低温合成高度分散的铝酸钙

IF 1.8 3区 化学 Q3 CHEMISTRY, INORGANIC & NUCLEAR
L. O. Kozlova, I. L. Voroshilov, Yu. V. Ioni, A. G. Son, A. S. Popova, I. V. Kozerozhets
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引用次数: 0

摘要

摘要 介绍了一种在 900°C 以下温度条件下制备具有所需特性(体积密度从 0.015 g/cm3 开始,粒度在 7-42 nm 范围内)的高分散铝酸钙的新方法,包括逐步热处理 CaO : Al2O3 = 1 : 2 的 Al(NO3)3、Ca(NO3)2 和 C6H8O7 的浓水溶液。通过 X 射线粉末衍射、红外光谱以及扫描和透射电子显微镜对合成的主要阶段进行了研究。利用所开发的方法获得的高分散铝酸钙具有明显的发光特性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Low-Temperature Synthesis of Highly Dispersed Calcium Aluminate

Low-Temperature Synthesis of Highly Dispersed Calcium Aluminate

Abstract

A new approach to prepare highly dispersed calcium aluminate at temperatures from 900°C with desired properties (bulk density starting from 0.015 g/cm3, particle size falling in the range of 7–42 nm) is described, which consists of step-by-step heat treatment of a concentrated aqueous solution of Al(NO3)3, Ca(NO3)2, and C6H8O7 in the molar ratio CaO : Al2O3 = 1 : 2. The main stages of the synthesis are studied by X-ray powder diffraction, IR spectroscopy, as well as scanning and transmission electron microscopies. The highly dispersed calcium aluminate obtained using the developed approach has pronounced luminescent properties.

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来源期刊
Russian Journal of Inorganic Chemistry
Russian Journal of Inorganic Chemistry 化学-无机化学与核化学
CiteScore
3.10
自引率
38.10%
发文量
237
审稿时长
3 months
期刊介绍: Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.
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