Nongmaithem Century Luwang, Devendra Kumar Rana, M. K. Yadav, Himanshu Sharma, Arun Kumar, Sarvendra Kumar, Surbhi
{"title":"利用种子技术，通过 CBD 和溶热法合成氧化锌纳米结构","authors":"Nongmaithem Century Luwang, Devendra Kumar Rana, M. K. Yadav, Himanshu Sharma, Arun Kumar, Sarvendra Kumar, Surbhi","doi":"10.1007/s10971-024-06557-9","DOIUrl":null,"url":null,"abstract":"<div><p>ZnO nanorods were synthesized by using the seeds technique. The seeds were synthesized by the low-cost synthesis technique, the Chemical Bath Deposition (CBD) method. Further, CBD and solvothermal methods used these seeds in the next deposition to coating. The XRD results confirm the formation of the ZnO hexagonal phase. FESEM high magnification images confirm the formation of hexagonal-shaped nanorods for Samples 1 and 3 and for Sample 2 mixed nanostructures of disk-like nanoparticles and nanorods were observed. Further, these nanorods were used as the catalytic material under the halogen lamp to study dye degradation. Samples 1 and 3 show degradation up to 55% and 68%, whereas Sample 3 showed a higher catalytic rate which degraded methyl orange 90% dye in 40 min. The enhancement in catalytic activity is explained by structural, morphological, and optical properties. The deposition using the seeds technique enhanced the degradation efficiency.</p><h3>Graphical abstract</h3><div><figure><div><div><picture><source><img></source></picture></div></div></figure></div></div>","PeriodicalId":664,"journal":{"name":"Journal of Sol-Gel Science and Technology","volume":"112 3","pages":"728 - 737"},"PeriodicalIF":2.3000,"publicationDate":"2024-10-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of ZnO nanostructure via CBD and solvothermal method using seed technique\",\"authors\":\"Nongmaithem Century Luwang, Devendra Kumar Rana, M. K. Yadav, Himanshu Sharma, Arun Kumar, Sarvendra Kumar, Surbhi\",\"doi\":\"10.1007/s10971-024-06557-9\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>ZnO nanorods were synthesized by using the seeds technique. The seeds were synthesized by the low-cost synthesis technique, the Chemical Bath Deposition (CBD) method. Further, CBD and solvothermal methods used these seeds in the next deposition to coating. The XRD results confirm the formation of the ZnO hexagonal phase. FESEM high magnification images confirm the formation of hexagonal-shaped nanorods for Samples 1 and 3 and for Sample 2 mixed nanostructures of disk-like nanoparticles and nanorods were observed. Further, these nanorods were used as the catalytic material under the halogen lamp to study dye degradation. Samples 1 and 3 show degradation up to 55% and 68%, whereas Sample 3 showed a higher catalytic rate which degraded methyl orange 90% dye in 40 min. The enhancement in catalytic activity is explained by structural, morphological, and optical properties. The deposition using the seeds technique enhanced the degradation efficiency.</p><h3>Graphical abstract</h3><div><figure><div><div><picture><source><img></source></picture></div></div></figure></div></div>\",\"PeriodicalId\":664,\"journal\":{\"name\":\"Journal of Sol-Gel Science and Technology\",\"volume\":\"112 3\",\"pages\":\"728 - 737\"},\"PeriodicalIF\":2.3000,\"publicationDate\":\"2024-10-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Sol-Gel Science and Technology\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s10971-024-06557-9\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Sol-Gel Science and Technology","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1007/s10971-024-06557-9","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Synthesis of ZnO nanostructure via CBD and solvothermal method using seed technique
ZnO nanorods were synthesized by using the seeds technique. The seeds were synthesized by the low-cost synthesis technique, the Chemical Bath Deposition (CBD) method. Further, CBD and solvothermal methods used these seeds in the next deposition to coating. The XRD results confirm the formation of the ZnO hexagonal phase. FESEM high magnification images confirm the formation of hexagonal-shaped nanorods for Samples 1 and 3 and for Sample 2 mixed nanostructures of disk-like nanoparticles and nanorods were observed. Further, these nanorods were used as the catalytic material under the halogen lamp to study dye degradation. Samples 1 and 3 show degradation up to 55% and 68%, whereas Sample 3 showed a higher catalytic rate which degraded methyl orange 90% dye in 40 min. The enhancement in catalytic activity is explained by structural, morphological, and optical properties. The deposition using the seeds technique enhanced the degradation efficiency.
期刊介绍：
The primary objective of the Journal of Sol-Gel Science and Technology (JSST), the official journal of the International Sol-Gel Society, is to provide an international forum for the dissemination of scientific, technological, and general knowledge about materials processed by chemical nanotechnologies known as the "sol-gel" process. The materials of interest include gels, gel-derived glasses, ceramics in form of nano- and micro-powders, bulk, fibres, thin films and coatings as well as more recent materials such as hybrid organic-inorganic materials and composites. Such materials exhibit a wide range of optical, electronic, magnetic, chemical, environmental, and biomedical properties and functionalities. Methods for producing sol-gel-derived materials and the industrial uses of these materials are also of great interest.
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