Kirill A. Gomonov, Vasilii V. Pelipko, Igor A. Litvinov, Ruslan I. Baichurin, Sergey V. Makarenko
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Nuclear Overhauser Effect in Determining the Configuration of 2-Nitrofuran-3-Carboxylates Hydrazones
The structure of 4-acetyl-2-nitrofuran-3-carboxylates hydrazones obtained from the interaction of 4-acetyl-5-methyl-2-nitrofuran-3-carboxylates with substituted hydrazines was studied using 1D and 2D 1H, 13C NMR spectroscopy. According to 1H–1H NOESY data, it was shown that the hydrazones under consideration exist in the E-configuration, confirmed by X-ray diffraction analysis.
期刊介绍:
Applied Magnetic Resonance provides an international forum for the application of magnetic resonance in physics, chemistry, biology, medicine, geochemistry, ecology, engineering, and related fields.
The contents include articles with a strong emphasis on new applications, and on new experimental methods. Additional features include book reviews and Letters to the Editor.