Ahmed Altarazi, Julfikar Haider, Abdulaziz Alhotan, Nick Silikas, Hugh Devlin
{"title":"人工老化对通过 3D 打印制作的义齿基底材料的物理和机械特性的影响。","authors":"Ahmed Altarazi, Julfikar Haider, Abdulaziz Alhotan, Nick Silikas, Hugh Devlin","doi":"10.1155/2024/8060363","DOIUrl":null,"url":null,"abstract":"<p><p>Three-dimensional (3D) printing is becoming more prevalent in the dental sector due to its potential to save time for dental practitioners, streamline fabrication processes, enhance precision and consistency in fabricating prosthetic models, and offer cost-effective solutions. However, the effect of aging in artificial saliva of this type of material has not been explored. To assess the physical and mechanical properties of the two types of 3D-printed materials before and after being subjected to artificial saliva, a total of 219 acrylic resin specimens were produced. These specimens were made with two types of 3D-printed materials, namely, NextDent (ND) and Formlabs (FLs), and a Schottlander heat-cured (HC) resin material that was used as a control. Water sorption and solubility specimens (<i>n</i> = 5) were tested after three months of storage in artificial saliva. Moreover, the Vickers hardness, Martens hardness, flexural strength/modulus, and impact strength were evaluated both under dry conditions and after three months of storage in artificial saliva. The degree of conversion (DC), elemental analysis, and filler content were also investigated. The ANOVA showed that 3D-printed resins had significantly greater sorption than the control group (<i>p</i> < 0.05). However, the flexural strength values of the 3D-printed materials were significantly greater (<i>p</i> < 0.05) than those of the heat-cured material. The DC of the 3D-printed resins was lower than that of the control group, but the difference was not significant (<i>p</i> > 0.05). The 3D-printed materials contained significantly more filler than the control (<i>p</i> < 0.05). Moreover, the artificial saliva had a significant effect on the Vickers hardness for all tested groups and on the Martens hardness for the control group only (<i>p</i> < 0.05). Compared with conventional heat-cured materials, 3D-printed denture base materials demonstrated relatively poorer performance in terms of sorption, solubility, and DC but exhibited either comparable or superior mechanical properties. The aging process also influenced the Vickers and Martens' hardness. The strength of the 3D-printed materials was in compliance with ISO recommendations, and the materials could be used alongside conventional heat-cured materials.</p>","PeriodicalId":13704,"journal":{"name":"International Journal of Biomaterials","volume":"2024 ","pages":"8060363"},"PeriodicalIF":3.0000,"publicationDate":"2024-06-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11199068/pdf/","citationCount":"0","resultStr":"{\"title\":\"Impact of Artificial Aging on the Physical and Mechanical Characteristics of Denture Base Materials Fabricated via 3D Printing.\",\"authors\":\"Ahmed Altarazi, Julfikar Haider, Abdulaziz Alhotan, Nick Silikas, Hugh Devlin\",\"doi\":\"10.1155/2024/8060363\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>Three-dimensional (3D) printing is becoming more prevalent in the dental sector due to its potential to save time for dental practitioners, streamline fabrication processes, enhance precision and consistency in fabricating prosthetic models, and offer cost-effective solutions. However, the effect of aging in artificial saliva of this type of material has not been explored. To assess the physical and mechanical properties of the two types of 3D-printed materials before and after being subjected to artificial saliva, a total of 219 acrylic resin specimens were produced. These specimens were made with two types of 3D-printed materials, namely, NextDent (ND) and Formlabs (FLs), and a Schottlander heat-cured (HC) resin material that was used as a control. Water sorption and solubility specimens (<i>n</i> = 5) were tested after three months of storage in artificial saliva. Moreover, the Vickers hardness, Martens hardness, flexural strength/modulus, and impact strength were evaluated both under dry conditions and after three months of storage in artificial saliva. The degree of conversion (DC), elemental analysis, and filler content were also investigated. The ANOVA showed that 3D-printed resins had significantly greater sorption than the control group (<i>p</i> < 0.05). However, the flexural strength values of the 3D-printed materials were significantly greater (<i>p</i> < 0.05) than those of the heat-cured material. The DC of the 3D-printed resins was lower than that of the control group, but the difference