用于油相有机液体溶剂检测的高灵敏度实时微波传感器

Bushra Kamal , Amirhossein Yazdanicherati , Mabkhot S. BinDahbag , Zahra Abbasi , Hassan Hassanzadeh
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引用次数: 0

摘要

准确测定油相中有机溶剂的浓度对于各种工业应用至关重要,包括提高石油采收率。常用的检测方法,如色谱法和基于蒸馏的方法,受到样品处理引起的溶剂损失的影响。在溶剂辅助采油过程中,缺乏检测采出流体中溶剂的标准方法。我们提出了一种利用平面微波传感器监测溶剂的新方法。所提出的传感器由使用电磁耦合无线通信的无芯片标签-读取器对组成。该传感器对不同溶剂浓度下介电常数的变化有很高的灵敏度响应,这反映在共振频谱中。为了最大限度地提高传感器的重复性响应,将传感器集成到一个塑料容器中,形成一个传感探头,可以作为现场在线仪器使用。实验用正戊烷、正己烷、正庚烷和乙酸乙酯四种溶剂进行。结果表明,当溶剂浓度从0 wt%变化到20 wt%时,被测溶剂的共振峰频移分别变化2.71、2.01、1.66和2.10 MHz,表明对油相溶剂测量具有优异的实时监测能力。提出的方法为应用平面微波传感器检测工业过程中的有机溶剂提供了潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Highly sensitive real-time microwave sensor for detection of organic liquid solvents in an oleic phase
Accurately determining the concentration of organic solvents in an oleic phase is essential for various industrial applications, including enhanced oil recovery. Popular detection methods, like chromatographic and distillation-based approaches, suffer from sample processing-induced solvent loss. There is a lack of standard methods for detecting solvents in produced fluid streams during solvent-aided oil recovery. We propose a novel sensing approach for solvent monitoring using planar microwave sensors. The proposed sensor consists of a chipless tag-reader pair communicating wirelessly using electromagnetic coupling. The sensor has a high sensitivity response to variations in permittivity at various solvent concentrations, which is reflected in the resonance-frequency spectrum. To maximize repeatability response of sensor, the sensor is integrated into a plastic container to form a sensing probe that can be used as an on-site in-line instrument. The experiments were conducted using four solvents, including n-pentane, n-hexane, n-heptane, and ethyl acetate. The results demonstrated that when solvent concentration changes from zero to 20 wt%, the frequency shift of resonance peak changes by 2.71, 2.01, 1.66, and 2.10 MHz for the examined solvents, respectively, indicating an exceptional capability of real-time monitoring for measuring solvents in oleic phase. The proposed approach offers the potential for applying planar microwave sensors to detect organic solvents in industrial processes.
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