{"title":"三重包晶氧化物 La3Mn2FeO9 的微结构、形态和磁性特征","authors":"Raghad K. Aljurays, Aicha Loucif","doi":"10.1134/S1063783424600663","DOIUrl":null,"url":null,"abstract":"<p>Triple perovskite La<sub>3</sub>Mn<sub>2</sub>FeO<sub>9</sub> powder was synthesized via the sol gel method. The microstructural, morphological and magnetic features of the prepared perovskite sample were examined by means of X‑ray diffraction (XRD), filed-emission scanning electron microscopy (FE-SEM), and vibrating sample magnetometry (VSM). The XRD pattern was refined using the MAUD software based on the Rietveld program. The results confirmed that the sample crystallized in a trigonal structure, with a crystallite size measuring approximately 257 ± 5 nm and a microstrain of about 0.16%. The FE-SEM image revealed spherical like-particles with an average grain size in the vicinity of 514 nm. The VSM curve revealed that the prepared La<sub>3</sub>Mn<sub>2</sub>FeO<sub>9</sub> powder exhibited a ferromagnetic behavior, and subsequent fitting using the law of approach to saturation revealed a saturation magnetization of 1.156438 ± 0.00384 emu/g.</p>","PeriodicalId":731,"journal":{"name":"Physics of the Solid State","volume":"66 6","pages":"165 - 168"},"PeriodicalIF":0.9000,"publicationDate":"2024-08-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstructural, Morphological, and Magnetic Features of the Triple Perovskite Oxide La3Mn2FeO9\",\"authors\":\"Raghad K. Aljurays, Aicha Loucif\",\"doi\":\"10.1134/S1063783424600663\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Triple perovskite La<sub>3</sub>Mn<sub>2</sub>FeO<sub>9</sub> powder was synthesized via the sol gel method. The microstructural, morphological and magnetic features of the prepared perovskite sample were examined by means of X‑ray diffraction (XRD), filed-emission scanning electron microscopy (FE-SEM), and vibrating sample magnetometry (VSM). The XRD pattern was refined using the MAUD software based on the Rietveld program. The results confirmed that the sample crystallized in a trigonal structure, with a crystallite size measuring approximately 257 ± 5 nm and a microstrain of about 0.16%. The FE-SEM image revealed spherical like-particles with an average grain size in the vicinity of 514 nm. The VSM curve revealed that the prepared La<sub>3</sub>Mn<sub>2</sub>FeO<sub>9</sub> powder exhibited a ferromagnetic behavior, and subsequent fitting using the law of approach to saturation revealed a saturation magnetization of 1.156438 ± 0.00384 emu/g.</p>\",\"PeriodicalId\":731,\"journal\":{\"name\":\"Physics of the Solid State\",\"volume\":\"66 6\",\"pages\":\"165 - 168\"},\"PeriodicalIF\":0.9000,\"publicationDate\":\"2024-08-07\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Physics of the Solid State\",\"FirstCategoryId\":\"101\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1063783424600663\",\"RegionNum\":4,\"RegionCategory\":\"物理与天体物理\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, CONDENSED MATTER\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Physics of the Solid State","FirstCategoryId":"101","ListUrlMain":"https://link.springer.com/article/10.1134/S1063783424600663","RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, CONDENSED MATTER","Score":null,"Total":0}
Microstructural, Morphological, and Magnetic Features of the Triple Perovskite Oxide La3Mn2FeO9
Triple perovskite La3Mn2FeO9 powder was synthesized via the sol gel method. The microstructural, morphological and magnetic features of the prepared perovskite sample were examined by means of X‑ray diffraction (XRD), filed-emission scanning electron microscopy (FE-SEM), and vibrating sample magnetometry (VSM). The XRD pattern was refined using the MAUD software based on the Rietveld program. The results confirmed that the sample crystallized in a trigonal structure, with a crystallite size measuring approximately 257 ± 5 nm and a microstrain of about 0.16%. The FE-SEM image revealed spherical like-particles with an average grain size in the vicinity of 514 nm. The VSM curve revealed that the prepared La3Mn2FeO9 powder exhibited a ferromagnetic behavior, and subsequent fitting using the law of approach to saturation revealed a saturation magnetization of 1.156438 ± 0.00384 emu/g.
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Presents the latest results from Russia’s leading researchers in condensed matter physics at the Russian Academy of Sciences and other prestigious institutions. Covers all areas of solid state physics including solid state optics, solid state acoustics, electronic and vibrational spectra, phase transitions, ferroelectricity, magnetism, and superconductivity. Also presents review papers on the most important problems in solid state physics.
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