{"title":"通过芳基乙二醛衍生物、芳基胺和吡唑酮的三组分反应高效合成新的吡唑酮取代的 C-酰亚胺衍生物","authors":"M. Anary‐Abbasinejad, Maryam Oudi","doi":"10.24820/ark.5550190.p012.219","DOIUrl":null,"url":null,"abstract":"An effective protocol for synthesis of some new pyrazolone-substituted C-acylimine derivatives is reported through a one-pot three-component reaction between arylglyoxals, aniline derivatives and pyrazolone. All reactions were conducted in ethanol/acetic acid mixture as solvent and the stable products were obtained by simple filtering off the precipitated solids in high yields. The structures of all products were proved by 1 H and 13 C NMR and IR spectral and elemental analysis data","PeriodicalId":8432,"journal":{"name":"Arkivoc","volume":null,"pages":null},"PeriodicalIF":0.8000,"publicationDate":"2024-07-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"An efficient synthesis of new pyrazolone-substituted C-acylimine derivatives by three-component reaction between arylglyoxal derivatives, arylamines and pyrazolone\",\"authors\":\"M. Anary‐Abbasinejad, Maryam Oudi\",\"doi\":\"10.24820/ark.5550190.p012.219\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"An effective protocol for synthesis of some new pyrazolone-substituted C-acylimine derivatives is reported through a one-pot three-component reaction between arylglyoxals, aniline derivatives and pyrazolone. All reactions were conducted in ethanol/acetic acid mixture as solvent and the stable products were obtained by simple filtering off the precipitated solids in high yields. The structures of all products were proved by 1 H and 13 C NMR and IR spectral and elemental analysis data\",\"PeriodicalId\":8432,\"journal\":{\"name\":\"Arkivoc\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.8000,\"publicationDate\":\"2024-07-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Arkivoc\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://doi.org/10.24820/ark.5550190.p012.219\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Arkivoc","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.24820/ark.5550190.p012.219","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}
引用次数: 0
摘要
通过芳基乙二醛、苯胺衍生物和吡唑酮之间的单锅三组分反应,报告了合成一些新的吡唑酮取代的 C-酰亚胺衍生物的有效方案。所有反应均在乙醇/乙酸混合溶剂中进行,只需过滤掉沉淀的固体,即可获得稳定的高产率产物。所有产物的结构均通过 1 H 和 13 C NMR、IR 光谱和元素分析数据得到证实。
An efficient synthesis of new pyrazolone-substituted C-acylimine derivatives by three-component reaction between arylglyoxal derivatives, arylamines and pyrazolone
An effective protocol for synthesis of some new pyrazolone-substituted C-acylimine derivatives is reported through a one-pot three-component reaction between arylglyoxals, aniline derivatives and pyrazolone. All reactions were conducted in ethanol/acetic acid mixture as solvent and the stable products were obtained by simple filtering off the precipitated solids in high yields. The structures of all products were proved by 1 H and 13 C NMR and IR spectral and elemental analysis data
期刊介绍:
Arkivoc publishes full papers (not accounts) describing sound original work that is of interest to organic chemists (in areas of synthetic organic chemistry, bio-organic, organometallic, theoretical, and physical organic chemistry:
General Papers describing sound original work
Reviews and Accounts of selected topics
Honorary Issues - Pay tribute to distinguished organic chemists (invited contributions)
Thematic Issues - Cover important current topics in organic chemistry
Regional Issues - Recognize organic chemistry in various countries.