使用针式捕集器进行挥发性有机化合物采样和分析

Ga-Yeong Jeong , Jun-Ho Kim , Yong-seok Hong , Pil-Gon Kim , In-Yong Eom
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引用次数: 0

摘要

挥发性有机化合物(VOCs)毒性很强,对生物体有害,是军事基地和工业场地等污染区的主要污染物。作为场地评估的一部分,需要对挥发性有机化合物进行定性和定量分析。挥发性有机化合物分析通常需要经过几个复杂的步骤,如溶剂萃取、反向萃取和纯化。针式捕集器(NTD)作为一种微型吸附采样器,可以改进和简化这一分析过程。NTD 是一种采样、样品制备和进样一步完成的装置,专为气相色谱法而优化,由于无需使用萃取溶剂从样品基质中提取挥发性有机化合物,因此非常环保。本报告利用 NTD 的优势,报告监测井的采样和分析结果。报告利用 NTD 的优势,报告了监测井的采样和分析结果,即确定了七种挥发性有机化合物,并成功地找出了它们随采样深度的浓度梯度。随着挥发性有机化合物远离受污染的地下水,它们通过扩散呈指数下降,其中四氯乙烯是在 1.5 米深度检测到的最多的成分,浓度为 80.74 纳克/毫升。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Volatile organic compounds sampling and analysis using needle trap device

Volatile organic compounds sampling and analysis using needle trap device

Volatile organic compounds(VOCs) are very toxic and harmful to living organisms and easily found as major pollutans in contaminated areas such as military bases and industrial sites. Qualitative and quantitative analysis of VOCs is required as part of the site assessment. VOC analysis is usually followed several complex steps such as solvent extraction, reverse extraction, and purification. Needle Trap Devices (NTDs) as an miniaturized adsorbent sampler can improve and simplify this analysis process. NTD is a one-step sampling, sample preparation and injection device optimized for gas chromatography, which is eco-friendly because no extraction solvent is required to extract VOCs from the sample matrix. This report uses the advantages of NTD to report the results of sampling and analysis from the monitoring well. That is, seven VOCs were identified and their concentration gradients according to the sampling depth were successfully figured out. VOCs decreased exponentially by diffusion as they moved away from contaminated groundwater, of which Tetrachloroethylene was the most detected component at 80.74 ng/mL at a depth of 1.5 m.

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来源期刊
Journal of chromatography open
Journal of chromatography open Analytical Chemistry
CiteScore
2.50
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