M. Yu. Tashmetov, B. S. Yuldashev, S. M. Adizov, S. E. Kichanov, Sh. R. Pidaev, N. B. Ismatov, N. D. Dvurechenskaya, I. A. Saprykina, B. A. Abdurakhimov, F. K. Khallokov
{"title":"利用中子断层扫描技术对乌孙达拉要塞出土的欧特海摩斯一世钱币和指环碎片进行无损结构研究","authors":"M. Yu. Tashmetov, B. S. Yuldashev, S. M. Adizov, S. E. Kichanov, Sh. R. Pidaev, N. B. Ismatov, N. D. Dvurechenskaya, I. A. Saprykina, B. A. Abdurakhimov, F. K. Khallokov","doi":"10.1134/S1027451024700587","DOIUrl":null,"url":null,"abstract":"<p>The penetration of corrosion into the volume of the copper coin of Euthydemus I and the fragments of rings from the Uzundara fortress was studied by the methods of neutron radiography and tomography using a facility installed on the horizontal beamline of the WWR-SM nuclear reactor of the Institute of Nuclear Physics, Academy of Sciences of the Republic of Uzbekistan. Three-dimensional models of the studied archaeological objects were reconstructed, and the volume fractions of the initial metal and corrosive materials were calculated. A large number of pores and cavities were found inside the volume of the coin, which may indicate a violation or imperfection of the casting technology, as well as active chemical processes due to the interaction of the coin with the soil. X-ray diffraction studies have established the presence of phases of copper, cuprite Cu<sub>2</sub>O, and nantokite CuCl on the surface of the Euthydemus I coin. According to neutron tomography data, the volume content of copper and corrosion products was determined to be 1469.93(2) and 169.04(2) mm<sup>3</sup>, respectively. The distribution of pores in the volume of the Euthydemus I coin by an equivalent diameter has also been established. Two rings were studied at the neutron radiography and tomography facility; the volume of the first ring was 1491.17(6) mm<sup>3</sup>, and the volume of a certain corrosion was 135.69(7) mm<sup>3</sup>. On the second ring, the corrosion volume was 373.67(3) mm<sup>3</sup>, which is 12.1% of the total ring volume.</p>","PeriodicalId":671,"journal":{"name":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","volume":"18 4","pages":"874 - 880"},"PeriodicalIF":0.5000,"publicationDate":"2024-09-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Nondestructive Structural Studies of the Euthydemus I Coin and Fragments of Rings from the Uzundara Fortress Using Neutron Tomography\",\"authors\":\"M. Yu. Tashmetov, B. S. Yuldashev, S. M. Adizov, S. E. Kichanov, Sh. R. Pidaev, N. B. Ismatov, N. D. Dvurechenskaya, I. A. Saprykina, B. A. Abdurakhimov, F. K. Khallokov\",\"doi\":\"10.1134/S1027451024700587\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The penetration of corrosion into the volume of the copper coin of Euthydemus I and the fragments of rings from the Uzundara fortress was studied by the methods of neutron radiography and tomography using a facility installed on the horizontal beamline of the WWR-SM nuclear reactor of the Institute of Nuclear Physics, Academy of Sciences of the Republic of Uzbekistan. Three-dimensional models of the studied archaeological objects were reconstructed, and the volume fractions of the initial metal and corrosive materials were calculated. A large number of pores and cavities were found inside the volume of the coin, which may indicate a violation or imperfection of the casting technology, as well as active chemical processes due to the interaction of the coin with the soil. X-ray diffraction studies have established the presence of phases of copper, cuprite Cu<sub>2</sub>O, and nantokite CuCl on the surface of the Euthydemus I coin. According to neutron tomography data, the volume content of copper and corrosion products was determined to be 1469.93(2) and 169.04(2) mm<sup>3</sup>, respectively. The distribution of pores in the volume of the Euthydemus I coin by an equivalent diameter has also been established. Two rings were studied at the neutron radiography and tomography facility; the volume of the first ring was 1491.17(6) mm<sup>3</sup>, and the volume of a certain corrosion was 135.69(7) mm<sup>3</sup>. On the second ring, the corrosion volume was 373.67(3) mm<sup>3</sup>, which is 12.1% of the total ring volume.</p>\",\"PeriodicalId\":671,\"journal\":{\"name\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"volume\":\"18 4\",\"pages\":\"874 - 880\"},\"PeriodicalIF\":0.5000,\"publicationDate\":\"2024-09-26\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1027451024700587\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, CONDENSED MATTER\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1134/S1027451024700587","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, CONDENSED MATTER","Score":null,"Total":0}
Nondestructive Structural Studies of the Euthydemus I Coin and Fragments of Rings from the Uzundara Fortress Using Neutron Tomography
The penetration of corrosion into the volume of the copper coin of Euthydemus I and the fragments of rings from the Uzundara fortress was studied by the methods of neutron radiography and tomography using a facility installed on the horizontal beamline of the WWR-SM nuclear reactor of the Institute of Nuclear Physics, Academy of Sciences of the Republic of Uzbekistan. Three-dimensional models of the studied archaeological objects were reconstructed, and the volume fractions of the initial metal and corrosive materials were calculated. A large number of pores and cavities were found inside the volume of the coin, which may indicate a violation or imperfection of the casting technology, as well as active chemical processes due to the interaction of the coin with the soil. X-ray diffraction studies have established the presence of phases of copper, cuprite Cu2O, and nantokite CuCl on the surface of the Euthydemus I coin. According to neutron tomography data, the volume content of copper and corrosion products was determined to be 1469.93(2) and 169.04(2) mm3, respectively. The distribution of pores in the volume of the Euthydemus I coin by an equivalent diameter has also been established. Two rings were studied at the neutron radiography and tomography facility; the volume of the first ring was 1491.17(6) mm3, and the volume of a certain corrosion was 135.69(7) mm3. On the second ring, the corrosion volume was 373.67(3) mm3, which is 12.1% of the total ring volume.
期刊介绍:
Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.