利用 RSM 优化从柚子皮中提取纤维素的条件、表征及其与商用纤维素的比较研究

Rangina Brahma, Subhajit Ray
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引用次数: 0

摘要

目前,大量的研究工作都集中在利用生物基材料来解决 21 世纪发展中的问题上。因此,在这项科学工作中,我们探索了纤维素的新来源。在柚子中,果肉占 30%,70-80% 的柚子成分是不可食用的;其中约 60%是外皮、花被和中心核,通常会被丢弃。因此,为了利用这种未被充分利用的水果,人们考虑将柚子皮作为提取纤维素(C6H10O5)的来源。通过优化萃取参数,即氢氧化钠和次氯酸钠的浓度,采用响应面方法(RSM)改进了纤维素的萃取。结果表明,氢氧化钠浓度为 5%、次氯酸钠浓度为 2%时,纤维素产量最高,达到 64-65% 的最佳条件。利用傅立叶变换红外光谱频率检测到了 α - 纤维素的存在以及半纤维素和木质素的缺失。根据热重分析的结果,最大分解温度为 200 ºC 至 300 ºC。能量色散 X 射线分析显示,柚子皮纤维素的碳含量为 44%,而商用纤维素的碳含量为 3%,这表明柚子皮纤维素的纯度更高。与商用纤维素相比,柚子皮纤维素显示出更好的水结合能力和油保持能力。研究结果表明,柚子皮含有大量纤维素,有潜力用于食品、造纸、涂料等多个行业。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Optimization of extraction conditions for cellulose from jackfruit peel using RSM, its characterization and comparative studies to commercial cellulose

Optimization of extraction conditions for cellulose from jackfruit peel using RSM, its characterization and comparative studies to commercial cellulose

A high level of research effort is now being focused on the use of bio-based materials to address the 21st century's developing problems. Thus, the search for new possible source of cellulose has been explored in this scientific work. In jackfruit, the pulp accounts for 30 % and 70–80 % of jackfruit components are non-edible; about 60 % of them are the outer rind, perianth, and central core, which are usually discarded. So, in order to utilize this underutilized fruit, jackfruit peel has been taken into consideration as a source for cellulose (C6H10O5) n extraction. Cellulose extraction was improved using the response surface methodology (RSM) approach by optimizing the extraction parameters viz. concentration of sodium hydroxide and sodium hypochlorite respectively. The results showed that the best conditions for the highest production of 64–65 % of cellulose were 5 % of sodium hydroxide and 2 % of sodium hypochlorite. The presence of α -cellulose and the absence of hemicellulose and lignin were detected using FTIR frequencies. According to the results of the thermogravimetric investigation, the maximum decomposition occurred between 200 ºC and 300 ºC. Energy dispersive X-ray analysis revealed that jackfruit peel cellulose displayed 44 % carbon as compared to 3 % carbon in commercial cellulose, indicating a higher purity. Compared to commercial cellulose, jackfruit peel cellulose shows better water binding capacity and oil holding capacity. The findings imply that jackfruit peel has a considerable amount of cellulose and has the potential to be used in various industries such as food, paper, paints etc.

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