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三乙二胺和四甲基乙二胺乙二胺四乙酰锌酸盐的晶体形态学

IF 0.6 4区 材料科学 Q4 CRYSTALLOGRAPHY
Crystallography Reports Pub Date : 2024-11-14 DOI:10.1134/S1063774523601491
V. V. Semenov, N. V. Zolotareva, N. M. Lazarev, B. I. Petrov, T. I. Lopatina, E. N. Razov
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引用次数: 0

摘要

乙二胺四乙酰锌酸盐三水合物（[HN(CH2CH2)3NH]ZnL⋅3H2О）和乙二胺四乙酰锌酸盐二水合物（[H(CH3)2NCH2CH2N(CH3)2H]ZnL⋅2H2О([H(CH3)2NCH2CH2N(CH3)2H]ZnL⋅2H2О)是通过氧化锌与乙二胺四乙酸反应，然后与乙二胺四乙酸盐或四甲基乙二胺盐反应合成的。合成的化合物从水溶液或有机溶剂中分离出来，呈纤维状、立方体和金字塔形晶体，并通过元素分析、扫描电子显微镜、红外光谱、热重分析和差示扫描量热法对其进行了表征。
本文章由计算机程序翻译，如有差异，请以英文原文为准。

Crystal Morphology of Triethylenediaminium and Tetramethylethylenediaminium Ethylenediaminetetraacetatozincates

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Crystal Morphology of Triethylenediaminium and Tetramethylethylenediaminium Ethylenediaminetetraacetatozincates

Triethylenediaminium ethylenediaminetetraacetatozincate trihydrate ([HN(CH2CH2)3NH]ZnL⋅ 3H2О) and tetramethylethylenediaminium ethylenediaminetetraacetatozincate dihydrate ([H(CH3)2NCH2CH2N(CH3)2H]ZnL⋅2H2О) were synthesized by the reaction of zinc oxides with ethylenediaminetetraacetic acid and then with its triethylenediaminum or tetramethylethylenediaminium salts. The synthesized compounds were isolated from aqueous solutions or organic solvents as fiber-like, cubic, and pyramidal crystals, which were characterized by elemental analysis, scanning electron microscopy, IR spectroscopy, thermogravimetry, and differential scanning calorimetry.

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来源期刊
Crystallography Reports
Crystallography Reports 化学-晶体学
CiteScore
1.10
自引率
28.60%
发文量
96
审稿时长
4-8 weeks
期刊介绍： Crystallography Reports is a journal that publishes original articles short communications, and reviews on various aspects of crystallography: diffraction and scattering of X-rays, electrons, and neutrons, determination of crystal structure of inorganic and organic substances, including proteins and other biological substances; UV-VIS and IR spectroscopy; growth, imperfect structure and physical properties of crystals; thin films, liquid crystals, nanomaterials, partially disordered systems, and the methods of studies.
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