探索溶胶-凝胶合成 CaO:MgAl2O4 纳米复合材料的多种应用:形态、光催化和电化学前景

IF 5.5 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
H. K. Jahnavi, S. Rajendra Prasad, H. P. Nagaswarupa, Ramachandra Naik, N. Basavaraju, C. R. Ravikumar, Burragoni Sravanthi Goud, Jae Hong Kim
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引用次数: 0

摘要

通过一种简单、经济的溶胶-凝胶法合成了 CaO:MgAl2O4 纳米复合材料。对新型 CaO:MgAl2O4 纳米复合材料的研究包括对其形态和结构变化的考察,以及对其光催化活性和电化学特性的探索。XRD 分析显示,纳米复合材料的尺寸为 24.15 纳米。扫描电子显微镜(SEM)显示了 CaO:MgAl2O4 样品的片状形态变化。对 CaO:MgAl2O4 纳米复合材料的 TEM、HRTEM 和 SAED 研究将揭示其形态、结晶学和纳米结构的重要细节。通过研究去离子水中酸性红-88(AR-88)染料的降解情况来量化光催化活性,在紫外线照射下,120 分钟内染料降解率达到 70%。利用降解染料的水进行了植物生长测试,以检验其是否适用于农业。利用 CaO:MgAl2O4 修饰的碳浆电极,通过循环伏安法(CV)和电化学阻抗谱法(EIS)检验了所制备纳米复合材料的电化学储能和传感应用。总之,合成的 CaO:MgAl2O4 纳米复合材料表现出了良好的形态和结构特征、高效的光催化活性以及在电化学储能方面的潜在应用,突显了其在各种技术和环境应用中的多功能性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Exploring the diverse applications of sol–gel synthesized CaO:MgAl2O4 nanocomposite: morphological, photocatalytic, and electrochemical perspectives

Exploring the diverse applications of sol–gel synthesized CaO:MgAl2O4 nanocomposite: morphological, photocatalytic, and electrochemical perspectives

A nanocomposite of CaO:MgAl2O4 was synthesized through a straightforward and cost-effective sol–gel method. The investigation of the novel CaO:MgAl2O4 nanocomposite encompassed an examination of its morphological and structural alterations, as well as an exploration of its photocatalytic activities and electrochemical characteristics. XRD analysis revealed a nanocomposite size of 24.15 nm. The band gap, determined through UV studies, was found to be 3.83 eV, and scanning electron microscopy (SEM) illustrated flake-like morphological changes in the CaO:MgAl2O4 samples. TEM, HRTEM, and SAED studies of a CaO:MgAl2O4 nanocomposite would reveal important details about its morphology, crystallography, and nanostructure. Photocatalytic activity was quantified by studying the degradation of Acid Red-88 (AR-88) dye in a deionized solution, achieving a 70% dye degradation under UV irradiation in 120 min. Plant growth examinations were carried out using dye degraded water to test its suitability for agriculture. The electrochemical energy storage and sensing applications of the prepared nanocomposite were examined using CaO:MgAl2O4 modified carbon paste electrode through cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS). In conclusion, the synthesized CaO:MgAl2O4 nanocomposite demonstrated promising morphological and structural characteristics, efficient photocatalytic activity, and potential applications in electrochemical energy storage, highlighting its versatility for various technological and environmental applications.

Graphical abstract

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来源期刊
Nanoscale Research Letters
Nanoscale Research Letters 工程技术-材料科学:综合
CiteScore
11.30
自引率
0.00%
发文量
110
审稿时长
48 days
期刊介绍: Nanoscale Research Letters (NRL) provides an interdisciplinary forum for communication of scientific and technological advances in the creation and use of objects at the nanometer scale. NRL is the first nanotechnology journal from a major publisher to be published with Open Access.
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