IF 3.3 2区 化学 Q1 CHEMISTRY, ORGANIC
Allan F. C. Rossini, Ana Carolina A. Muraca, Gleison A. Casagrande, Cristiano Raminelli
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引用次数: 0

摘要

对于 1,2,11-三甲氧基-6-甲基-5,6,6a,7-四氢-4H-二苯并[de,g]喹啉 (5),应考虑以下提供的正确 1H 和 13C NMR 数据,而不是原始论文中提供的数据。此外,对于化合物 5,应考虑修订版 "辅助信息 "中提供的正确 1H NMR 光谱,而不是原始 "辅助信息 "中提供的光谱。1H NMR(300 MHz,CDCl3)δ 7.19-7.13(m,1H),6.85-6.81(m,2H),6.57(s,1H),3.81(s,3H),3.80(s,3H),3.53(s,3H),3.05-2.94(m,3H),2.87(d,J = 13.4 Hz,1H),2.60(dd,J = 16.2,3.6Hz,1H),2.47(s,3H),2.44-2.35(m,2H);13C NMR(75 MHz,CDCl3)δ 156.7,151.7,145.5,138.8,128.6,128.2,127.2,124.3,121.2,119.7,110.9,110.0,62.9,60.8,55.8,55.6,52.9,43.7,35.8,28.5。辅助信息可在 https://pubs.acs.org/doi/10.1021/acs.joc.4c02931 免费获取。核磁共振光谱和单晶 X 射线衍射数据副本(PDF 大多数电子版 "支持信息 "文件无需订阅 ACS Web Editions 即可获得。此类文件可按文章下载,供研究使用(如果相关文章链接了公共使用许可,则该许可可能允许其他用途)。如需其他用途,可通过 RightsLink 许可系统 http://pubs.acs.org/page/copyright/permissions.html 向 ACS 申请许可。本文尚未被其他出版物引用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Correction to “Total Syntheses of Aporphine Alkaloids via Benzyne Chemistry: An Approach to the Formation of Aporphine Cores”
For 1,2,11-trimethoxy-6-methyl-5,6,6a,7-tetrahydro-4H-dibenzo[de,g]quinoline (5), the correct 1H and 13C NMR data presented below should be considered instead of those presented in the original paper. In addition, for compound 5, the correct 1H NMR spectrum presented in the revised Supporting Information should be considered instead of that presented in the original Supporting Information. 1H NMR (300 MHz, CDCl3) δ 7.19–7.13 (m, 1H), 6.85–6.81 (m, 2H), 6.57 (s, 1H), 3.81 (s, 3H), 3.80 (s, 3H), 3.53 (s, 3H), 3.05–2.94 (m, 3H), 2.87 (d, J = 13.4 Hz, 1H), 2.60 (dd, J = 16.2, 3.6 Hz, 1H), 2.47 (s, 3H), 2.44–2.35 (m, 2H); 13C NMR (75 MHz, CDCl3) δ 156.7, 151.7, 145.5, 138.8, 128.6, 128.2, 127.2, 124.3, 121.2, 119.7, 110.9, 110.0, 62.9, 60.8, 55.8, 55.6, 52.9, 43.7, 35.8, 28.5. The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acs.joc.4c02931. Copies of NMR spectra and single-crystal X-ray diffraction data (PDF) Most electronic Supporting Information files are available without a subscription to ACS Web Editions. Such files may be downloaded by article for research use (if there is a public use license linked to the relevant article, that license may permit other uses). Permission may be obtained from ACS for other uses through requests via the RightsLink permission system: http://pubs.acs.org/page/copyright/permissions.html. This article has not yet been cited by other publications.
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来源期刊
Journal of Organic Chemistry
Journal of Organic Chemistry 化学-有机化学
CiteScore
6.20
自引率
11.10%
发文量
1467
审稿时长
2 months
期刊介绍: Journal of Organic Chemistry welcomes original contributions of fundamental research in all branches of the theory and practice of organic chemistry. In selecting manuscripts for publication, the editors place emphasis on the quality and novelty of the work, as well as the breadth of interest to the organic chemistry community.
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