MAX 相的进步:合成、表征和挑战

IF 1.8 Q3 COMPUTER SCIENCE, INTERDISCIPLINARY APPLICATIONS
Md. Shahinoor Alam, Mohammad Asaduzzaman Chowdhury, Md. Arefin Kowser, Md. Saiful Islam, Md. Moynul Islam, Tasmina Khandaker
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引用次数: 0

摘要

MAX 相及其 MXene 化合物因其广泛的潜在应用而备受关注。MAX 相的质量和纯度保证了 MXene 产品的理想质量,这对于包括能量存储、催化和电气设备在内的各种应用至关重要。由于 MAX 相的纯度、质量、复杂结构以及无法获得商业纯 MAX 粉末,因此经常需要对预期的 MAX 产品采用复杂的合成和表征技术。进入这一领域的许多研究人员都在寻求一种综合方法来合成和表征 MAX 相。尽管如此,很大一部分现有综述都忽略了 MAX 相的合成和表征方法,尤其是在讨论 MXenes 时。因此,本综述旨在全面概述 MAX 相通常需要的各种合成方法和表征技术。本综述还讨论了各种合成技术,包括其优缺点。研究发现,表征技术,尤其是 X 射线衍射 (XRD) 对新研究人员来说至关重要。然而,其他技术的整合,如扫描电子显微镜、透射电子显微镜、X 射线光电子能谱和红外分析等,可以增强和补充 X 射线衍射的研究结果。本综述还强调了与 MAX 相合成相关的挑战,并提出了潜在的解决方案,同时强调要评估它们在广泛应用中的适用性。总之,本综述为从事 MAX 相探索和应用的研究人员提供了全面的资源和指南,强调了合成和表征的基本技术,以利用其巨大潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Advances of MAX phases: Synthesis, characterizations and challenges

Advances of MAX phases: Synthesis, characterizations and challenges

MAX phases and their MXene compounds have received significant attention owing to their extensive potential applications. The quality and purity of the MAX phase guarantee the desired quality of the MXene product, which is essential for a variety of applications, including energy storage, catalysis, and electrical devices. Due to the purity, quality, complex structure, and unavailable commercial pure MAX powders, it is frequently required to have sophisticated synthesis and characterization techniques for the expected MAX products. Many researchers entering this field seek a comprehensive approach to the synthesis and characterization of MAX phases. Despite this, a significant portion of existing reviews have overlooked the synthesis and characterization methods specific to MAX phases, particularly when addressing MXenes. Consequently, this review aims to offer a thorough overview of the various synthesis methods and characterization techniques that are often required for MAX phases. In this review, various synthesis techniques, including their advantages and disadvantages, have also been discussed. Characterization techniques, especially x-ray diffraction (XRD), were found to be quite critical for new researchers. However, the integration of other techniques such as scanning electron microscopy, transmission electron microscopy, x-ray photoelectron spectroscopy, and infrared analysis enhances and complements the findings obtained through XRD. The review also underscores the challenges associated with MAX phase synthesis and proposes potential solutions, emphasizing the assessment of their suitability across a broad spectrum of applications. Overall, this review serves as a comprehensive resource and guide for researchers engaged in the exploration and application of MAX phases, emphasizing the essential techniques of synthesis and characterization in harnessing their massive potential.

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CiteScore
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