声发射用于实时监测受污染磷酸环境中奥氏体不锈钢的界面侵蚀-腐蚀情况

IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL
Wear Pub Date : 2024-11-22 DOI:10.1016/j.wear.2024.205666
Sabah Aftimi , Younes Kerroum , Hassane Idrissi , Rachid Boulif , Nawal Semlal , Maha Elhawary , Abdelkbir Bellaouchou , Anton José Garcia , Hatem M.A. Amin , Maria Boudalia
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引用次数: 0

摘要

腐蚀-腐蚀是一个复杂的问题,会对磷酸生产中使用的奥氏体不锈钢设备造成严重破坏。本文对声发射(AE)信号以及腐蚀电位和重量损失进行了时间分辨分析,以在线监测和评估 904L 不锈钢在碳化硅磨料颗粒作用下的动态降解和去钝化过程。通过分析 AE 波形及其参数,可以深入了解侵蚀-腐蚀过程。AE 信号的均方根(RMS)电压和声能特征揭示了被动膜的自修复难度,其中 AE 信号的波形表现为不完美的连续高强度波形,范围在 0.1 至 0.4 mV 之间。对平均频谱的评估表明,SiC 颗粒的数量改变了损伤机制,从以犁耕为主的 AE 事件转变为以微切割为主的 AE 事件。这表明,不完美的连续波形可能是新声源(爆裂型)出现的前兆:切屑从切口突然跳出。这种反应导致合金的质量损失与高颗粒负荷(24 g L-1)下的相应声学反应呈准线性关系。非线性侵蚀-腐蚀行为表明,去钝化-再钝化事件是相互依赖的。这些结果使声学和电化学分析相结合成为在线研究同步变化的侵蚀和腐蚀速率的一种有效的可持续方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Acoustic emission for real-time monitoring of interfacial erosion-corrosion of austenitic stainless steel in polluted phosphoric acid environment

Acoustic emission for real-time monitoring of interfacial erosion-corrosion of austenitic stainless steel in polluted phosphoric acid environment
Erosion-corrosion is a complex problem causing severe damage of austenitic stainless-steel equipment used in phosphoric acid production. Herein, time-resolved analyses of the acoustic emission (AE) signal together with the corrosion potential and weight loss were performed to online monitor and evaluate the dynamic degradation and depassivation of the 904L stainless steel under the effect of abrasive SiC particles. Important insights into the erosion-corrosion process are gained from the analysis of the AE waveform and its parameters. The characteristic root mean square (RMS) voltage and acoustic energy of AE signals revealed the self-healing difficulty of the passive film, of which the waveform of AE signals showed the appearance of imperfect continuous high intensity waveform, ranging from 0.1 to 0.4 mV. Evaluation of the average frequency spectrum showed that the amount of SiC particles alters the damage mechanism from AE events dominated by ploughing to AE events driven by micro-cutting. This suggests that the imperfect continuous waveform is possibly a precursor to the emergence of new acoustic sources (burst type): sudden jumps of chips from the cutting lips. This response resulted in a quasi-linearity in the mass loss of the alloy with the respective acoustic response at high particle loading (24 g L−1). The non-linear erosion-corrosion behavior suggests that the depassivation-repassivation events are dependent. These results render the combined AE and electrochemical analysis an effective sustainable approach for the online investigation of the synchronously changing erosion and corrosion rates.
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来源期刊
Wear
Wear 工程技术-材料科学:综合
CiteScore
8.80
自引率
8.00%
发文量
280
审稿时长
47 days
期刊介绍: Wear journal is dedicated to the advancement of basic and applied knowledge concerning the nature of wear of materials. Broadly, topics of interest range from development of fundamental understanding of the mechanisms of wear to innovative solutions to practical engineering problems. Authors of experimental studies are expected to comment on the repeatability of the data, and whenever possible, conduct multiple measurements under similar testing conditions. Further, Wear embraces the highest standards of professional ethics, and the detection of matching content, either in written or graphical form, from other publications by the current authors or by others, may result in rejection.
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