溶胶-凝胶法合成的Sr(1−x)CuxO2纳米粒子的结构、介电和抗菌性能增强

IF 2.5 Q2 MULTIDISCIPLINARY SCIENCES
Ahmed S. Atlam, Abeer T. Talha, Talaat M. Meaz, Mohamed S. Hasanin, Amany M. El Nahrawy
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引用次数: 0

摘要

在这项研究中,我们研究了不同比例的氧化铜(CuO)(1、2、3和4 mol.%)掺杂的氧化锶(SrO)纳米颗粒的制备、表征和抗菌性能。SrO@CuO纳米颗粒是用溶胶-凝胶法合成的,这种方法以一种多功能和经济高效的方式生产高度均匀和纯净的纳米颗粒而闻名。研究了氧化铜对纳米颗粒生长及其抗菌和介电性能的影响。利用x射线衍射、透射电子显微镜、FTIR和介电光谱等技术分析了SrO@CuO纳米颗粒的形态、晶体学和电学性质。研究了纳米颗粒的介电性能,研究了界面极化、能量损失(tan ε)和0.1 Hz ~ 20 MHz范围内的电导率。Koop的双层模型被用来解释阻抗随频率的变化。模型表明,样品中含有定向良好的晶粒,这些晶粒被一些绝缘晶界分离开。随着频率的增加,阻抗减小,界面极化减小。当介电偶极子停止跟随施加的往复电场时,就会发生这种情况。同时观察了氧化铜纳米颗粒对铜绿假单胞菌、金黄色葡萄球菌和枯草芽孢杆菌的抑菌作用。样品具有抗菌效果。研究发现,CuO浓度显著影响CuO纳米颗粒的结构、光谱性质和抗菌效果。结果表明,SrO@CuO纳米颗粒适用于能量存储、记录介质、微波和抗菌剂。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Enhanced structural, dielectric, and antibacterial properties of Sr(1−x)CuxO2 nanoparticles synthesized via sol–gel method

In this study, we investigated the preparation, characterization, and antibacterial properties of strontium oxide (SrO) nanoparticles doped with different ratios of copper oxide (CuO) (1, 2, 3, and 4 mol.%). The SrO@CuO nanoparticles were synthesized using the sol–gel method, which is known for producing highly homogeneous and pure nanoparticles in a versatile and cost-effective manner. The study investigates the impact of CuO on the growth of the nanoparticles and their antibacterial and dielectric properties. Several techniques including X-ray diffraction, transmission electron microscopy, FTIR, and dielectric spectroscopy were used to analyze the morphological, crystallographic, and electric properties of the SrO@CuO nanoparticles. The dielectric properties of the nanoparticles were performed to study the polarization at the interface, energy loss (tan ε), and conductivity from 0.1 Hz to 20 MHz. Koop's two-layer model was suggested to explain the changes in impedance with frequency. The model suggests that the samples contain well-directing grains detached by some insulating grain boundary. As the frequency increases, the impedance decreases, and the interfacial polarization goes down. This happens when the dielectric dipoles stop following the applied reciprocating electric field. The antibacterial effects of CuO nanoparticles on Pseudomonas aeruginosa, Staphylococcus aureus, and Bacillus subtilis were also observed. The samples showed antibacterial efficacy. The study found that the concentration of CuO significantly affects the structure, spectroscopic properties, and antibacterial efficacy of the CuO nanoparticles. The results indicate that SrO@CuO nanoparticles are appropriate for energy storage, recording media, microwaves, and antimicrobial agents.

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来源期刊
CiteScore
2.60
自引率
0.00%
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0
期刊介绍: Beni-Suef University Journal of Basic and Applied Sciences (BJBAS) is a peer-reviewed, open-access journal. This journal welcomes submissions of original research, literature reviews, and editorials in its respected fields of fundamental science, applied science (with a particular focus on the fields of applied nanotechnology and biotechnology), medical sciences, pharmaceutical sciences, and engineering. The multidisciplinary aspects of the journal encourage global collaboration between researchers in multiple fields and provide cross-disciplinary dissemination of findings.
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