纳米粒子合成过程中的反向微乳液激光诊断技术

IF 0.8 4区物理与天体物理 Q4 OPTICS

Optics and Spectroscopy Pub Date : 2024-09-11 DOI:10.1134/S0030400X24030159

I. V. Plastinin, T. A. Dolenko

{"title":"纳米粒子合成过程中的反向微乳液激光诊断技术","authors":"I. V. Plastinin, T. A. Dolenko","doi":"10.1134/S0030400X24030159","DOIUrl":null,"url":null,"abstract":"In this work, laser spectroscopy was used to study reverse microemulsions, in which the reaction of ZnS nanoparticle synthesis was carried out. The sizes of the synthesized nanoparticles do not exceed 5 nm. As a result of studying the processes in the reaction medium, it was found that the band of stretching vibrations of HS– ions in the region of 2568 cm–1 is an identification sign of the synthesis of nanoparticles: by its intensity it is possible to determine the stage and completion of the ZnS synthesis.","PeriodicalId":723,"journal":{"name":"Optics and Spectroscopy","volume":"132 3","pages":"287 - 289"},"PeriodicalIF":0.8000,"publicationDate":"2024-09-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Laser Diagnostics of Reverse Microemulsions in the Process of Nanoparticle Synthesis\",\"authors\":\"I. V. Plastinin, T. A. Dolenko\",\"doi\":\"10.1134/S0030400X24030159\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this work, laser spectroscopy was used to study reverse microemulsions, in which the reaction of ZnS nanoparticle synthesis was carried out. The sizes of the synthesized nanoparticles do not exceed 5 nm. As a result of studying the processes in the reaction medium, it was found that the band of stretching vibrations of HS– ions in the region of 2568 cm–1 is an identification sign of the synthesis of nanoparticles: by its intensity it is possible to determine the stage and completion of the ZnS synthesis.\",\"PeriodicalId\":723,\"journal\":{\"name\":\"Optics and Spectroscopy\",\"volume\":\"132 3\",\"pages\":\"287 - 289\"},\"PeriodicalIF\":0.8000,\"publicationDate\":\"2024-09-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Optics and Spectroscopy\",\"FirstCategoryId\":\"101\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S0030400X24030159\",\"RegionNum\":4,\"RegionCategory\":\"物理与天体物理\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"OPTICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Optics and Spectroscopy","FirstCategoryId":"101","ListUrlMain":"https://link.springer.com/article/10.1134/S0030400X24030159","RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"OPTICS","Score":null,"Total":0}

引用次数: 0

摘要

摘要在这项工作中，使用激光光谱法研究了反向微乳液，其中进行了合成 ZnS 纳米粒子的反应。合成的纳米粒子尺寸不超过 5 nm。通过研究反应介质中的过程，发现 2568 cm-1 区域的 HS- 离子伸缩振动带是纳米粒子合成的识别标志：根据其强度可以确定 ZnS 合成的阶段和完成情况。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

Laser Diagnostics of Reverse Microemulsions in the Process of Nanoparticle Synthesis

查看原文本刊更多论文

Laser Diagnostics of Reverse Microemulsions in the Process of Nanoparticle Synthesis

In this work, laser spectroscopy was used to study reverse microemulsions, in which the reaction of ZnS nanoparticle synthesis was carried out. The sizes of the synthesized nanoparticles do not exceed 5 nm. As a result of studying the processes in the reaction medium, it was found that the band of stretching vibrations of HS^– ions in the region of 2568 cm^–1 is an identification sign of the synthesis of nanoparticles: by its intensity it is possible to determine the stage and completion of the ZnS synthesis.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Optics and Spectroscopy 物理-光谱学

CiteScore

1.60

自引率

0.00%

发文量

审稿时长

4.5 months

期刊介绍： Optics and Spectroscopy (Optika i spektroskopiya), founded in 1956, presents original and review papers in various fields of modern optics and spectroscopy in the entire wavelength range from radio waves to X-rays. Topics covered include problems of theoretical and experimental spectroscopy of atoms, molecules, and condensed state, lasers and the interaction of laser radiation with matter, physical and geometrical optics, holography, and physical principles of optical instrument making.