锻造纯钽中的变形行为和微结构演变研究

IF 4.2 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Zhong Jiahao , Jia Zhiqiang , Zhang Long , Zhu Yanchun , Wu Hao
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引用次数: 0

摘要

本研究使用 Gleeble-3800 热模拟试验机研究了锻造纯钽的变形特性,试验温度范围为室温至 350 °C,应变速率范围为 0.1 至 10 s-1,最大变形量为 60 %。结果表明,在达到峰值应力之前,变形抗力随着变形温度的降低和应变速率的增加而增加。达到峰值应力后,变形由动态恢复机制主导。根据实验得到的真实应力-应变曲线,计算出该材料的变形活化能(Q)和应力指数(n)分别为 5.133 kJ/mol 和 3.1989。建立了描述流变行为的构成方程。利用加工图结合变形后的微观结构,确定了最佳加工参数为室温变形温度、3.5 至 10 s-1 的应变速率和 0.12 的耗散率。在这些最佳加工参数下,材料的微观结构主要由动态再结晶晶粒和变形晶粒组成。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The study of deformation behavior and microstructure evolution in forged pure tantalum
In this study, the deformation characteristics of as-forged pure tantalum were investigated using a Gleeble-3800 thermal simulation testing machine in the temperature range of room temperature to 350 °C and strain rates ranging from 0.1 to 10 s−1, with a maximum deformation of 60 %. Results show that the deformation resistance increases with decreasing deformation temperature and increasing strain rate before reaching the peak stress. After reaching peak stress, deformation is dominated by dynamic recovery mechanisms. Based on the true stress-strain curves obtained from experiments, the deformation activation energy (Q) and stress exponent (n) of the material were calculated to be 5.133 kJ/mol and 3.1989, respectively. A constitutive equation describing the rheological behavior was established. Utilizing processing maps combined with post-deformation microstructures, optimal processing parameters were determined to be a deformation temperature of room temperature, a strain rate ranging from 3.5 to 10 s−1, and a dissipation rate of 0.12. Under these optimal processing parameters, the material microstructure mainly consisted of dynamically recrystallized grains and deformed grains.
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来源期刊
CiteScore
7.00
自引率
13.90%
发文量
236
审稿时长
35 days
期刊介绍: The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.
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