was not significant (<i>p</i> > 0.05). The 3D-printed materials contained significantly more filler than the control (<i>p</i> < 0.05). Moreover, the artificial saliva had a significant effect on the Vickers hardness for all tested groups and on the Martens hardness for the control group only (<i>p</i> < 0.05). Compared with conventional heat-cured materials, 3D-printed denture base materials demonstrated relatively poorer performance in terms of sorption, solubility, and DC but exhibited either comparable or superior mechanical properties. The aging process also influenced the Vickers and Martens' hardness. The strength of the 3D-printed materials was in compliance with ISO recommendations, and the materials could be used alongside conventional heat-cured materials.</p>\",\"PeriodicalId\":13704,\"journal\":{\"name\":\"International Journal of Biomaterials\",\"volume\":\"2024 \",\"pages\":\"8060363\"},\"PeriodicalIF\":3.0000,\"publicationDate\":\"2024-06-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11199068/pdf/\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Biomaterials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1155/2024/8060363\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2024/1/1 0:00:00\",\"PubModel\":\"eCollection\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, BIOMATERIALS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Biomaterials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1155/2024/8060363","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2024/1/1 0:00:00","PubModel":"eCollection","JCR":"Q3","JCRName":"MATERIALS SCIENCE, BIOMATERIALS","Score":null,"Total":0}
引用次数: 0
摘要
三维(3D)打印技术可以为牙科医生节省时间、简化制作流程、提高制作修复模型的精度和一致性,并提供具有成本效益的解决方案,因此在牙科领域正变得越来越普遍。然而,这类材料在人工唾液中的老化效应尚未得到研究。为了评估两种 3D 打印材料在人工唾液中老化前后的物理和机械性能,共制作了 219 个丙烯酸树脂试样。这些试样由两种 3D 打印材料制成,即 NextDent(ND)和 Formlabs(FLs),以及作为对照的 Schottlander 热固化(HC)树脂材料。在人工唾液中存放三个月后,对吸水性和溶解性试样(n = 5)进行了测试。此外,还对干燥条件下和在人工唾液中存放三个月后的维氏硬度、马氏硬度、抗弯强度/模量和冲击强度进行了评估。此外,还对转化率(DC)、元素分析和填料含量进行了研究。方差分析结果表明,三维打印树脂的吸附力明显高于对照组(p < 0.05)。不过,三维打印材料的抗弯强度值明显高于热固化材料(p < 0.05)。三维打印树脂的直流电低于对照组,但差异不显著(p > 0.05)。三维打印材料所含的填料明显多于对照组(p < 0.05)。此外,人工唾液对所有测试组的维氏硬度都有显著影响,仅对对照组的马氏硬度有显著影响(p < 0.05)。与传统的热固化材料相比,三维打印义齿基底材料在吸附性、溶解性和直流电方面的性能相对较差,但在机械性能方面却具有可比性或优越性。老化过程也会影响维氏硬度和马氏硬度。三维打印材料的强度符合 ISO 建议,可与传统热固化材料一起使用。
Impact of Artificial Aging on the Physical and Mechanical Characteristics of Denture Base Materials Fabricated via 3D Printing.
Three-dimensional (3D) printing is becoming more prevalent in the dental sector due to its potential to save time for dental practitioners, streamline fabrication processes, enhance precision and consistency in fabricating prosthetic models, and offer cost-effective solutions. However, the effect of aging in artificial saliva of this type of material has not been explored. To assess the physical and mechanical properties of the two types of 3D-printed materials before and after being subjected to artificial saliva, a total of 219 acrylic resin specimens were produced. These specimens were made with two types of 3D-printed materials, namely, NextDent (ND) and Formlabs (FLs), and a Schottlander heat-cured (HC) resin material that was used as a control. Water sorption and solubility specimens (n = 5) were tested after three months of storage in artificial saliva. Moreover, the Vickers hardness, Martens hardness, flexural strength/modulus, and impact strength were evaluated both under dry conditions and after three months of storage in artificial saliva. The degree of conversion (DC), elemental analysis, and filler content were also investigated. The ANOVA showed that 3D-printed resins had significantly greater sorption than the control group (p < 0.05). However, the flexural strength values of the 3D-printed materials were significantly greater (p < 0.05) than those of the heat-cured material. The DC of the 3D-printed resins was lower than that of the control group, but the difference was not significant (p > 0.05). The 3D-printed materials contained significantly more filler than the control (p < 0.05). Moreover, the artificial saliva had a significant effect on the Vickers hardness for all tested groups and on the Martens hardness for the control group only (p < 0.05). Compared with conventional heat-cured materials, 3D-printed denture base materials demonstrated relatively poorer performance in terms of sorption, solubility, and DC but exhibited either comparable or superior mechanical properties. The aging process also influenced the Vickers and Martens' hardness. The strength of the 3D-printed materials was in compliance with ISO recommendations, and the materials could be used alongside conventional heat-cured materials.