在带漩涡流的微反应器中合成钇铝石榴石前驱体

IF 0.8 4区材料科学 Q4 MATERIALS SCIENCE, CERAMICS

Glass Physics and Chemistry Pub Date : 2024-03-08 DOI:10.1134/S1087659623600989

A. V. Zdravkov, Yu. S. Kudryashova, R. Sh. Abiev, N. N. Khimich

{"title":"在带漩涡流的微反应器中合成钇铝石榴石前驱体","authors":"A. V. Zdravkov, Yu. S. Kudryashova, R. Sh. Abiev, N. N. Khimich","doi":"10.1134/S1087659623600989","DOIUrl":null,"url":null,"abstract":"Nanosized yttrium–aluminum garnet (YAG) powders are synthesized in a microreactor with swirling flows by the coprecipitation of yttrium and aluminum hydroxides followed by heat treatment. The resulting mixture of hydroxides is X-ray amorphous according to X-ray phase analysis. Thermal treatment of hydroxides at 1100°C for 1 h leads to the formation of Y3Al5O12 nanocrystals. The method we developed is technologically advanced, easily scalable, saves energy and time, and does not require labor-intensive operati-ons.","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 1 supplement","pages":"S71 - S76"},"PeriodicalIF":0.8000,"publicationDate":"2024-03-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of Yttrium–Aluminum Garnet Precursors in a Microreactor with Swirling Flows\",\"authors\":\"A. V. Zdravkov, Yu. S. Kudryashova, R. Sh. Abiev, N. N. Khimich\",\"doi\":\"10.1134/S1087659623600989\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Nanosized yttrium–aluminum garnet (YAG) powders are synthesized in a microreactor with swirling flows by the coprecipitation of yttrium and aluminum hydroxides followed by heat treatment. The resulting mixture of hydroxides is X-ray amorphous according to X-ray phase analysis. Thermal treatment of hydroxides at 1100°C for 1 h leads to the formation of Y3Al5O12 nanocrystals. The method we developed is technologically advanced, easily scalable, saves energy and time, and does not require labor-intensive operati-ons.\",\"PeriodicalId\":580,\"journal\":{\"name\":\"Glass Physics and Chemistry\",\"volume\":\"49 1 supplement\",\"pages\":\"S71 - S76\"},\"PeriodicalIF\":0.8000,\"publicationDate\":\"2024-03-08\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Glass Physics and Chemistry\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1087659623600989\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Glass Physics and Chemistry","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1134/S1087659623600989","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}

引用次数: 0

摘要

摘要纳米钇铝石榴石（YAG）粉末是通过钇和铝的氢氧化物共沉淀，然后进行热处理，在漩涡流的微反应器中合成的。根据 X 射线相分析，所得氢氧化物混合物为 X 射线非晶体。在 1100°C 下对氢氧化物进行 1 小时的热处理，可形成 Y3Al5O12 纳米晶体。我们开发的方法技术先进，易于扩展，节省能源和时间，并且不需要劳动密集型操作。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

Synthesis of Yttrium–Aluminum Garnet Precursors in a Microreactor with Swirling Flows

查看原文本刊更多论文

Synthesis of Yttrium–Aluminum Garnet Precursors in a Microreactor with Swirling Flows

Nanosized yttrium–aluminum garnet (YAG) powders are synthesized in a microreactor with swirling flows by the coprecipitation of yttrium and aluminum hydroxides followed by heat treatment. The resulting mixture of hydroxides is X-ray amorphous according to X-ray phase analysis. Thermal treatment of hydroxides at 1100°C for 1 h leads to the formation of Y₃Al₅O₁₂ nanocrystals. The method we developed is technologically advanced, easily scalable, saves energy and time, and does not require labor-intensive operati-ons.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Glass Physics and Chemistry 工程技术-材料科学：硅酸盐

CiteScore

1.20

自引率

14.30%

发文量

审稿时长

6-12 weeks

期刊介绍： Glass Physics and Chemistry presents results of research on the inorganic and physical chemistry of glass, ceramics, nanoparticles, nanocomposites, and high-temperature oxides and coatings. The journal welcomes manuscripts from all countries in the English or Russian language.