{"title":"New online beam intensity synchronous monitoring system in scanning transmission X-ray microscopy.","authors":"Yuchen Jiao, Xiangzhi Zhang, Zijian Xu, Zhen Yao, Tianxiao Sun, Yufei Zhang, Bo Zhao, Zhi Guo, Yong Wang, Xiangjun Zhen, Haigang Liu, Shasha Liang, Haitao Li, Xuanyu Zhao, Jian He, Renzhong Tai","doi":"10.1107/S1600577524012141","DOIUrl":null,"url":null,"abstract":"<p><p>The scanning transmission X-ray microscopy (STXM) platform based on synchrotron radiation has achieved nanoscale imaging with chemical sensitivity using spectro-microscopy techniques. However, the quality of STXM imaging is affected by the stability of the beam intensity. The top-up operation mode of synchrotrons to maintain a constant electron beam intensity introduces periodic fluctuations in the X-ray beam intensity, leading to notable imaging noise that decreases both contrast and precision. To address this issue, a high-speed real-time beam intensity monitoring system was designed and implemented at the BL08U1A beamline of the Shanghai Synchrotron Radiation Facility. This system utilizes an yttrium-aluminium-garnet crystal along with dual detectors having an acquisition frequency of up to 1 MHz and a synchronization error of less than 20 ns between them. This system can precisely and synchronously monitor the X-ray beam intensity variations which are used to remove noise due to electron injection from STXM images, thereby markedly improving the quality of STXM imaging.</p>","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"424-431"},"PeriodicalIF":2.5000,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11892909/pdf/","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Synchrotron Radiation","FirstCategoryId":"101","ListUrlMain":"https://doi.org/10.1107/S1600577524012141","RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2025/2/4 0:00:00","PubModel":"Epub","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
基于同步辐射的扫描透射 X 射线显微镜(STXM)平台利用光谱显微技术实现了具有化学灵敏度的纳米级成像。然而,STXM 的成像质量受到光束强度稳定性的影响。同步加速器为保持电子束强度恒定而采用的顶升运行模式会导致 X 射线束强度周期性波动,从而产生显著的成像噪声,降低对比度和精度。为解决这一问题,上海同步辐射装置 BL08U1A 光束线设计并实施了一套高速实时光束强度监测系统。该系统采用钇铝石榴石晶体和双探测器,采集频率高达 1 MHz,同步误差小于 20 ns。该系统可精确同步监测 X 射线束强度变化,用于消除 STXM 图像中因电子注入而产生的噪声,从而显著提高 STXM 图像的质量。
New online beam intensity synchronous monitoring system in scanning transmission X-ray microscopy.
The scanning transmission X-ray microscopy (STXM) platform based on synchrotron radiation has achieved nanoscale imaging with chemical sensitivity using spectro-microscopy techniques. However, the quality of STXM imaging is affected by the stability of the beam intensity. The top-up operation mode of synchrotrons to maintain a constant electron beam intensity introduces periodic fluctuations in the X-ray beam intensity, leading to notable imaging noise that decreases both contrast and precision. To address this issue, a high-speed real-time beam intensity monitoring system was designed and implemented at the BL08U1A beamline of the Shanghai Synchrotron Radiation Facility. This system utilizes an yttrium-aluminium-garnet crystal along with dual detectors having an acquisition frequency of up to 1 MHz and a synchronization error of less than 20 ns between them. This system can precisely and synchronously monitor the X-ray beam intensity variations which are used to remove noise due to electron injection from STXM images, thereby markedly improving the quality of STXM imaging.
期刊介绍:
Synchrotron radiation research is rapidly expanding with many new sources of radiation being created globally. Synchrotron radiation plays a leading role in pure science and in emerging technologies. The Journal of Synchrotron Radiation provides comprehensive coverage of the entire field of synchrotron radiation and free-electron laser research including instrumentation, theory, computing and scientific applications in areas such as biology, nanoscience and materials science. Rapid publication ensures an up-to-date information resource for scientists and engineers in the field.