- Book学术

发布求助

文献互助智能选刊最新文献

IF 3.2 3区材料科学 Q2 ENGINEERING, CHEMICAL

International Journal of Adhesion and Adhesives Pub Date : 2025-03-09 DOI:10.1016/j.ijadhadh.2025.104003

Luiza Freitas Brum Souza , Kétlin Fagundes Teixeira , Ana Carolina Cadore-Rodrigues , Felipe Somavilla Binotto , Natália de Freitas Daudt , Luiz Felipe Valandro , Rafael R. Moraes , Mutlu Özcan , Gabriel Kalil Rocha Pereira

{"title":"Optimizing adhesion protocols between 3D-printed ceramic-containing composite and resin cement","authors":"Luiza Freitas Brum Souza , Kétlin Fagundes Teixeira , Ana Carolina Cadore-Rodrigues , Felipe Somavilla Binotto , Natália de Freitas Daudt , Luiz Felipe Valandro , Rafael R. Moraes , Mutlu Özcan , Gabriel Kalil Rocha Pereira","doi":"10.1016/j.ijadhadh.2025.104003","DOIUrl":null,"url":null,"abstract":"<div><div>This study evaluated the microshear bond strength (μSBS) of resin cement to a 3D-printed ceramic-containing resin composite (PriZma 3D Bio Crown, Makertech) subjected to different adhesive protocols (surface pretreatments and adhesive systems), in both baseline and aging conditions. For this, 3D-printed resin composite slices were fabricated and divided into groups based on adhesive protocols, considering three surface pretreatments: alumina grit-blasting (AlOx), 37 % phosphoric acid (PA), and a combination of both (AlOx + PA); and two adhesive systems: conventional (Adper Single Bond 2, 3M) and universal (Single Bond Universal, 3M). The resin cement (RelyX Ultimate, 3M) cylinder specimens (n = 18) underwent μSBS testing before and after thermocycling (12,000 cycles, 5-55 °C). Surface roughness (R<sub>a</sub> and R<sub>z</sub>), SEM topography, and failure modes were analyzed. Statistical analysis included One- and Two-Way ANOVA with Tukey tests for roughness and μSBS, respectively, and paired <em>t</em>-test to compare baseline and aging conditions considering the same adhesive protocol (α = 0.05). AlOx + PA with the universal adhesive demonstrated the highest bond strength in both baseline and aged conditions, with a minimal reduction after aging (11.68 %, p = 0.294). The PA-conventional adhesive group had the greatest reduction post-aging (50.32 %, p < 0.001). After aging, AlOx and PA with universal adhesive showed intermediate bond strengths, similar to AlOx + PA-universal, while the use of conventional adhesive resulted in lower bonding performance. In Baseline, AlOx + PA-universal exhibited the highest Weibull modulus, while AlOx + PA-conventional had the lowest. After aging, AlOx + PA-universal remained the highest, differing from the other groups but similar to AlOx + PA-conventional, whereas PA-universal had the lowest modulus. The other groups showed intermediate values without significant differences. The combination of alumina grit-blasting and phosphoric acid with a universal adhesive provides superior and more reliable bond strength under aging conditions.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"140 ","pages":"Article 104003"},"PeriodicalIF":3.2000,"publicationDate":"2025-03-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Adhesion and Adhesives","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0143749625000703","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"ENGINEERING, CHEMICAL","Score":null,"Total":0}

