用姜黄素-羟基磷灰石纳米粒子注入粘合剂,用Nd: YAG和Er: Cr, YSGG激光预处理正畸支架牙釉质:FTIR、SEM和背散射电子成像评价。

IF 2 3区 工程技术 Q2 ANATOMY & MORPHOLOGY
Muhammad Abdullah Kamran, Salem Almoammar
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引用次数: 0

摘要

评价1 wt % cu - hnps正畸粘接剂对牙托与牙釉质表面粘接的SBS、DC和流变学评价;Nd: YAG和Er: Cr, YSGG激光器。制备了两种胶粘剂:实验胶粘剂(EA)和负载1 wt % cu - hnp的EA。利用扫描电镜和能谱仪对负载电流的HNP进行了表面表征。采用PA-gel、Er、Cr:YSGG激光、Nd: YAG激光三种不同策略制备和调理标本。将预处理托架粘接后,对样品进行人工老化,并通过BSE在扫描电镜下对每个釉质预处理方案的两个样品进行评估。SBS测试通过UTM完成,然后使用ARI进行故障分析。用FTIR对改性和未改性的胶粘剂进行直流试验,并进行流变学评价。SBS和DC采用方差分析和事后多重比较检验进行评估。SBS在PA处理的牙釉质表面最高。Nd: YAG激光处理的牙釉质表面SBS最低。ARI结果表明,含cu - hnp改性胶粘剂的失效次数最高,失效次数在1 ~ 2之间。两种胶粘剂在DC方面无显著差异。用1% curr - hnp改性的粘合剂粘度增加,流动性降低。使用Er,Cr:YSGG激光在支架放置前进行牙釉质预处理显示出替代传统酸蚀刻的潜力,特别是当与含有cu - hnps的实验性正畸粘合剂结合使用时。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Orthodontic Bracket to Enamel Pretreated With Nd: YAG and Er: Cr, YSGG Lasers Using Curcumin-Hydroxyapatite Nanoparticles Infused Adhesive: A FTIR, SEM Evaluation via Backscattered Electron Imaging.

To evaluate the SBS, DC, and rheological valuation of experimental 1 wt % Cur-loaded-HNPs orthodontic adhesive to bond bracket to enamel surface treated with PA; Nd: YAG, and Er: Cr, YSGG lasers. Two adhesives were prepared experimental adhesive (EA) and EA loaded with 1-wt % Cur-HNP. Surface characterization of Cur-loaded HNP was performed under SEM along with EDS. Specimens were prepared and conditioned with three different strategies PA-gel, Er,Cr:YSGG laser, Nd: YAG laser. Following pretreatment brackets were bonded, samples underwent artificial aging and two samples from each enamel pretreatment regime were assessed under SEM via BSE. SBS testing was achieved via UTM followed by failure analysis using ARI. Modified and unmodified adhesives underwent DC using FTIR and rheological valuation was performed. SBS and DC were assessed using ANOVA and post hoc multiple comparison tests. The highest SBS was seen in the enamel surface treated with PA. The lowest SBS was remarked in the enamel surface treated with Nd: YAG laser. Based on ARI it was noted that modified adhesive containing Cur-HNP exhibited the highest number of failures between 1 and 2. No significant difference was observed between both adhesives in terms of DC. Adhesive modified with 1% Cur-HNP increased viscosity with a decrease in fluidity. The use of Er,Cr:YSGG laser for enamel pretreatment before bracket placement showed potential as a substitute for conventional acid etching, especially when combined with an experimental orthodontic adhesive containing Cur-HNPs.

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来源期刊
Microscopy Research and Technique
Microscopy Research and Technique 医学-解剖学与形态学
CiteScore
5.30
自引率
20.00%
发文量
233
审稿时长
4.7 months
期刊介绍: Microscopy Research and Technique (MRT) publishes articles on all aspects of advanced microscopy original architecture and methodologies with applications in the biological, clinical, chemical, and materials sciences. Original basic and applied research as well as technical papers dealing with the various subsets of microscopy are encouraged. MRT is the right form for those developing new microscopy methods or using the microscope to answer key questions in basic and applied research.
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