模拟体液中的腐蚀对三维打印聚乳酸涂层 AM60 镁合金疲劳特性的影响

Surfaces Pub Date : 2024-02-05 DOI:10.3390/surfaces7010007
Seyed Ali Ashraf Talesh, Mohammad Azadi
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引用次数: 0

摘要

本研究评估了带有聚乳酸(PLA)涂层的 AM60 镁合金(PF-AM60-PLA)的纯疲劳行为和带有聚乳酸涂层的镁合金(CF-AM60-PLA)的腐蚀疲劳行为。聚合物涂层是用 3D 打印机通过熔融沉积建模(FDM)制成的,并用胶水粘附在标准疲劳试样上。然后,在模拟体液(SBF)中浸泡 27 天后,对试样进行高循环弯曲疲劳试验。由于腐蚀,试样的重量平均减少了 35%。腐蚀率在最初的 7 天内有所下降,随后有所上升。带有涂层的 PF 样品的疲劳寿命平均延长了 49%。至于 CF 样品,尽管使用了 10 倍强度的溶液,这些样品的疲劳寿命仅减少了 35%。场发射扫描电子显微镜(FESEM)的结果还显示了裂纹板和条纹。此外,还观察到胶水与涂层和镁分离的现象。CF 试样的断裂面上除了微裂纹和孔洞外,还出现了腐蚀产物,这导致了应力集中和裂纹萌生。在通过三维打印制造的聚合物涂层中也观察到了气体释放造成的孔洞。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Impact of Corrosion in Simulated Body Fluid on Fatigue Characteristics of 3D-Printed Polylactic Acid-Coated AM60 Magnesium Alloys
In this research, the pure fatigue behaviors of AM60 magnesium alloy with polylactic acid (PLA) coating (PF-AM60-PLA) and the corrosion fatigue behaviors of magnesium alloy with PLA coating (CF-AM60-PLA) were evaluated. Polymer coating was made by fused deposition modeling (FDM) with a 3D printer and attached to standard fatigue test specimens with glue. Then, after 27 days of immersion in the simulated body fluid (SBF), the high-cycle bending fatigue test was performed on samples. Due to corrosion, the weight of the specimens was reduced by an average of 35%. The corrosion rate decreased in the first 7 days and then increased. PF samples with a coating had an average 49% increase in fatigue lifetime. Regarding the CF samples, despite the use of a 10-times stronger solution, the fatigue lifetime of these samples decreased by only 35%. The field-emission scanning electron microscopy (FESEM) results also showed cleavage plates and striations. In addition, the separation of the glue from the coating and Mg was observed. Corrosion products, in addition to microcracks and holes, were seen on the fracture surface of CF specimens, which caused the stress concentration and the crack initiation. Holes caused by the release of gases were also observed in polymer coatings, which were fabricated by 3D printing.
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