用3-甲基- 1h -吡唑-4(5H)- 1、芳基苯基腙和芳基乙二醛三组分反应高效合成了一些新的联吡唑衍生物

IF 1.8 3区化学 Q3 CHEMISTRY, ORGANIC

Synthetic Communications Pub Date : 2025-01-17 DOI:10.1080/00397911.2024.2431990

Maryam Oudi , Mohammad Anary-Abbasinejad

{"title":"用3-甲基- 1h -吡唑-4(5H)- 1、芳基苯基腙和芳基乙二醛三组分反应高效合成了一些新的联吡唑衍生物","authors":"Maryam Oudi , Mohammad Anary-Abbasinejad","doi":"10.1080/00397911.2024.2431990","DOIUrl":null,"url":null,"abstract":"<div><div>A simple one-pot and catalyst-free method is reported for synthesis of some new bipyrazole derivatives by three-component reaction between arylglyoxals, 3-methyl-1<em>H</em>-pyrazol-4(5<em>H</em>)-one and aroylphenylhydrazone derivatives. The reactions were carried out in ethanol as a green solvent in neutral reaction conditions and products were simply isolated by filtering of the precipitated solids in high yields. All products were characterized by their <sup>1</sup>H and <sup>13</sup>C NMR and IR spectral and elemental analysis data.</div></div>","PeriodicalId":22119,"journal":{"name":"Synthetic Communications","volume":"55 2","pages":"Pages 146-151"},"PeriodicalIF":1.8000,"publicationDate":"2025-01-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"An efficient synthesis of some new bipyrazole derivatives by three-component reaction between 3-methyl-1H-pyrazol-4(5H)-one, aroylphenylhydrazones and arylglyoxals\",\"authors\":\"Maryam Oudi , Mohammad Anary-Abbasinejad\",\"doi\":\"10.1080/00397911.2024.2431990\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>A simple one-pot and catalyst-free method is reported for synthesis of some new bipyrazole derivatives by three-component reaction between arylglyoxals, 3-methyl-1<em>H</em>-pyrazol-4(5<em>H</em>)-one and aroylphenylhydrazone derivatives. The reactions were carried out in ethanol as a green solvent in neutral reaction conditions and products were simply isolated by filtering of the precipitated solids in high yields. All products were characterized by their <sup>1</sup>H and <sup>13</sup>C NMR and IR spectral and elemental analysis data.</div></div>\",\"PeriodicalId\":22119,\"journal\":{\"name\":\"Synthetic Communications\",\"volume\":\"55 2\",\"pages\":\"Pages 146-151\"},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2025-01-17\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Synthetic Communications\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://www.sciencedirect.com/org/science/article/pii/S0039791124001413\",\"RegionNum\":3,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Synthetic Communications","FirstCategoryId":"92","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S0039791124001413","RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}

引用次数: 0

摘要

本文报道了芳基乙二醛、3-甲基- 1h -吡唑-4(5H)- 1和芳基苯基腙衍生物三组分反应合成新的双吡唑衍生物的一锅无催化剂简易方法。该反应以乙醇为绿色溶剂，在中性条件下进行，产物只需过滤沉淀固体即可得到，收率高。所有产物均通过1H、13C NMR、IR光谱及元素分析数据进行了表征。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

An efficient synthesis of some new bipyrazole derivatives by three-component reaction between 3-methyl-1H-pyrazol-4(5H)-one, aroylphenylhydrazones and arylglyoxals

A simple one-pot and catalyst-free method is reported for synthesis of some new bipyrazole derivatives by three-component reaction between arylglyoxals, 3-methyl-1H-pyrazol-4(5H)-one and aroylphenylhydrazone derivatives. The reactions were carried out in ethanol as a green solvent in neutral reaction conditions and products were simply isolated by filtering of the precipitated solids in high yields. All products were characterized by their ¹H and ¹³C NMR and IR spectral and elemental analysis data.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Synthetic Communications 化学-有机化学

CiteScore

4.40

自引率

4.80%

发文量

156

审稿时长

4.3 months

期刊介绍： Synthetic Communications presents communications describing new methods, reagents, and other synthetic work pertaining to organic chemistry with sufficient experimental detail to permit reported reactions to be repeated by a chemist reasonably skilled in the art. In addition, the Journal features short, focused review articles discussing topics within its remit of synthetic organic chemistry.