemical parameters were analyzed. It was found that most of the tocopherols and tocotrienols were preserved, and there was little to no impact on other key quality parameters.</p>\n <p><i>Practical Applications</i>: Our study offers valuable insights into the development of a deacidification technology for removing FFAs from oil using resins. This environment-friendly method effectively tackles the challenge of high acidity in oils by efficiently adsorbing FFAs. 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引用次数: 0
摘要
在食品领域,植物油的脱酸对提高食用油的稳定性、质量和保质期至关重要。目前还很难找到一种高效的脱酸方法,利用高酸值油生产出高质量和高附加值的食用产品。本工作提供了一种新开发的适应性强、长效的离子交换脱酸方法。以不同浓度的Amberlite IRA 400 (AMT)、Amberlyst A26 (A26)和Dowex WGR-2 (DOX)三种不同的离子交换树脂为吸附柱,对游离脂肪酸(FFAs)的去除效果进行了评价,其中AMT(85.92%)和A26(98.02%)的效果优于DOX(75.4%)。为了进一步证实处理后油的酸值降低,采用了多种方法,包括滴定法测定FFA、气相色谱法(GC)、高效液相色谱法(HPLC)和衰减全反射傅里叶变换红外光谱法(ATR-FTIR)。所有这些方法一致表明,树脂处理后收集的油中FFA水平降低。此外,为了评估树脂对油的影响,分析了各种理化参数。结果发现,大部分生育酚和生育三烯醇被保存下来,对其他关键质量参数的影响很小或没有影响。实际应用:我们的研究为使用树脂从油中去除游离脂肪酸的脱酸技术的发展提供了有价值的见解。这种环境友好的方法通过有效地吸附游离脂肪酸,有效地解决了油脂中高酸度的挑战。树脂的使用提供了一种有效的解决方案,同时保留了油的营养特性,使其成为传统方法的一种有吸引力的替代方案。这项技术在工业应用方面具有巨大的潜力,例如通过去除FFA来提高食用油的质量和保质期,以及减少碱处理过程中的浪费。实施这项技术有助于在石油加工行业推广更好的做法。
Deacidification of Coconut Oil Using Different Resins: A Comparative Study
In the food sector, deacidification of vegetable oil is essential for enhancing edible oil's stability, quality, and shelf life. It is still difficult to come up with an efficient deacidification method that makes use of high-acid-value oil to produce edible goods that are both high-quality and value-added. The present work provides a newly developed, adaptable, and long-lasting ion exchange deacidification method. Three different ion exchange resins, that is, Amberlite IRA 400 (AMT), Amberlyst A26 (A26), and Dowex WGR-2 (DOX) at different concentrations were assessed to remove free fatty acids (FFAs) by adsorption using a column, where AMT (85.92%) and A26 (98.02%) showed a good result compared to DOX (75.4%). To further confirm the reduction in the acid value of the treated oil, multiple methods were used, including FFA measurement by titration, gas chromatography (GC), high-performance liquid chromatography (HPLC), and attenuated total reflectance Fourier-transform infrared spectroscopy (ATR-FTIR). All these methods consistently demonstrated a reduction in FFA levels in the oil collected after treatment with resin. Additionally, to assess the effect of the resin on the oil, various physicochemical parameters were analyzed. It was found that most of the tocopherols and tocotrienols were preserved, and there was little to no impact on other key quality parameters.
Practical Applications: Our study offers valuable insights into the development of a deacidification technology for removing FFAs from oil using resins. This environment-friendly method effectively tackles the challenge of high acidity in oils by efficiently adsorbing FFAs. The use of resins provides an efficient solution while retaining the nutritional properties of the oil, making it an appealing alternative to traditional methods. This technology holds significant potential for industrial applications, such as improving the quality and shelf life of edible oils by removing FFA, as well as reducing waste during alkali treatment. Implementing this technique can help promote better practices in the oil processing industry.
期刊介绍:
The European Journal of Lipid Science and Technology is a peer-reviewed journal publishing original research articles, reviews, and other contributions on lipid related topics in food science and technology, biomedical science including clinical and pre-clinical research, nutrition, animal science, plant and microbial lipids, (bio)chemistry, oleochemistry, biotechnology, processing, physical chemistry, and analytics including lipidomics. A major focus of the journal is the synthesis of health related topics with applied aspects.
Following is a selection of subject areas which are of special interest to EJLST:
Animal and plant products for healthier foods including strategic feeding and transgenic crops
Authentication and analysis of foods for ensuring food quality and safety
Bioavailability of PUFA and other nutrients
Dietary lipids and minor compounds, their specific roles in food products and in nutrition
Food technology and processing for safer and healthier products
Functional foods and nutraceuticals
Lipidomics
Lipid structuring and formulations
Oleochemistry, lipid-derived polymers and biomaterials
Processes using lipid-modifying enzymes
The scope is not restricted to these areas. Submissions on topics at the interface of basic research and applications are strongly encouraged. The journal is the official organ the European Federation for the Science and Technology of Lipids (Euro Fed Lipid).