基于响应面方法学-正交试验的缓释盐储存融雪骨料制备工艺及其缓释性能优化研究

IF 4.4 2区 化学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Zhenzheng Liu , Bo Li , Tengfei Yao , Mengkai Sun , Yaping Wang , Liangliang Niu , Yuan Du
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引用次数: 0

摘要

储盐式沥青路面能有效缓解冬季路面积雪结冰问题,保证行车安全和运输能力。储盐型融雪抑冰材料是储盐沥青路面发挥作用的关键。本文旨在通过正交试验和响应面法的耦合,开发一种持续释放性能优异的融雪抑冰骨料。通过正交试验和响应面法对吸附时间、融雪盐溶液浓度、多孔集料与融雪盐的质量比等三个工艺变量进行了优化。然后,通过吸附性能测试确定了储盐骨料的制备工艺。最后,测试了缓释储盐融雪骨料的物理机械性能、缓释性能和融冰性能。结果表明,储盐骨料的最佳制备工艺为吸附时间为 12 h,融雪剂溶液浓度为 30 %,融雪盐与储盐载体的质量比为 0.5:1。储盐骨料与包裹材料(酚醛树脂)的最佳质量比为 1:2.5。180 分钟后,缓释储盐融雪骨料的盐释放量比未包裹的储盐骨料低约 43.75%。同时,5 克缓释储盐融雪骨料在零下 5 摄氏度时的融冰量为 0.9 克。此外,用不同比例的沥青包裹的缓释蓄盐融雪骨料可以释放盐分,其电导率在稳定阶段至少为 1200 μs/cm。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Optimization of slow-release salt storage snowmelt aggregate preparation process and its slow-release performance based on response surface methodology-orthogonal test

Salt storage asphalt pavement can effectively alleviate the problem of pavement snow and ice in winter, and ensure the driving safety and transportation capacity. Salt storage type snow melting and ice suppression materials are the key to the function of salt storage asphalt pavement. The purpose of this paper is to develop a snow-melting and ice suppression aggregate with outstanding sustained release performance by coupling the orthogonal test and response surface method. Three process variables, such as adsorption time, concentration of snow-melting salt solution and mass ratio of porous aggregate to snow melting salt, were optimized by orthogonal test and response surface method. Then, the preparation process of salt storage aggregate was determined by adsorption performance test. Finally, the physical and mechanical properties, slow release performance and ice melting performance of the slow-release salt-storage snowmelt aggregate were tested. The results showed that the optimum preparation process of salt-storing aggregate was the adsorption time of 12 h, concentration of snow-melting agent solution of 30 %, and mass ratio of snow-melting salt to salt-storing carrier of 0.5:1. The optimum mass ratio of salt-storing aggregate to wrapping material (phenolic resin) was 1:2.5. The salt release amount of the slow-release salt-storing snowmelt aggregate at 180 min was about 43.75 % lower than that of the unwrapped salt-storing aggregate. At the same time, 5 g of slow-release salt-storing snow-melting aggregate had a melting ice amount of 0.9 g at a temperature of −5°C. In addition, the slow-release salt-storing snow-melting aggregates wrapped with different proportions of asphalt could release salt, and its conductivity was at least 1200 μs/cm in the stable stage.

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来源期刊
CiteScore
7.20
自引率
6.00%
发文量
810
期刊介绍: ACS Applied Polymer Materials is an interdisciplinary journal publishing original research covering all aspects of engineering, chemistry, physics, and biology relevant to applications of polymers. The journal is devoted to reports of new and original experimental and theoretical research of an applied nature that integrates fundamental knowledge in the areas of materials, engineering, physics, bioscience, polymer science and chemistry into important polymer applications. The journal is specifically interested in work that addresses relationships among structure, processing, morphology, chemistry, properties, and function as well as work that provide insights into mechanisms critical to the performance of the polymer for applications.
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