Concetta Pelligra , Babak Shalchi Amirkhiz , Nafiseh Zafer , Jidong Kang , David S. Wilkinson
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A comprehensive understanding of the microstructural damage processes leading to fracture is presented using quasi in-situ Scanning Electron Microscope tensile testing as well as X-ray Computed Microtomography. In addition, we precisely evaluated the TRIP kinetics of this steel using a combined Digital Image Correlation (DIC) and synchrotron-sourced High Energy X-ray Diffraction technique. With these methods, we demonstrate that an abundance of voids nucleate during deformation, but their growth can be suppressed by prolonging TRIP over a large strain range. Moreover, novel post-processing techniques to assess DIC acquired data at the microscopic scale have been used to gauge the severity of strain partitioning amongst phases and strain gradient evolution across dissimilar phase interfaces. By comparing it to another 3G TRIP-assisted steel and an ultrafine grained Dual Phase steel. Overall, it has been found that, in addition to carefully moderating TRIP kinetics, the introduction of polygonal ferrite, as is conventional in med-Mn steels, enhances the local forming properties and damage tolerance in 3G TRIP-assisted microstructures.</div></div>","PeriodicalId":385,"journal":{"name":"Materials Science and Engineering: A","volume":"919 ","pages":"Article 147447"},"PeriodicalIF":6.1000,"publicationDate":"2024-10-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstrain partitioning, transformation induced plasticity, and damage evolution of a third generation medium Mn advanced high strength steel\",\"authors\":\"Concetta Pelligra , Babak Shalchi Amirkhiz , Nafiseh Zafer , Jidong Kang , David S. Wilkinson\",\"doi\":\"10.1016/j.msea.2024.147447\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>An experimental Medium Mn (med-Mn) steel (0.15C-5.8Mn-1.8Al-0.71Si) with a martensitic starting microstructure, intercritically annealed at 685 °C for 120s, was discovered to have a large true strain at fracture (ɛ<sub>f</sub> = 0.61) while also meeting established (strength x elongation) targets (28,809 MPa%), sustained monotonic work hardening and prolonged Transformation Induced Plasticity (TRIP) kinetics. This was found by varying the intercritical annealing (IA) temperature within a narrow temperature interval in order to isolate its impact on TRIP kinetics and damage development on such med-Mn steel. A comprehensive understanding of the microstructural damage processes leading to fracture is presented using quasi in-situ Scanning Electron Microscope tensile testing as well as X-ray Computed Microtomography. In addition, we precisely evaluated the TRIP kinetics of this steel using a combined Digital Image Correlation (DIC) and synchrotron-sourced High Energy X-ray Diffraction technique. With these methods, we demonstrate that an abundance of voids nucleate during deformation, but their growth can be suppressed by prolonging TRIP over a large strain range. Moreover, novel post-processing techniques to assess DIC acquired data at the microscopic scale have been used to gauge the severity of strain partitioning amongst phases and strain gradient evolution across dissimilar phase interfaces. By comparing it to another 3G TRIP-assisted steel and an ultrafine grained Dual Phase steel. 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引用次数: 0
摘要
一种具有马氏体起始显微组织的实验性中锰钢(0.15C-5.8Mn-1.8Al-0.71Si)在 685 °C 下进行 120s 的中间退火,发现其断裂时具有较大的真实应变(ɛf = 0.61),同时还满足既定的(强度 x 伸长率)目标(28,809 MPa%)、持续的单调加工硬化和较长的变形诱导塑性(TRIP)动力学。通过在较窄的温度区间内改变临界退火(IA)温度,我们发现了这一点,目的是隔离临界退火温度对中锰钢 TRIP 动力学和损伤发展的影响。我们利用准原位扫描电子显微镜拉伸测试和 X 射线计算机显微层析技术,全面了解了导致断裂的微观结构损伤过程。此外,我们还利用数字图像相关性(DIC)和同步辐射源高能 X 射线衍射技术,对这种钢的 TRIP 动力学进行了精确评估。通过这些方法,我们证明在变形过程中会产生大量空洞,但通过在较大应变范围内延长 TRIP 可以抑制空洞的生长。此外,我们还采用了新颖的后处理技术来评估微观尺度上的 DIC 采集数据,以衡量各相之间应变分化的严重程度以及不同相界面上应变梯度的演变情况。通过将其与另一种 3G TRIP 辅助钢和超细晶粒双相钢进行比较。总之,研究发现,除了精心调节 TRIP 动力学之外,按照中锰钢的传统做法引入多边形铁素体还能增强 3G TRIP 辅助微结构的局部成形性能和损伤耐受性。
Microstrain partitioning, transformation induced plasticity, and damage evolution of a third generation medium Mn advanced high strength steel
An experimental Medium Mn (med-Mn) steel (0.15C-5.8Mn-1.8Al-0.71Si) with a martensitic starting microstructure, intercritically annealed at 685 °C for 120s, was discovered to have a large true strain at fracture (ɛf = 0.61) while also meeting established (strength x elongation) targets (28,809 MPa%), sustained monotonic work hardening and prolonged Transformation Induced Plasticity (TRIP) kinetics. This was found by varying the intercritical annealing (IA) temperature within a narrow temperature interval in order to isolate its impact on TRIP kinetics and damage development on such med-Mn steel. A comprehensive understanding of the microstructural damage processes leading to fracture is presented using quasi in-situ Scanning Electron Microscope tensile testing as well as X-ray Computed Microtomography. In addition, we precisely evaluated the TRIP kinetics of this steel using a combined Digital Image Correlation (DIC) and synchrotron-sourced High Energy X-ray Diffraction technique. With these methods, we demonstrate that an abundance of voids nucleate during deformation, but their growth can be suppressed by prolonging TRIP over a large strain range. Moreover, novel post-processing techniques to assess DIC acquired data at the microscopic scale have been used to gauge the severity of strain partitioning amongst phases and strain gradient evolution across dissimilar phase interfaces. By comparing it to another 3G TRIP-assisted steel and an ultrafine grained Dual Phase steel. Overall, it has been found that, in addition to carefully moderating TRIP kinetics, the introduction of polygonal ferrite, as is conventional in med-Mn steels, enhances the local forming properties and damage tolerance in 3G TRIP-assisted microstructures.
期刊介绍:
Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.