用浸渍磷酸二氢铝的刺槐纤维增强硅溶胶壳的强度和断裂特性

IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
Hao Liu, Chang Liu, Hua Feng, Zhongxing Tian, Xiangdong Liu
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引用次数: 0

摘要

用氢氧化钠水溶液对刺槐纤维进行碱煮沸处理,并在磷酸二氢铝溶液中浸渍,以提高其抗热震性并加固用于熔模铸造的型壳。分析了经处理纤维的微观结构和抗热震性,并研究了它们对加固型壳性能的影响。研究发现,经过碱煮沸处理的纤维表面的半纤维素和木质素被去除。在 15.0 重量%的磷酸二氢铝溶液中浸渍后,煮沸后的纤维表面形成了一层致密的保护膜。此外,研究结果表明,与未加工的纤维相比,煮沸浸渍纤维的重量损失减少了 44.61%,这表明纤维的抗热震性显著提高。此外,用 1.29 wt.% 的沸腾浸渍纤维增强的试样的高温强度达到了 20.11 MPa 的峰值,与未增强的试样相比提高了 68.12%。而碱性沸腾浸渍纤维增强的外壳在高温下发生的低变形重量仅为 0.49%。尤其是具有抗热震性的浸渍纤维,不仅保证了增强壳体良好的透气性,还增强了高温抗裂能力。这充分证明了浸渍处理在提高纤维抗热震性方面的有效性,在实际制壳中的应用前景十分广阔。 图文摘要
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Strength and Fracture Characteristics of Silica Sol Shell Reinforced with Abaca Fibers Impregnated with Aluminum Dihydrogen Phosphate

Strength and Fracture Characteristics of Silica Sol Shell Reinforced with Abaca Fibers Impregnated with Aluminum Dihydrogen Phosphate

Abaca fibers were alkaline boiling treated with sodium hydroxide aqueous solution combined with impregnating in aluminum dihydrogen phosphate solution to improve the thermal shock resistance and reinforce shells for investment casting. The microstructure and thermal shock resistance of the treated fibers were analyzed, and their influence on the properties of reinforced shells was investigated. It is found that the hemicellulose and lignin at the surfaces of the fibers undergoing alkaline boiling were removed. A dense protective film was formed on the boiled fibers surfaces through impregnating in a solution of 15.0 wt.% aluminum dihydrogen phosphate. Moreover, the results demonstrated that the weight loss of the boiled-impregnated fibers reduces by 44.61%, compared to the raw fibers, indicating significantly improving the thermal shock resistance. Furthermore, the high-temperature strength of specimens reinforced with boiled-impregnated fibers of 1.29 wt.% reached a peak of 20.11 MPa, increasing by 68.12% compared to the unreinforced. And the alkaline boiled-immersed fibers reinforced shell occurred at elevated temperature a low deformation underweight of only 0.49%. Especially, the impregnated fibers with thermal shock resistance not only ensured good permeability of reinforced shells, but also enhanced the high-temperature cracking resistance capacity. This fully demonstrates the effectiveness of impregnating treatment in improving thermal shock resistance of fibers, and it is very promising to be applied in practical shell-making.

Graphical Abstract

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来源期刊
Journal of Materials Engineering and Performance
Journal of Materials Engineering and Performance 工程技术-材料科学:综合
CiteScore
3.90
自引率
13.00%
发文量
1120
审稿时长
4.9 months
期刊介绍: ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance. The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication. Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered
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