一种半透明氧化锆的光学性质和颜色稳定性:研磨后精加工的影响。

Brazilian dental journal Pub Date : 2024-12-16 eCollection Date: 2024-01-01 DOI:10.1590/0103-6440202406094
Pablo Machado Soares, Camila Pauleski Zucuni, Bruna Dias Ilha, Leticia Borges Jacques, Liliana Gressler May, Luiz Felipe Valandro
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引用次数: 0

摘要

本研究评估了研磨和抛光处理(抛光或上釉)对浸泡在红酒中的半透明氧化锆(3Y-TZP)的颜色稳定性、半透明性和乳白色的影响。圆盘(Ø= 12 mm;厚度0.8 mm)的3Y-TZP (Zenostar T, Ivoclar AG)根据表面处理因子随机分配(n= 8): Ctrl - as-烧结;用4219号金刚石钎头磨削;Gr + Pol先磨后抛光;Gr + Gl -研磨后上釉。表面粗糙度和扫描电镜分析。所有标本在18天内每天浸泡在红酒中30分钟。在浸泡9天和18天后,通过CIEDE2000公式测量色差(ΔE00),与半透明(TP00)和乳光(OP)参数相同。采用Kruskal Wallis、重复测量ANOVA/Tukey和Spearman相关检验分别评价粗糙度、光学和相关数据。Gr + Gl在9天后的ΔE00值最低。Gr组在所有浸泡时间中ΔE00值最高,而其他组在18天后表现出相似的行为。Gr和Gr + Pol组的Ra和Rz值最高。粗糙度与颜色变化呈中度显著相关(p= 0.02, r= 0.42)。TP00和op的表面处理影响了氧化锆的粗糙度和颜色稳定性,使釉面应用更有效地减少浸渍后的颜色变化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Optical properties and color stability of a translucent zirconia: effects of finishing after grinding.

This study evaluated the effect of grinding and finishing treatments (polishing or glaze) on the color stability, translucency and opalescence of a translucent zirconia (3Y-TZP) after immersion in red wine. Discs (Ø= 12 mm; thickness 0.8 mm) of 3Y-TZP (Zenostar T, Ivoclar AG) were randomly allocated (n= 8) according to the surface treatment factor: Ctrl - as-sintered; Gr - grinding with diamond bur #4219; Gr + Pol - grinding followed by polishing; Gr + Gl - grinding followed by glaze. Surface roughness and scanning electron microscopy were carried out. All specimens were subjected to daily immersions in red wine for 30 minutes during 18 days. The color differences (ΔE00) were measured prior, after 9 and 18 days of immersion through the CIEDE2000 formula, as same as translucency (TP00) and opalescence (OP) parameters. Kruskal Wallis, repeated measures ANOVA/Tukey, and Spearman's correlation tests were performed to evaluate the roughness, optical and correlation data, respectively. The Gr + Gl depicted the lowest ΔE00 value after 9 days. The Gr group showed the greatest ΔE00 values in all immersion times, whereas the other groups presented similar behavior after 18 days. The Gr and Gr + Pol groups had the highest Ra and Rz values. The correlation between roughness and color change was moderate and significant (p= 0.02, r= 0.42). No differences were observed for TP00 and OP. The surface treatments affected the roughness and color stability of zirconia, being glaze application more effective to reduce color alterations after the immersion protocol.

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