基于光流算法的集成微压痕测试评价聚合物粘弹性

IF 5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING
Giyeol Han , Yeongmin Yoon , Hyungyil Lee
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引用次数: 0

摘要

本研究旨在通过将微压痕测试与光流(of)算法和嵌入式膨胀中心(ECD)模型相结合,直接评估聚合物材料的粘弹性(蠕变)参数。压痕后,使用OF算法测量试样表面的平面内位移场随时间的变化,从而捕捉压痕印记的恢复行为。通过位移和空间分异得到蠕变应变随时间的演化曲线。采用ECD模型来估计压痕过程引起的初始残余应力,而无需进行复杂的逆分析。通过有限元分析验证了估算表面残余应力的可靠性。然后采用时间硬化模型推导蠕变应变-时间关系。利用初始残余应力和压痕蠕变应变曲线,确定了时间硬化蠕变参数。对聚甲基丙烯酸甲酯(PMMA)和聚碳酸酯(PC)的实验测试表明,与常规拉伸蠕变试验相比,所提出的方法产生的蠕变参数误差在5%左右。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Evaluation of polymer viscoelasticity by integrated micro-indentation test with optical flow algorithm
This study aims to directly evaluate the viscoelastic (creep) parameters of polymer materials by integrating a micro-indentation test with an optical flow (OF) algorithm and an embedded center of dilatation (ECD) model. After indentation, the in-plane displacement field on the specimen surface is measured over time using the OF algorithm, thereby capturing the recovery behavior of the indentation imprint. Subsequently, the creep strain evolution curve over time is obtained through displacement and spatial differentiation. The ECD model is employed to estimate the initial residual stress induced by indentation process without resorting to complex inverse analysis. The reliability of estimated surface residual stress was validated through FEA. A time hardening model is then used to derive the creep strain-time relationship. Using the initial residual stress and the creep strain curve obtained from indentation, the time hardening creep parameters are determined. The experimental tests on polymethyl methacrylate (PMMA) and polycarbonate (PC) have demonstrated that the proposed method yields creep parameters within an approximate 5% error margin relative to conventional tensile creep tests.
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来源期刊
Polymer Testing
Polymer Testing 工程技术-材料科学:表征与测试
CiteScore
10.70
自引率
5.90%
发文量
328
审稿时长
44 days
期刊介绍: Polymer Testing focuses on the testing, analysis and characterization of polymer materials, including both synthetic and natural or biobased polymers. Novel testing methods and the testing of novel polymeric materials in bulk, solution and dispersion is covered. In addition, we welcome the submission of the testing of polymeric materials for a wide range of applications and industrial products as well as nanoscale characterization. The scope includes but is not limited to the following main topics: Novel testing methods and Chemical analysis • mechanical, thermal, electrical, chemical, imaging, spectroscopy, scattering and rheology Physical properties and behaviour of novel polymer systems • nanoscale properties, morphology, transport properties Degradation and recycling of polymeric materials when combined with novel testing or characterization methods • degradation, biodegradation, ageing and fire retardancy Modelling and Simulation work will be only considered when it is linked to new or previously published experimental results.
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