Sanaz Kamrani, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh, Mahboob Nemati, Aramdokht Khatibi
{"title":"开发基于分子印迹聚合物的分散微固相萃取技术,用于选择性萃取金枪鱼罐头样品中的组胺,然后利用气相色谱-质谱联用仪进行测定","authors":"Sanaz Kamrani, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh, Mahboob Nemati, Aramdokht Khatibi","doi":"10.1007/s11696-024-03682-1","DOIUrl":null,"url":null,"abstract":"<div><p>A molecularly imprinted polymer-based dispersive micro-solid-phase extraction method has been developed for the efficient extraction and preconcentration of histamine from tuna fish samples prior to its determination by gas chromatography–flame ionization detector. In this approach, a molecularly imprinted polymer was prepared by chemical oxidation of pyrrole using iron (III) chloride, and then, it was characterized by Fourier transform infrared spectroscopy and scanning electron microscopy and used in the extraction procedure. The method was validated using the International Council Research Protocol, and the results showed low limits of detection (0.06 mg kg<sup>−1</sup>) and quantification (0.21 mg kg<sup>−1</sup>), good precision (relative standard deviation = 3.2%), linearity (r<sup>2</sup> ≥ 0.9969) and acceptable extraction recovery (98%). The method was successfully done on various tuna fish samples, and histamine was determined in them.</p></div>","PeriodicalId":513,"journal":{"name":"Chemical Papers","volume":null,"pages":null},"PeriodicalIF":2.2000,"publicationDate":"2024-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Development of molecularly imprinted polymer-based dispersive micro-solid-phase extraction for the selective extraction of histamine from canned tuna fish samples prior to its determination by GC–FID\",\"authors\":\"Sanaz Kamrani, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh, Mahboob Nemati, Aramdokht Khatibi\",\"doi\":\"10.1007/s11696-024-03682-1\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>A molecularly imprinted polymer-based dispersive micro-solid-phase extraction method has been developed for the efficient extraction and preconcentration of histamine from tuna fish samples prior to its determination by gas chromatography–flame ionization detector. In this approach, a molecularly imprinted polymer was prepared by chemical oxidation of pyrrole using iron (III) chloride, and then, it was characterized by Fourier transform infrared spectroscopy and scanning electron microscopy and used in the extraction procedure. The method was validated using the International Council Research Protocol, and the results showed low limits of detection (0.06 mg kg<sup>−1</sup>) and quantification (0.21 mg kg<sup>−1</sup>), good precision (relative standard deviation = 3.2%), linearity (r<sup>2</sup> ≥ 0.9969) and acceptable extraction recovery (98%). The method was successfully done on various tuna fish samples, and histamine was determined in them.</p></div>\",\"PeriodicalId\":513,\"journal\":{\"name\":\"Chemical Papers\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":2.2000,\"publicationDate\":\"2024-10-09\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Chemical Papers\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s11696-024-03682-1\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"Engineering\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemical Papers","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1007/s11696-024-03682-1","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"Engineering","Score":null,"Total":0}
Development of molecularly imprinted polymer-based dispersive micro-solid-phase extraction for the selective extraction of histamine from canned tuna fish samples prior to its determination by GC–FID
A molecularly imprinted polymer-based dispersive micro-solid-phase extraction method has been developed for the efficient extraction and preconcentration of histamine from tuna fish samples prior to its determination by gas chromatography–flame ionization detector. In this approach, a molecularly imprinted polymer was prepared by chemical oxidation of pyrrole using iron (III) chloride, and then, it was characterized by Fourier transform infrared spectroscopy and scanning electron microscopy and used in the extraction procedure. The method was validated using the International Council Research Protocol, and the results showed low limits of detection (0.06 mg kg−1) and quantification (0.21 mg kg−1), good precision (relative standard deviation = 3.2%), linearity (r2 ≥ 0.9969) and acceptable extraction recovery (98%). The method was successfully done on various tuna fish samples, and histamine was determined in them.
Chemical PapersChemical Engineering-General Chemical Engineering
CiteScore
3.30
自引率
4.50%
发文量
590
期刊介绍:
Chemical Papers is a peer-reviewed, international journal devoted to basic and applied chemical research. It has a broad scope covering the chemical sciences, but favors interdisciplinary research and studies that bring chemistry together with other disciplines.