{"title":"粉末混合对压缩成型法制备的聚酰胺 6-AZ61 镁复合材料机械强度的影响","authors":"Song-Jeng Huang , Yopi Yusuf Tanoto , Chuan Li","doi":"10.1016/j.coco.2024.102169","DOIUrl":null,"url":null,"abstract":"<div><div>A composite material of polyamide 6 and AZ61 magnesium alloy was produced by hot press molding. Both matrix and reinforcement powders were thoroughly mixed by ball milling and then hot pressed to forge a bulk material. Four process parameters of the mixing process including milling time, milling speed, ball-to-powder weight ratio, and the AZ61 wt percentage at various levels were investigated for their influences on the mechanical strength of the composites. Material characterization includes XRD, scanning electron microscopy, uniaxial tensile test, and Vickers hardness. An experimental design using Taguchi (L9 (3,4)) and an analysis of variance indicate that the AZ61 wt percentage is the most influential factor in the ultimate strength of the PA6-AZ61 composite. Adding 5 wt% reinforcement powders to PA6 and milled at 300 rpm for 30 min can increase the average ultimate tensile strength of composites to 63.83 MPa with a maximum strain of 7.71 %, and Vickers hardness of 21.97 HV. As compared to those in the pure PA6 matrix (58.83 MPa 2.29 %, and 13.01 HV), this enhancement in ductility is achieved by the well-dispersed AZ61 particles in the PA6 matrix.</div></div>","PeriodicalId":10533,"journal":{"name":"Composites Communications","volume":"53 ","pages":"Article 102169"},"PeriodicalIF":6.5000,"publicationDate":"2024-11-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of powder mixing on the mechanical strength of polyamide 6-AZ61 magnesium composites prepared by compression molding\",\"authors\":\"Song-Jeng Huang , Yopi Yusuf Tanoto , Chuan Li\",\"doi\":\"10.1016/j.coco.2024.102169\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>A composite material of polyamide 6 and AZ61 magnesium alloy was produced by hot press molding. Both matrix and reinforcement powders were thoroughly mixed by ball milling and then hot pressed to forge a bulk material. Four process parameters of the mixing process including milling time, milling speed, ball-to-powder weight ratio, and the AZ61 wt percentage at various levels were investigated for their influences on the mechanical strength of the composites. Material characterization includes XRD, scanning electron microscopy, uniaxial tensile test, and Vickers hardness. An experimental design using Taguchi (L9 (3,4)) and an analysis of variance indicate that the AZ61 wt percentage is the most influential factor in the ultimate strength of the PA6-AZ61 composite. Adding 5 wt% reinforcement powders to PA6 and milled at 300 rpm for 30 min can increase the average ultimate tensile strength of composites to 63.83 MPa with a maximum strain of 7.71 %, and Vickers hardness of 21.97 HV. As compared to those in the pure PA6 matrix (58.83 MPa 2.29 %, and 13.01 HV), this enhancement in ductility is achieved by the well-dispersed AZ61 particles in the PA6 matrix.</div></div>\",\"PeriodicalId\":10533,\"journal\":{\"name\":\"Composites Communications\",\"volume\":\"53 \",\"pages\":\"Article 102169\"},\"PeriodicalIF\":6.5000,\"publicationDate\":\"2024-11-17\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Composites Communications\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2452213924003607\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, COMPOSITES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Communications","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2452213924003607","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, COMPOSITES","Score":null,"Total":0}
Effect of powder mixing on the mechanical strength of polyamide 6-AZ61 magnesium composites prepared by compression molding
A composite material of polyamide 6 and AZ61 magnesium alloy was produced by hot press molding. Both matrix and reinforcement powders were thoroughly mixed by ball milling and then hot pressed to forge a bulk material. Four process parameters of the mixing process including milling time, milling speed, ball-to-powder weight ratio, and the AZ61 wt percentage at various levels were investigated for their influences on the mechanical strength of the composites. Material characterization includes XRD, scanning electron microscopy, uniaxial tensile test, and Vickers hardness. An experimental design using Taguchi (L9 (3,4)) and an analysis of variance indicate that the AZ61 wt percentage is the most influential factor in the ultimate strength of the PA6-AZ61 composite. Adding 5 wt% reinforcement powders to PA6 and milled at 300 rpm for 30 min can increase the average ultimate tensile strength of composites to 63.83 MPa with a maximum strain of 7.71 %, and Vickers hardness of 21.97 HV. As compared to those in the pure PA6 matrix (58.83 MPa 2.29 %, and 13.01 HV), this enhancement in ductility is achieved by the well-dispersed AZ61 particles in the PA6 matrix.
期刊介绍:
Composites Communications (Compos. Commun.) is a peer-reviewed journal publishing short communications and letters on the latest advances in composites science and technology. With a rapid review and publication process, its goal is to disseminate new knowledge promptly within the composites community. The journal welcomes manuscripts presenting creative concepts and new findings in design, state-of-the-art approaches in processing, synthesis, characterization, and mechanics modeling. In addition to traditional fiber-/particulate-reinforced engineering composites, it encourages submissions on composites with exceptional physical, mechanical, and fracture properties, as well as those with unique functions and significant application potential. This includes biomimetic and bio-inspired composites for biomedical applications, functional nano-composites for thermal management and energy applications, and composites designed for extreme service environments.