{"title":"从 Iris kashmiriana(Mazar-Graveyard)植物提取物中绿色合成氧化铁纳米颗粒及其生物活性和光催化活性表征","authors":"Asima Imtiyaz, Ajay Singh, Abhishek Bhardwaj","doi":"10.1016/j.jiec.2024.09.004","DOIUrl":null,"url":null,"abstract":"A significant area of interest for researchers has been the creation of trustworthy experimental techniques for producing metallic nanoparticles with specified structures and dimensions. Due to the unique features that make them usable in various scientific and technological disciplines, metallic nanoparticles made by green synthesis have attracted enormous interest over the past ten years. In this study, the plant extract of was used to create iron oxide nanoparticles utilizing a relatively affordable and straightforward conventional heating process. Fourier transform infrared spectroscopy, scanning electron microscopy, energy dispersive X-ray, and X-ray diffraction were used to analyze the iron nanoparticles. Particles with diameters of 20–40 nm were created. The synthesized Iron oxide nanoparticles exhibit significant antibacterial effects against four pathogens by exhibiting a zone of inhibition for Vancomycin. The antioxidant activity DPPH of the iron oxide nanoparticles showed 83.29 %, 84.96 %, 86.71 %, 88.62 %, and 88.65 % at a different concentration, demonstrating that the scavenging percentage increases with increasing the iron oxide nanoparticles concentrations. After an investigation, Iron oxide nanoparticles were capable of photo-catalytically degrading Congo red. It was observed that at the maximum exposure length of 60 min, approximately 95 % of the dye was destroyed. This study’s findings open up new possibilities for creating, modifying, and using plant extract in nanoparticle design, development, and application.","PeriodicalId":363,"journal":{"name":"Journal of Industrial and Engineering Chemistry","volume":"266 1","pages":""},"PeriodicalIF":5.9000,"publicationDate":"2024-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Green synthesis of iron oxide nanoparticles from Iris kashmiriana (Mazar-Graveyard) Plant Extract its characterization of biological activities and photocatalytic activity\",\"authors\":\"Asima Imtiyaz, Ajay Singh, Abhishek Bhardwaj\",\"doi\":\"10.1016/j.jiec.2024.09.004\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A significant area of interest for researchers has been the creation of trustworthy experimental techniques for producing metallic nanoparticles with specified structures and dimensions. Due to the unique features that make them usable in various scientific and technological disciplines, metallic nanoparticles made by green synthesis have attracted enormous interest over the past ten years. In this study, the plant extract of was used to create iron oxide nanoparticles utilizing a relatively affordable and straightforward conventional heating process. Fourier transform infrared spectroscopy, scanning electron microscopy, energy dispersive X-ray, and X-ray diffraction were used to analyze the iron nanoparticles. Particles with diameters of 20–40 nm were created. The synthesized Iron oxide nanoparticles exhibit significant antibacterial effects against four pathogens by exhibiting a zone of inhibition for Vancomycin. The antioxidant activity DPPH of the iron oxide nanoparticles showed 83.29 %, 84.96 %, 86.71 %, 88.62 %, and 88.65 % at a different concentration, demonstrating that the scavenging percentage increases with increasing the iron oxide nanoparticles concentrations. After an investigation, Iron oxide nanoparticles were capable of photo-catalytically degrading Congo red. It was observed that at the maximum exposure length of 60 min, approximately 95 % of the dye was destroyed. This study’s findings open up new possibilities for creating, modifying, and using plant extract in nanoparticle design, development, and application.\",\"PeriodicalId\":363,\"journal\":{\"name\":\"Journal of Industrial and Engineering Chemistry\",\"volume\":\"266 1\",\"pages\":\"\"},\"PeriodicalIF\":5.9000,\"publicationDate\":\"2024-09-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Industrial and Engineering Chemistry\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://doi.org/10.1016/j.jiec.2024.09.004\",\"RegionNum\":3,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Industrial and Engineering Chemistry","FirstCategoryId":"5","ListUrlMain":"https://doi.org/10.1016/j.jiec.2024.09.004","RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
摘要
研究人员关注的一个重要领域是创造出值得信赖的实验技术,用于生产具有特定结构和尺寸的金属纳米粒子。在过去的十年中,通过绿色合成技术制造的金属纳米粒子因其独特的特性而在各种科学和技术学科中得到了广泛的应用。在这项研究中,我们采用了一种相对经济实惠、简单直接的传统加热工艺,利用植物提取物来制造氧化铁纳米粒子。傅立叶变换红外光谱、扫描电子显微镜、能量色散 X 射线和 X 射线衍射被用来分析铁纳米粒子。生成的颗粒直径为 20-40 纳米。合成的氧化铁纳米粒子对四种病原体有明显的抗菌效果,对万古霉素有一定的抑制作用。在不同浓度下,纳米氧化铁的 DPPH 抗氧化活性分别为 83.29%、84.96%、86.71%、88.62% 和 88.65%,表明随着纳米氧化铁浓度的增加,其清除率也在增加。经过研究,纳米氧化铁粒子能够光催化降解刚果红。据观察,在 60 分钟的最长曝光时间内,约 95% 的染料被破坏。这项研究的发现为在纳米粒子的设计、开发和应用中创造、改造和使用植物提取物提供了新的可能性。
Green synthesis of iron oxide nanoparticles from Iris kashmiriana (Mazar-Graveyard) Plant Extract its characterization of biological activities and photocatalytic activity
A significant area of interest for researchers has been the creation of trustworthy experimental techniques for producing metallic nanoparticles with specified structures and dimensions. Due to the unique features that make them usable in various scientific and technological disciplines, metallic nanoparticles made by green synthesis have attracted enormous interest over the past ten years. In this study, the plant extract of was used to create iron oxide nanoparticles utilizing a relatively affordable and straightforward conventional heating process. Fourier transform infrared spectroscopy, scanning electron microscopy, energy dispersive X-ray, and X-ray diffraction were used to analyze the iron nanoparticles. Particles with diameters of 20–40 nm were created. The synthesized Iron oxide nanoparticles exhibit significant antibacterial effects against four pathogens by exhibiting a zone of inhibition for Vancomycin. The antioxidant activity DPPH of the iron oxide nanoparticles showed 83.29 %, 84.96 %, 86.71 %, 88.62 %, and 88.65 % at a different concentration, demonstrating that the scavenging percentage increases with increasing the iron oxide nanoparticles concentrations. After an investigation, Iron oxide nanoparticles were capable of photo-catalytically degrading Congo red. It was observed that at the maximum exposure length of 60 min, approximately 95 % of the dye was destroyed. This study’s findings open up new possibilities for creating, modifying, and using plant extract in nanoparticle design, development, and application.
期刊介绍:
Journal of Industrial and Engineering Chemistry is published monthly in English by the Korean Society of Industrial and Engineering Chemistry. JIEC brings together multidisciplinary interests in one journal and is to disseminate information on all aspects of research and development in industrial and engineering chemistry. Contributions in the form of research articles, short communications, notes and reviews are considered for publication. The editors welcome original contributions that have not been and are not to be published elsewhere. Instruction to authors and a manuscript submissions form are printed at the end of each issue. Bulk reprints of individual articles can be ordered. This publication is partially supported by Korea Research Foundation and the Korean Federation of Science and Technology Societies.