优化 Sasa quelpaertensis Nakai 的提取，开发具有抗氧化和美白活性的天然化妆品

IF 1.3 4区农林科学 Q2 MATERIALS SCIENCE, PAPER & WOOD

Bioresources Pub Date : 2024-07-24 DOI:10.15376/biores.19.3.6427-6443

Eun-Hye Han, Hyeyun Kim, Jaemin Jo, Su-Yeon Lee, Bonwook Koo

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引用次数: 0

摘要

采用响应面方法（RSM）对提取程序进行了优化，以提高中井莎莎提取物的抗氧化活性和美白效果。中心复合设计是 RSM 的一个组成部分，它分别对乙醇提取物的抗氧化活性和热水提取物的美白效果进行了优化和验证。抗氧化和美白活性通过 DPPH 和酪氨酸酶抑制实验进行测定。与其他因素相比，乙醇浓度（p = 0.0344）对抗氧化活性的影响更大。抗氧化效果的最佳条件是乙醇浓度为 54%，温度为 52 °C，提取时间为 3 小时，抗氧化活性为 83.65±1.56%。另一方面，与其他因素相比，超声波照射时间对美白效果有显著影响（p = 0.0175）。最佳增白条件为 41 ℃、样品与溶剂的比例为 1:19、超声波照射 8 分钟，酪氨酸酶抑制活性为 51.00±1.80%。通过高效液相色谱（HPLC）分析，确定了优化条件下具有抗氧化活性的三嗪类化合物和具有美白效果的对香豆酸、熊果苷等化合物。结果表明，优化后的 S. quelpaertensis 提取物可用作有益的药妆材料。

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Optimizing the extraction of Sasa quelpaertensis Nakai to develop natural cosmetics with antioxidant and whitening activities

Optimization of the extraction procedure was performed to enhance the antioxidant activity and whitening effect of Sasa quelpaertensis Nakai extract using response surface methodology (RSM). The central composite design, a component of RSM, was utilized to optimize and validate the ethanol extract for antioxidant activity and the hot water extract for the whitening effect, respectively. Activities of antioxidant and whitening were determined by DPPH and tyrosinase inhibition assays. The antioxidant activity was notably influenced by ethanol concentration (p = 0.0344) more than other factors. The optimal conditions for the antioxidant effect were 54% ethanol concentration, 52 °C, and 3 h extraction time, yielding an antioxidant activity of 83.65±1.56%. On the other hand, the whitening effect was significantly impacted by ultrasonic irradiation time (p = 0.0175) compared to other factors. The optimal conditions for whitening were 41 °C, 1:19 of sample-to-solvent ratio, and 8 min of ultrasonic irradiation, achieving a tyrosinase inhibition activity of 51.00±1.80%. High-performance liquid chromatography (HPLC) analysis was conducted to identify compounds such as tricin with antioxidant activity and p-coumaric acid, arbutin with whitening effect under the optimized conditions. The results suggest that the optimized extracts from S. quelpaertensis could be utilized as beneficial cosmeceutical materials.

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来源期刊

Bioresources 工程技术-材料科学：纸与木材

CiteScore

2.90

自引率

13.30%

发文量

397

审稿时长

2.3 months

期刊介绍： The purpose of BioResources is to promote scientific discourse and to foster scientific developments related to sustainable manufacture involving lignocellulosic or woody biomass resources, including wood and agricultural residues. BioResources will focus on advances in science and technology. Emphasis will be placed on bioproducts, bioenergy, papermaking technology, wood products, new manufacturing materials, composite structures, and chemicals derived from lignocellulosic biomass.