Daniel Monceau, Hugo Enjalbert, Clara Desgranges, Tom Sanviemvongsak, Antoine Casadebaigt, Thomas Perez
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Stepwise Multi-Temperature Thermogravimetric Analysis (SMT-TGA) for Rapid Alloy Development
A stepwise multi-temperature thermogravimetric analysis (SMT-TGA) method is a rapid and time- and material-efficient measurement procedure for oxidation kinetics over a wide range of temperatures. It is suitable for alloy design and material selection procedures. It involves subjecting a sample to a series of steps at increasing temperatures, followed by steps at decreasing temperatures to identify possible effects on the evolution of oxide layer microstructures on oxidation kinetics. This method has been tested for a wide range of metallic alloys in the present work, allowing for the mapping of possible ranges of parabolic oxidation kinetics of industrial alloys between 600 and 1300°C. Two examples of effects of thermal history have also been described in this publication.
期刊介绍：
Oxidation of Metals is the premier source for the rapid dissemination of current research on all aspects of the science of gas-solid reactions at temperatures greater than about 400˚C, with primary focus on the high-temperature corrosion of bulk and coated systems. This authoritative bi-monthly publishes original scientific papers on kinetics, mechanisms, studies of scales from structural and morphological viewpoints, transport properties in scales, phase-boundary reactions, and much more. Articles may discuss both theoretical and experimental work related to gas-solid reactions at the surface or near-surface of a material exposed to elevated temperatures, including reactions with oxygen, nitrogen, sulfur, carbon and halogens. In addition, Oxidation of Metals publishes the results of frontier research concerned with deposit-induced attack. Review papers and short technical notes are encouraged.
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