{"title":"确定微注塑成型过程中聚合物熔体压力相关特性的新方法","authors":"","doi":"10.1016/j.polymertesting.2024.108520","DOIUrl":null,"url":null,"abstract":"<div><p>Micro injection molding is used to manufacture thin-walled parts with micron-scale structures. wherein high shear rate and high injection pressure process conditions appear. Consequently, the pressure dependence of polymer melt viscosity at the microscale cannot be ignored. However, in the simulation analysis of the microinjection molding process, almost all the Cross-WLF models of polymeric materials are omitting the pressure dependence parameter <em>D</em><sub><em>3</em></sub>. This has a huge impact on the accuracy of the simulation results. Herein, a method that combines experimental characterization and filling simulation is proposed for the determination of the pressure dependence of polymer melts during micro injection molding. <em>D</em><sub><em>3</em></sub> in the Cross-WLF model of Polymethyl methacrylate (PMMA) and Cycloolefin copolymer (COC) is characterized by capillary rheometer and counter pressure chamber. The developed viscosity model including <em>D</em><sub><em>3</em></sub> is used for a filling simulation and is compared with the experimental results. The model flow simulation results showcases that the prediction accuracy of the viscosity model is significantly improved after considering <em>D</em><sub><em>3</em></sub>. These results are of great significance, as they can be used to reduce the development cost and to improve the simulation accuracy of the micro injection molding filling process.</p></div>","PeriodicalId":20628,"journal":{"name":"Polymer Testing","volume":null,"pages":null},"PeriodicalIF":5.0000,"publicationDate":"2024-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S0142941824001971/pdfft?md5=62fd89ad6b26fc72f80e01cc36df7d13&pid=1-s2.0-S0142941824001971-main.pdf","citationCount":"0","resultStr":"{\"title\":\"A novel method for determining the pressure dependent characteristics of polymer melt during micro injection molding\",\"authors\":\"\",\"doi\":\"10.1016/j.polymertesting.2024.108520\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Micro injection molding is used to manufacture thin-walled parts with micron-scale structures. wherein high shear rate and high injection pressure process conditions appear. Consequently, the pressure dependence of polymer melt viscosity at the microscale cannot be ignored. However, in the simulation analysis of the microinjection molding process, almost all the Cross-WLF models of polymeric materials are omitting the pressure dependence parameter <em>D</em><sub><em>3</em></sub>. This has a huge impact on the accuracy of the simulation results. Herein, a method that combines experimental characterization and filling simulation is proposed for the determination of the pressure dependence of polymer melts during micro injection molding. <em>D</em><sub><em>3</em></sub> in the Cross-WLF model of Polymethyl methacrylate (PMMA) and Cycloolefin copolymer (COC) is characterized by capillary rheometer and counter pressure chamber. The developed viscosity model including <em>D</em><sub><em>3</em></sub> is used for a filling simulation and is compared with the experimental results. The model flow simulation results showcases that the prediction accuracy of the viscosity model is significantly improved after considering <em>D</em><sub><em>3</em></sub>. These results are of great significance, as they can be used to reduce the development cost and to improve the simulation accuracy of the micro injection molding filling process.</p></div>\",\"PeriodicalId\":20628,\"journal\":{\"name\":\"Polymer Testing\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":5.0000,\"publicationDate\":\"2024-07-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.sciencedirect.com/science/article/pii/S0142941824001971/pdfft?md5=62fd89ad6b26fc72f80e01cc36df7d13&pid=1-s2.0-S0142941824001971-main.pdf\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Polymer Testing\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0142941824001971\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Polymer Testing","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0142941824001971","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
A novel method for determining the pressure dependent characteristics of polymer melt during micro injection molding
Micro injection molding is used to manufacture thin-walled parts with micron-scale structures. wherein high shear rate and high injection pressure process conditions appear. Consequently, the pressure dependence of polymer melt viscosity at the microscale cannot be ignored. However, in the simulation analysis of the microinjection molding process, almost all the Cross-WLF models of polymeric materials are omitting the pressure dependence parameter D3. This has a huge impact on the accuracy of the simulation results. Herein, a method that combines experimental characterization and filling simulation is proposed for the determination of the pressure dependence of polymer melts during micro injection molding. D3 in the Cross-WLF model of Polymethyl methacrylate (PMMA) and Cycloolefin copolymer (COC) is characterized by capillary rheometer and counter pressure chamber. The developed viscosity model including D3 is used for a filling simulation and is compared with the experimental results. The model flow simulation results showcases that the prediction accuracy of the viscosity model is significantly improved after considering D3. These results are of great significance, as they can be used to reduce the development cost and to improve the simulation accuracy of the micro injection molding filling process.
期刊介绍:
Polymer Testing focuses on the testing, analysis and characterization of polymer materials, including both synthetic and natural or biobased polymers. Novel testing methods and the testing of novel polymeric materials in bulk, solution and dispersion is covered. In addition, we welcome the submission of the testing of polymeric materials for a wide range of applications and industrial products as well as nanoscale characterization.
The scope includes but is not limited to the following main topics:
Novel testing methods and Chemical analysis
• mechanical, thermal, electrical, chemical, imaging, spectroscopy, scattering and rheology
Physical properties and behaviour of novel polymer systems
• nanoscale properties, morphology, transport properties
Degradation and recycling of polymeric materials when combined with novel testing or characterization methods
• degradation, biodegradation, ageing and fire retardancy
Modelling and Simulation work will be only considered when it is linked to new or previously published experimental results.