在无低温超导磁体中进行原子分辨的新颖、紧凑和坚硬的扫描隧穿显微镜。

IF 16.4 1区 化学 Q1 CHEMISTRY, MULTIDISCIPLINARY
Behnam Esmaeilzadeh, Muhammad Touqeer, Liu Junwei, Shaofeng Zheng, Tao Geng, Yubin Hou, Qingyou Lu
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引用次数: 0

摘要

我们介绍了在无低温超导磁体中运行的新型扫描隧道显微镜(STM)的设计和性能。我们自制的 STM 头结构紧凑(长 51.5 毫米,直径 20 毫米),有一个单臂,在针尖和样品之间的扫描区域完全开放。STM 头由两个压电管 (PT) 组成,一个压电扫描管 (PST) 安装在抛光良好的氧化锆轴上,另一个大型 PT 安装在称为电机管的蓝宝石管中。STM 头的主体由钽制成。在这种设计中,我们用螺钉将蓝宝石管固定在框架上,这样就可以快速改变蓝宝石管的位置。为了分析 STM 头单元的刚度,我们通过有限元分析确定了弯曲模式的最低特征频率为 3 和 4 kHz,扭转模式为 8 kHz,纵向模式为 9 kHz,并测量了 X-Y 平面和 Z 方向的低漂移率。我们的结果证实了我们新开发的 STM 的高稳定性、抗振性和对高磁场的不敏感性,以及在物理、化学、材料和生物科学领域研究具有高静态支撑刚度的低频系统的应用潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Atomic resolution imaging using a novel, compact and stiff scanning tunnelling microscope in cryogen-free superconducting magnet

We present the design and performance of a novel scanning tunnelling microscope (STM) operating in a cryogen-free superconducting magnet. Our home-built STM head is compact (51.5 mm long and 20 mm in diameter) and has a single arm that provides complete openness in the scanning area between the tip and sample. The STM head consists of two piezoelectric tubes (PTs), a piezoelectric scanning tube (PST) mounted on a well-polished zirconia shaft, and a large PT housed in a sapphire tube called the motor tube. The main body of the STM head is made of tantalum. In this design, we fixed the sapphire tube to the frame with screws so that the tube's position can be changed quickly. To analyse the stiffness of the STM head unit, we identified the lowest eigenfrequencies with 3 and 4 kHz in the bending modes, 8 kHz in a torsional mode, and 9 kHz in a longitudinal mode by finite element analysis, and also measured the low drift rates in the XY plane and in the Z direction. The high performance of the home-built STM was demonstrated by images of the hexagonal graphite lattice at 300 K and in a sweeping magnetic field from 0 T to 9 T. Our results confirm the high stability, vibration resistance, insensitivity to high magnetic fields and the application potential of our newly developed STM for the investigation of low-frequency systems with high static support stiffness in physics, chemistry, material and biological sciences.

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来源期刊
Accounts of Chemical Research
Accounts of Chemical Research 化学-化学综合
CiteScore
31.40
自引率
1.10%
发文量
312
审稿时长
2 months
期刊介绍: Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.
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