使用 CS2 和环氧胺合成 1,3-噻唑烷-2-硫醚

IF 1.5 4区化学 Q3 CHEMISTRY, ORGANIC

Tetrahedron Letters Pub Date : 2024-11-06 DOI:10.1016/j.tetlet.2024.155361

Azim Ziyaei Halimehjani , Farzaneh Noorakhtar , Zahra Marjani

引用次数: 0

摘要

通过二硫化碳与 N-烷基（芳基）环氧胺的反应，开发出一种合成 5-（水氧甲基）-1,3-噻唑烷-2-硫代化合物的高效方法。该反应通过分子内环氧化物开环与原位制备的二硫代氨基甲酸进行。产物的收率很高。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

Synthesis of 1,3-thiazolidine-2-thiones using CS2 and epoxy amines

查看原文本刊更多论文

Synthesis of 1,3-thiazolidine-2-thiones using CS2 and epoxy amines

An efficient method for the synthesis of 5-(hydoxymethyl)-1,3-thiazolidine-2-thiones is developed via the reaction of carbon disulfide with N-alkyl(aryl) epoxy amines. The reaction proceeds via intramolecular epoxide ring opening with in situ prepared dithiocarbamic acid. The products were obtained in good to high yields.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Tetrahedron Letters 化学-有机化学

CiteScore

3.50

自引率

5.60%

发文量

521

审稿时长

28 days

期刊介绍： Tetrahedron Letters provides maximum dissemination of outstanding developments in organic chemistry. The journal is published weekly and covers developments in techniques, structures, methods and conclusions in experimental and theoretical organic chemistry. Rapid publication of timely and significant research results enables researchers from all over the world to transmit quickly their new contributions to large, international audiences.