{"title":"锻造纯钽中的变形行为和微结构演变研究","authors":"Zhong Jiahao , Jia Zhiqiang , Zhang Long , Zhu Yanchun , Wu Hao","doi":"10.1016/j.ijrmhm.2024.106965","DOIUrl":null,"url":null,"abstract":"<div><div>In this study, the deformation characteristics of as-forged pure tantalum were investigated using a Gleeble-3800 thermal simulation testing machine in the temperature range of room temperature to 350 °C and strain rates ranging from 0.1 to 10 s<sup>−1</sup>, with a maximum deformation of 60 %. Results show that the deformation resistance increases with decreasing deformation temperature and increasing strain rate before reaching the peak stress. After reaching peak stress, deformation is dominated by dynamic recovery mechanisms. Based on the true stress-strain curves obtained from experiments, the deformation activation energy (Q) and stress exponent (n) of the material were calculated to be 5.133 kJ/mol and 3.1989, respectively. A constitutive equation describing the rheological behavior was established. Utilizing processing maps combined with post-deformation microstructures, optimal processing parameters were determined to be a deformation temperature of room temperature, a strain rate ranging from 3.5 to 10 s<sup>−1</sup>, and a dissipation rate of 0.12. Under these optimal processing parameters, the material microstructure mainly consisted of dynamically recrystallized grains and deformed grains.</div></div>","PeriodicalId":14216,"journal":{"name":"International Journal of Refractory Metals & Hard Materials","volume":"127 ","pages":"Article 106965"},"PeriodicalIF":4.2000,"publicationDate":"2024-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"The study of deformation behavior and microstructure evolution in forged pure tantalum\",\"authors\":\"Zhong Jiahao , Jia Zhiqiang , Zhang Long , Zhu Yanchun , Wu Hao\",\"doi\":\"10.1016/j.ijrmhm.2024.106965\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>In this study, the deformation characteristics of as-forged pure tantalum were investigated using a Gleeble-3800 thermal simulation testing machine in the temperature range of room temperature to 350 °C and strain rates ranging from 0.1 to 10 s<sup>−1</sup>, with a maximum deformation of 60 %. Results show that the deformation resistance increases with decreasing deformation temperature and increasing strain rate before reaching the peak stress. After reaching peak stress, deformation is dominated by dynamic recovery mechanisms. Based on the true stress-strain curves obtained from experiments, the deformation activation energy (Q) and stress exponent (n) of the material were calculated to be 5.133 kJ/mol and 3.1989, respectively. A constitutive equation describing the rheological behavior was established. Utilizing processing maps combined with post-deformation microstructures, optimal processing parameters were determined to be a deformation temperature of room temperature, a strain rate ranging from 3.5 to 10 s<sup>−1</sup>, and a dissipation rate of 0.12. Under these optimal processing parameters, the material microstructure mainly consisted of dynamically recrystallized grains and deformed grains.</div></div>\",\"PeriodicalId\":14216,\"journal\":{\"name\":\"International Journal of Refractory Metals & Hard Materials\",\"volume\":\"127 \",\"pages\":\"Article 106965\"},\"PeriodicalIF\":4.2000,\"publicationDate\":\"2024-11-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Refractory Metals & Hard Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S026343682400413X\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Refractory Metals & Hard Materials","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S026343682400413X","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
The study of deformation behavior and microstructure evolution in forged pure tantalum
In this study, the deformation characteristics of as-forged pure tantalum were investigated using a Gleeble-3800 thermal simulation testing machine in the temperature range of room temperature to 350 °C and strain rates ranging from 0.1 to 10 s−1, with a maximum deformation of 60 %. Results show that the deformation resistance increases with decreasing deformation temperature and increasing strain rate before reaching the peak stress. After reaching peak stress, deformation is dominated by dynamic recovery mechanisms. Based on the true stress-strain curves obtained from experiments, the deformation activation energy (Q) and stress exponent (n) of the material were calculated to be 5.133 kJ/mol and 3.1989, respectively. A constitutive equation describing the rheological behavior was established. Utilizing processing maps combined with post-deformation microstructures, optimal processing parameters were determined to be a deformation temperature of room temperature, a strain rate ranging from 3.5 to 10 s−1, and a dissipation rate of 0.12. Under these optimal processing parameters, the material microstructure mainly consisted of dynamically recrystallized grains and deformed grains.
期刊介绍:
The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.