搅动运动辅助气泡去除:提高 PDMS 混合物质量的低成本方法

IF 4.3 3区 化学 Q2 CHEMISTRY, MULTIDISCIPLINARY
Anoop Kanjirakat, Naresh Kumar Mani* and Dolfred Vijay Fernandes*, 
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引用次数: 0

摘要

在制备聚二甲基硅氧烷(PDMS)的基础弹性体和固化剂混合过程中,气泡的形成是一项重大挑战,传统的解决方法是真空脱气或离心分离。本研究介绍了一种去除 PDMS 混合物中气泡的新型替代方法:受工业乳品分离工艺启发的搅动运动。为此,我们开发了一种低成本、手动操作、自己动手(DIY)的搅动装置。我们研究了三种不同的搅动速度和两种不同粘度的 PDMS 混合物在消除气泡方面的效果。通过分析搅动过程中捕捉到的图像,对该方法的功效进行了定量评估。结果表明,在粘度较高的 PDMS 混合物中,由于气泡凝聚作用增强,气泡去除效率明显更高。在测试的速度中,快速搅动是最有效的,在不到 100 秒的时间内就能去除气泡,明显优于传统的真空脱气方法,后者需要 3000 秒以上。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Churning-Motion-Assisted Bubble Removal: A Low-Cost Approach for Enhancing PDMS Mixture Quality

Churning-Motion-Assisted Bubble Removal: A Low-Cost Approach for Enhancing PDMS Mixture Quality

Bubble formation during mixing of the base elastomer and the curing agent for polydimethylsiloxane (PDMS) preparation presents a significant challenge, traditionally addressed through vacuum degassing or centrifugation. This study introduces a novel alternative for bubble removal in PDMS mixtures: a churning motion inspired by industrial dairy separation processes. A low-cost, manually operated, do-it-yourself (DIY) churning device has been developed for this purpose. We investigate the effectiveness of churning in eliminating bubbles across three different churning speeds and two PDMS mixtures with differing viscosities. The efficacy of this method is quantitatively assessed through the analysis of images captured during the churning process. The results demonstrate that bubble removal is notably more efficient in the PDMS mixture with a higher viscosity due to enhanced bubble coalescence. Among the tested speeds, fast churning emerges as the most effective, achieving bubble removal in less than 100 s─significantly outperforming the traditional vacuum degassing method, which requires over 3000 s. These findings highlight churning motion as a rapid, efficient, and cost-effective alternative for bubble removal in PDMS processing, promising significant advancements in material preparation techniques.

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来源期刊
ACS Omega
ACS Omega Chemical Engineering-General Chemical Engineering
CiteScore
6.60
自引率
4.90%
发文量
3945
审稿时长
2.4 months
期刊介绍: ACS Omega is an open-access global publication for scientific articles that describe new findings in chemistry and interfacing areas of science, without any perceived evaluation of immediate impact.
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