{"title":"喷射成形Al-Zn-Mg-Cu合金热挤压及固溶过程中组织演变的研究","authors":"Zhiwu Zhang , Ruxue Liu , Yihui Zhou , Guowei Zhou , Dayong Li , Zhen Zhao , Yinghong Peng , Dongnan Huang","doi":"10.1016/j.jallcom.2024.178387","DOIUrl":null,"url":null,"abstract":"<div><div>The microstructural evolution of spray formed Al-Zn-Mg-Cu alloy was investigated during the hot extrusion with the extrusion speed of 5–70 mm/min at 400 ℃ and 450 ℃. Then, the extruded rods at different deformation conditions were subjected to solution treatment for 2 h at 350 ℃ and 2 h at 475 ℃. The influence of temperature and extrusion speed on the recrystallization mechanism and abnormal grain growth (AGG) has been unveiled. The results show that continuous dynamic recrystallization (CDRX) is the primary dynamic recrystallization (DRX) mechanism at the surface of the extrusion rod, and the main texture components were Brass {110} < 112 > . The center region is primarily characterized by a fiber texture (<100 > and <111 ><em>//</em>ED) and a limited number of fine recrystallized grains, formed through geometric dynamic recrystallization (GDRX), are observed at the grain boundaries. Furthermore, a fine-grained layer has been discovered on the extrusion rod surface and the thickness is primarily influenced by the deformation temperature. As the deformation temperature and extrusion speed increase, the dissolution of second phase particles leads to a reduction in pinning resistance, resulting in ACG at the outermost layer of the extruded rod and gradually developing into the peripheral coarse grain (PCG). In addition, the mechanism of PCG formation is primarily influenced by the history of local deformation. Considering the thermal-mechanical process and the pinning effect of the spray formed material, the optimal extrusion parameters are recommended to be at 450 ℃ with an extrusion speed of 10 mm/min.</div></div>","PeriodicalId":344,"journal":{"name":"Journal of Alloys and Compounds","volume":"1014 ","pages":"Article 178387"},"PeriodicalIF":6.3000,"publicationDate":"2025-02-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Investigation on microstructural evolution of spray formed Al-Zn-Mg-Cu alloy during hot extrusion processes and subsequent solution treatment\",\"authors\":\"Zhiwu Zhang , Ruxue Liu , Yihui Zhou , Guowei Zhou , Dayong Li , Zhen Zhao , Yinghong Peng , Dongnan Huang\",\"doi\":\"10.1016/j.jallcom.2024.178387\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The microstructural evolution of spray formed Al-Zn-Mg-Cu alloy was investigated during the hot extrusion with the extrusion speed of 5–70 mm/min at 400 ℃ and 450 ℃. Then, the extruded rods at different deformation conditions were subjected to solution treatment for 2 h at 350 ℃ and 2 h at 475 ℃. The influence of temperature and extrusion speed on the recrystallization mechanism and abnormal grain growth (AGG) has been unveiled. The results show that continuous dynamic recrystallization (CDRX) is the primary dynamic recrystallization (DRX) mechanism at the surface of the extrusion rod, and the main texture components were Brass {110} < 112 > . The center region is primarily characterized by a fiber texture (<100 > and <111 ><em>//</em>ED) and a limited number of fine recrystallized grains, formed through geometric dynamic recrystallization (GDRX), are observed at the grain boundaries. Furthermore, a fine-grained layer has been discovered on the extrusion rod surface and the thickness is primarily influenced by the deformation temperature. As the deformation temperature and extrusion speed increase, the dissolution of second phase particles leads to a reduction in pinning resistance, resulting in ACG at the outermost layer of the extruded rod and gradually developing into the peripheral coarse grain (PCG). In addition, the mechanism of PCG formation is primarily influenced by the history of local deformation. Considering the thermal-mechanical process and the pinning effect of the spray formed material, the optimal extrusion parameters are recommended to be at 450 ℃ with an extrusion speed of 10 mm/min.</div></div>\",\"PeriodicalId\":344,\"journal\":{\"name\":\"Journal of Alloys and Compounds\",\"volume\":\"1014 \",\"pages\":\"Article 178387\"},\"PeriodicalIF\":6.3000,\"publicationDate\":\"2025-02-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Alloys and Compounds\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0925838824049752\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, PHYSICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Alloys and Compounds","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0925838824049752","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}
Investigation on microstructural evolution of spray formed Al-Zn-Mg-Cu alloy during hot extrusion processes and subsequent solution treatment
The microstructural evolution of spray formed Al-Zn-Mg-Cu alloy was investigated during the hot extrusion with the extrusion speed of 5–70 mm/min at 400 ℃ and 450 ℃. Then, the extruded rods at different deformation conditions were subjected to solution treatment for 2 h at 350 ℃ and 2 h at 475 ℃. The influence of temperature and extrusion speed on the recrystallization mechanism and abnormal grain growth (AGG) has been unveiled. The results show that continuous dynamic recrystallization (CDRX) is the primary dynamic recrystallization (DRX) mechanism at the surface of the extrusion rod, and the main texture components were Brass {110} < 112 > . The center region is primarily characterized by a fiber texture (<100 > and <111 >//ED) and a limited number of fine recrystallized grains, formed through geometric dynamic recrystallization (GDRX), are observed at the grain boundaries. Furthermore, a fine-grained layer has been discovered on the extrusion rod surface and the thickness is primarily influenced by the deformation temperature. As the deformation temperature and extrusion speed increase, the dissolution of second phase particles leads to a reduction in pinning resistance, resulting in ACG at the outermost layer of the extruded rod and gradually developing into the peripheral coarse grain (PCG). In addition, the mechanism of PCG formation is primarily influenced by the history of local deformation. Considering the thermal-mechanical process and the pinning effect of the spray formed material, the optimal extrusion parameters are recommended to be at 450 ℃ with an extrusion speed of 10 mm/min.
期刊介绍:
The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.