不同后处理温度对选择性激光熔化TiC-Ni金属陶瓷显微组织和力学性能的影响

IF 4.2 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Song Huang , Huachen Liu , Liangcai Du , Lichao Gong , Yunqi Xie , Qianqian Kong , Zhenhua Yao
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引用次数: 0

摘要

选择性激光熔化与后处理相结合是制造复杂形状陶瓷部件的常用方法。本研究利用slm制备的样品,采用真空烧结作为后处理技术,研究了不同后处理温度(1350°C, 1375°C, 1400°C, 1425°C, 1450°C)对TiC-35 wt% Ni金属陶瓷显微组织和力学性能的影响。结果表明,采用激光功率为240 W、扫描速度为300 mm/s的SLM打印参数,可获得成形良好的样品。随着烧结温度的升高,烧结机理逐渐由固相烧结过渡到液相烧结。相对密度、硬度、抗弯强度和断裂韧性均呈现先增大后减小的趋势。在1400℃时达到峰值:相对密度97.7%,HRA硬度82.7,抗弯强度901.8 MPa,断裂韧性8.72 MPa·m1/2。超过此温度,晶粒过度长大和脆性Ni3Ti相增加导致力学性能下降。真空烧结是一种很有前途的后处理技术,可以消除slm相关缺陷,提高机械性能。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effects of different post-processing temperatures on the microstructure and mechanical properties of TiC-Ni cermets fabricated by selective laser melting
Selective laser melting (SLM) combined with post-processing is a common method for fabricating complex-shaped cermets components. This study utilized SLM-fabricated samples and employed vacuum sintering as a post-processing technique to investigate the effects of different post-processing temperatures (1350 °C, 1375 °C, 1400 °C, 1425 °C, 1450 °C) on the microstructure and mechanical properties of TiC-35 wt% Ni cermets. The results showed that using SLM printing parameters of 240 W laser power and 300 mm/s scanning speed produced well-formed samples. As the sintering temperature increased, the sintering mechanism gradually transitioned from solid-phase sintering to liquid-phase sintering. Relative density, hardness, bending strength, and fracture toughness showed a trend of first increasing and then decreasing. At 1400 °C, peak values were achieved: 97.7 % relative density, 82.7 HRA hardness, 901.8 MPa bending strength, and 8.72 MPa·m1/2 fracture toughness. Beyond this temperature, excessive grain growth and an increase in the brittle Ni3Ti phase led to a decline in mechanical properties. Vacuum sintering could be a promising post-processing technique for eliminating SLM-related defects and enhancing mechanical properties.
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来源期刊
CiteScore
7.00
自引率
13.90%
发文量
236
审稿时长
35 days
期刊介绍: The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.
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