美元法沉积时间对氧化锌特性的影响

N. Madaoui, M. Azibi, I. Djabrouhou, N. Saoula
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引用次数: 0

摘要

这项研究旨在通过沉积氧化锌薄膜来改善 304 L 不锈钢(SS)基底的性能,以用于腐蚀、机械和生物医学应用。采用超声喷涂技术制备氧化锌薄膜,沉积时间分别为 1、4 和 9 分钟。XRD 和拉曼研究了氧化锌样品的表面特征。XRD 分析表明,氧化锌呈六边形结构,平均结晶尺寸为 22 纳米。纳米压痕测量表明,受检薄膜的硬度有所提高。为了确定导电类型和估计电荷载流子密度,进行了电位极化、电化学阻抗光谱(EIS)和莫特-肖特基分析。结果发现,沉积 9 分钟的薄膜在提高耐腐蚀性方面最为有效。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effect of deposition time on properties of the ZnO by USD Method
This investigation aims to improve the properties of 304 L stainless steel (SS) substrates for use in corrosion, mechanical, and biomedical applications by depositing ZnO thin films. The ultrasonic spraying technique was used to prepare ZnO thin films with depositional times of 1, 4, and 9 minutes. XRD and Raman studied the surface characteristics of ZnO samples. XRD analysis revealed a hexagonal structure with an average crystallite size of 22 nm for ZnO. Indentation nano measurements indicated an increase in the hardness of the films examined. To determine the type of conductivity and estimate the charge carrier density, potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and Mott-Schottky analysis were performed. The thin film deposited for 9 minutes was found to be the most effective in improving corrosion resistance.
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