O. K. Kamynina, S. G. Vadchenko, I. D. Kovalev, D. V. Prokhorov, D. E. Andreev, A. N. Nekrasov
{"title":"层状铌-金属陶瓷复合材料","authors":"O. K. Kamynina, S. G. Vadchenko, I. D. Kovalev, D. V. Prokhorov, D. E. Andreev, A. N. Nekrasov","doi":"10.1134/S1027451024020307","DOIUrl":null,"url":null,"abstract":"<p>Layered composite materials based on niobium and cermet are produced via the self-propagating high-temperature synthesis of preliminarily structured samples using metal foils (Ti, Nb, Ta, Ni) and reaction tapes (Ti + 1.7B) and (5Ti + 3Si). The reaction tapes for synthesis are produced by rolling powder mixtures. The microstructure, and elemental and phase compositions of the synthesized multilayer composite materials are studied by scanning electron microscopy and X-ray phase analysis. Particular attention is paid to the formation of intermediate layers and surface modification occurring during combustion. The strength characteristics of the synthesized materials are determined according to the three-point loading scheme at temperatures of 1100°C. Analysis of the obtained materials shows that joining in the combustion mode of metal foils and reaction tapes is provided due to reaction diffusion, mutual impregnation, and chemical reactions occurring in the reaction tapes and on the surface of the metal foils. The formation of thin intermediate layers in the form of cermet and eutectic solutions provides the synthesized multilayer materials with good strength properties up to 87 MPa at 1100°C. These results are of interest for the development of structural materials operating under extreme conditions.</p>","PeriodicalId":671,"journal":{"name":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","volume":"18 2","pages":"445 - 452"},"PeriodicalIF":0.5000,"publicationDate":"2024-05-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Layered Niobium-Cermet Composite Material\",\"authors\":\"O. K. Kamynina, S. G. Vadchenko, I. D. Kovalev, D. V. Prokhorov, D. E. Andreev, A. N. Nekrasov\",\"doi\":\"10.1134/S1027451024020307\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Layered composite materials based on niobium and cermet are produced via the self-propagating high-temperature synthesis of preliminarily structured samples using metal foils (Ti, Nb, Ta, Ni) and reaction tapes (Ti + 1.7B) and (5Ti + 3Si). The reaction tapes for synthesis are produced by rolling powder mixtures. The microstructure, and elemental and phase compositions of the synthesized multilayer composite materials are studied by scanning electron microscopy and X-ray phase analysis. Particular attention is paid to the formation of intermediate layers and surface modification occurring during combustion. The strength characteristics of the synthesized materials are determined according to the three-point loading scheme at temperatures of 1100°C. Analysis of the obtained materials shows that joining in the combustion mode of metal foils and reaction tapes is provided due to reaction diffusion, mutual impregnation, and chemical reactions occurring in the reaction tapes and on the surface of the metal foils. The formation of thin intermediate layers in the form of cermet and eutectic solutions provides the synthesized multilayer materials with good strength properties up to 87 MPa at 1100°C. These results are of interest for the development of structural materials operating under extreme conditions.</p>\",\"PeriodicalId\":671,\"journal\":{\"name\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"volume\":\"18 2\",\"pages\":\"445 - 452\"},\"PeriodicalIF\":0.5000,\"publicationDate\":\"2024-05-07\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1027451024020307\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, CONDENSED MATTER\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1134/S1027451024020307","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, CONDENSED MATTER","Score":null,"Total":0}
Layered composite materials based on niobium and cermet are produced via the self-propagating high-temperature synthesis of preliminarily structured samples using metal foils (Ti, Nb, Ta, Ni) and reaction tapes (Ti + 1.7B) and (5Ti + 3Si). The reaction tapes for synthesis are produced by rolling powder mixtures. The microstructure, and elemental and phase compositions of the synthesized multilayer composite materials are studied by scanning electron microscopy and X-ray phase analysis. Particular attention is paid to the formation of intermediate layers and surface modification occurring during combustion. The strength characteristics of the synthesized materials are determined according to the three-point loading scheme at temperatures of 1100°C. Analysis of the obtained materials shows that joining in the combustion mode of metal foils and reaction tapes is provided due to reaction diffusion, mutual impregnation, and chemical reactions occurring in the reaction tapes and on the surface of the metal foils. The formation of thin intermediate layers in the form of cermet and eutectic solutions provides the synthesized multilayer materials with good strength properties up to 87 MPa at 1100°C. These results are of interest for the development of structural materials operating under extreme conditions.
期刊介绍:
Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.