引用次数: 0

摘要

本研究评估了树脂水泥与三维打印含陶瓷树脂复合材料（PriZma 3D Bio Crown，Makertech）的微剪切粘接强度（μSBS），该复合材料在基线和老化条件下均采用了不同的粘接方案（表面预处理和粘接系统）。为此，我们制作了三维打印树脂复合片，并根据粘接方案将其分为几组，考虑了三种表面预处理方法：氧化铝喷砂（AlOx）、37% 磷酸（PA）和两种方法的组合（AlOx + PA）；以及两种粘接系统：传统粘接系统（Adper Single Bond 2，3M）和通用粘接系统（Single Bond Universal，3M）。树脂水泥（RelyX Ultimate，3M）圆柱体试样（n = 18）在热循环（12,000 个循环，5-55 °C）前后进行了 μSBS 测试。对表面粗糙度（Ra 和 Rz）、SEM 形貌和失效模式进行了分析。统计分析包括对粗糙度和 μSBS 分别进行单向和双向方差分析及 Tukey 检验，以及配对 t 检验来比较基线和老化条件（考虑到相同的粘合剂协议）（α = 0.05）。使用通用粘合剂的 AlOx + PA 组在基线和老化条件下均表现出最高的粘合强度，老化后的粘合强度降低幅度最小（11.68%，p = 0.294）。传统 PA 粘合剂组在老化后降低幅度最大（50.32%，p = 0.001）。老化后，AlOx 和 PA 与通用粘合剂显示出中等粘合强度，与 AlOx + PA- 通用粘合剂相似，而使用传统粘合剂则导致粘合性能降低。在基线中，AlOx + PA-universal 的 Weibull 模量最高，而 AlOx + PA-conventional 的最低。老化后，AlOx + PA-universal 仍然最高，与其他组不同，但与 AlOx + PA-conventional 相似，而 PA-universal 的模量最低。其他组的模量值介于两者之间，差异不大。氧化铝喷砂和磷酸与通用粘合剂的结合可在老化条件下提供更出色、更可靠的粘合强度。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

Optimizing adhesion protocols between 3D-printed ceramic-containing composite and resin cement

This study evaluated the microshear bond strength (μSBS) of resin cement to a 3D-printed ceramic-containing resin composite (PriZma 3D Bio Crown, Makertech) subjected to different adhesive protocols (surface pretreatments and adhesive systems), in both baseline and aging conditions. For this, 3D-printed resin composite slices were fabricated and divided into groups based on adhesive protocols, considering three surface pretreatments: alumina grit-blasting (AlOx), 37 % phosphoric acid (PA), and a combination of both (AlOx + PA); and two adhesive systems: conventional (Adper Single Bond 2, 3M) and universal (Single Bond Universal, 3M). The resin cement (RelyX Ultimate, 3M) cylinder specimens (n = 18) underwent μSBS testing before and after thermocycling (12,000 cycles, 5-55 °C). Surface roughness (R_a and R_z), SEM topography, and failure modes were analyzed. Statistical analysis included One- and Two-Way ANOVA with Tukey tests for roughness and μSBS, respectively, and paired t-test to compare baseline and aging conditions considering the same adhesive protocol (α = 0.05). AlOx + PA with the universal adhesive demonstrated the highest bond strength in both baseline and aged conditions, with a minimal reduction after aging (11.68 %, p = 0.294). The PA-conventional adhesive group had the greatest reduction post-aging (50.32 %, p < 0.001). After aging, AlOx and PA with universal adhesive showed intermediate bond strengths, similar to AlOx + PA-universal, while the use of conventional adhesive resulted in lower bonding performance. In Baseline, AlOx + PA-universal exhibited the highest Weibull modulus, while AlOx + PA-conventional had the lowest. After aging, AlOx + PA-universal remained the highest, differing from the other groups but similar to AlOx + PA-conventional, whereas PA-universal had the lowest modulus. The other groups showed intermediate values without significant differences. The combination of alumina grit-blasting and phosphoric acid with a universal adhesive provides superior and more reliable bond strength under aging conditions.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

International Journal of Adhesion and Adhesives 工程技术-材料科学：综合

CiteScore

6.90

自引率

8.80%

发文量

200

审稿时长

8.3 months

期刊介绍： The International Journal of Adhesion and Adhesives draws together the many aspects of the science and technology of adhesive materials, from fundamental research and development work to industrial applications. Subject areas covered include: interfacial interactions, surface chemistry, methods of testing, accumulation of test data on physical and mechanical properties, environmental effects, new adhesive materials, sealants, design of bonded joints, and manufacturing technology.