E. Martines-López, D. Cárdenas-García, D. Cywiak-Córdova
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引用次数: 0
摘要
烘箱干燥重量法被广泛应用于固体材料的水分测量,该方法采用的干燥方案包括干燥时间和温度等特定条件。虽然这种方法对许多类型的材料都很可靠,但在某些情况下,含水量高的材料需要在低温下进行预干燥,然后再进行最终干燥。例如,新收获的谷物无法按照典型的干燥方案进行研磨。在这种情况下,干燥过程可以分几个阶段进行,以达到有利的研磨条件。根据含水量的定义,可以推导出采用 N 级干燥法测定含水量的测量模型。在此基础上,本文提出了一个在 N 个阶段中获得水分含量的模型。将该模型应用于玉米和小麦样品的多个阶段的干燥,得到了可比较的结果。根据该模型,样品的水分只取决于初始质量和最后干燥阶段后的质量。通过计算归一化误差,验证了测量结果的等效性。此外,还对不确定性进行了估计。
Measuring Model for the Gravimetric Method by Drying in N-Stages Applied to Materials with High Moisture Content
The gravimetric method by oven drying is widely used for moisture measurement in solid materials following a drying protocol which includes specific conditions such as drying time and temperature. Although this method is reliable for many types of materials, there are some cases where materials with high moisture content require a pre-drying process at low temperature before performing the final drying. Some examples of such materials are freshly harvested grains which cannot be grounded according to the typical drying protocol. In these cases, the drying process can be applied in several stages to reach a favorable grinding condition. The measurement model for the moisture content determination using N-stages of drying can be derived from the definition of moisture content. Based on this, in this paper, a model to obtain the moisture content in N-stages is presented. The model was applied to samples of corn and wheat by drying in several stages, obtaining comparable results. According to this model, the moisture of the sample only depends on the initial mass and the mass after the final drying stage. The equivalence in the measured results was verified calculating the normalized error. Also, the estimation of the uncertainty was carried out.
期刊介绍:
MAPAN-Journal Metrology Society of India is a quarterly publication. It is exclusively devoted to Metrology (Scientific, Industrial or Legal). It has been fulfilling an important need of Metrologists and particularly of quality practitioners by publishing exclusive articles on scientific, industrial and legal metrology.
The journal publishes research communication or technical articles of current interest in measurement science; original work, tutorial or survey papers in any metrology related area; reviews and analytical studies in metrology; case studies on reliability, uncertainty in measurements; and reports and results of intercomparison and proficiency testing.